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1.
J Appl Crystallogr ; 56(Pt 4): 1032-1037, 2023 Aug 01.
Artigo em Inglês | MEDLINE | ID: mdl-37555222

RESUMO

The CITIUS detector is a next-generation high-speed X-ray imaging detector. It has integrating-type pixels and is designed to show a consistent linear response at a frame rate of 17.4 kHz, which results in a saturation count rate of over 30 Mcps pixel-1 when operating at an acquisition duty cycle close to 100%, and up to 20 times higher with special extended acquisition modes. Here, its application for Bragg coherent diffraction imaging is demonstrated by taking advantage of the fourth-generation Extremely Brilliant Source of the European Synchrotron (ESRF-EBS, Grenoble, France). The CITIUS detector outperformed a photon-counting detector, similar spatial resolution being achieved (20 ±â€…6 nm versus 22 ±â€…9 nm) with greatly reduced acquisition times (23 s versus 200 s). It is also shown how the CITIUS detector can be expected to perform during dynamic Bragg coherent diffraction imaging measurements. Finally, the current limitations of the CITIUS detector and further optimizations for coherent imaging techniques are discussed.

2.
Sensors (Basel) ; 23(7)2023 Mar 25.
Artigo em Inglês | MEDLINE | ID: mdl-37050510

RESUMO

Pixelated LGADs have been established as the baseline technology for timing detectors for the High Granularity Timing Detector (HGTD) and the Endcap Timing Layer (ETL) of the ATLAS and CMS experiments, respectively. The drawback of segmenting an LGAD is the non-gain area present between pixels and the consequent reduction in the fill factor. To overcome this issue, the inverse LGAD (iLGAD) technology has been proposed by IMB-CNM to enhance the fill factor and provide excellent tracking capabilities. In this work, we explore the use of iLGAD sensors for surface damage irradiation by developing a new generation of iLGADs, the periphery of which is optimized to improve the performance of irradiated sensors. The fabricated iLGAD sensors exhibit good electrical performances before and after X-ray irradiation.

3.
Sensors (Basel) ; 21(4)2021 Feb 23.
Artigo em Inglês | MEDLINE | ID: mdl-33672262

RESUMO

Chromium compensated GaAs or GaAs:Cr sensors provided by the Tomsk State University (Russia) were characterized using the low noise, charge integrating readout chip JUNGFRAU with a pixel pitch of 75 × 75 µm2 regarding its application as an X-ray detector at synchrotrons sources or FELs. Sensor properties such as dark current, resistivity, noise performance, spectral resolution capability and charge transport properties were measured and compared with results from a previous batch of GaAs:Cr sensors which were produced from wafers obtained from a different supplier. The properties of the sample from the later batch of sensors from 2017 show a resistivity of 1.69 × 109 Ω/cm, which is 47% higher compared to the previous batch from 2016. Moreover, its noise performance is 14% lower with a value of (101.65 ± 0.04) e- ENC and the resolution of a monochromatic 60 keV photo peak is significantly improved by 38% to a FWHM of 4.3%. Likely, this is due to improvements in charge collection, lower noise, and more homogeneous effective pixel size. In a previous work, a hole lifetime of 1.4 ns for GaAs:Cr sensors was determined for the sensors of the 2016 sensor batch, explaining the so-called "crater effect" which describes the occurrence of negative signals in the pixels around a pixel with a photon hit due to the missing hole contribution to the overall signal causing an incomplete signal induction. In this publication, the "crater effect" is further elaborated by measuring GaAs:Cr sensors using the sensors from 2017. The hole lifetime of these sensors was 2.5 ns. A focused photon beam was used to illuminate well defined positions along the pixels in order to corroborate the findings from the previous work and to further characterize the consequences of the "crater effect" on the detector operation.

4.
J Synchrotron Radiat ; 26(Pt 4): 1226-1237, 2019 Jul 01.
Artigo em Inglês | MEDLINE | ID: mdl-31274448

RESUMO

Recent advances in segmented low-gain avalanche detectors (LGADs) make them promising for the position-sensitive detection of low-energy X-ray photons thanks to their internal gain. LGAD microstrip sensors fabricated by Fondazione Bruno Kessler have been investigated using X-rays with both charge-integrating and single-photon-counting readout chips developed at the Paul Scherrer Institut. In this work it is shown that the charge multiplication occurring in the sensor allows the detection of X-rays with improved signal-to-noise ratio in comparison with standard silicon sensors. The application in the tender X-ray energy range is demonstrated by the detection of the sulfur Kα and Kß lines (2.3 and 2.46 keV) in an energy-dispersive fluorescence spectrometer at the Swiss Light Source. Although further improvements in the segmentation and in the quantum efficiency at low energy are still necessary, this work paves the way for the development of single-photon-counting detectors in the soft X-ray energy range.

6.
J Synchrotron Radiat ; 21(Pt 5): 986-95, 2014 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-25177987

RESUMO

Although beamline instrumentation is by nature driven by science, some recent examples serve as reminders that new technologies also enable new science. Indeed, exploiting the full scientific potential of forthcoming new storage rings with unprecedented source characteristics will, in many cases, require the development and implementation of novel instrumentation. In comparison with present synchrotron radiation facilities, the majority of beamlines should reap immediate performance benefits from the improved source emittance, principally through increased flux and/or horizontal beam size reduction at the sample. Instrumentation will have to develop along similar quantitative and qualitative trends. More speculative and more challenging is anticipating instrumentation that will be required by the new science made possible thanks to the unique coherence properties of diffraction-limited storage rings (DLSRs). ESRF has recently carried out a detailed feasibility study for a new ultra-low-emittance 6 GeV hybrid multibend storage ring, identified as ESRF Upgrade Programme Phase II. Although its performance is not expected to be equivalent to a DLSR source, the successful implementation of the ESRF Phase II project has to address scientific instrumentation issues that are also common to DLSRs. This article aims at providing a comprehensive review of some of the challenges encountered by the ESRF, in the context of the preparation of Phase II of its upgrade programme.

7.
Artigo em Inglês | MEDLINE | ID: mdl-23944598

RESUMO

This Brief Report studies the linear stability of a thermoconvective problem in an annular domain for relatively low (~1) Prandtl (viscosity effects) and Biot (heat transfer) numbers. The four possible patterns for the instabilities, namely, hydrothermal waves of first and second class, longitudinal rolls, and corotating rolls, are present in a small region of the Biot-Prandtl plane. This region can be split in four zones, depending on the sort of instability found. The boundary of these four zones is composed of codimension-two points. Authors have also found two codimension-three points, where some of the former curves intersect. Results shown in this Brief Report clarify some reported experiments, predict new instabilities, and, by giving a deeper insight into how physical parameters affect bifurcations, open a gateway to control those instabilities.


Assuntos
Temperatura Alta , Modelos Teóricos , Viscosidade
8.
J Synchrotron Radiat ; 13(Pt 3): 227-38, 2006 May.
Artigo em Inglês | MEDLINE | ID: mdl-16645249

RESUMO

The demand for access to macromolecular crystallography synchrotron beam time continues to increase. To meet this demand the ESRF has constructed a dual station beamline using a canted undulator system as the X-ray source. The first phase of the beamline to be constructed is ID23-1, a tunable MAD-capable station with a mini-focus X-ray beam. The beamline makes use of well characterized optical elements: a channel-cut monochromator with a high-precision toroidal mirror to focus the X-ray beam. The beamline has been conceived with the aim of providing high levels of automation to create an industrial-like environment for protein crystallography. A new software suite has been developed to permit reliable easy operation for the beamline users and beamline staff. High levels of diagnostics are built in to allow rapid trouble-shooting. These developments are now being exported to the ESRF macromolecular crystallography beamline complex and have been made in a modular fashion to facilitate transportability to other synchrotrons.


Assuntos
Cristalografia por Raios X/instrumentação , Óptica e Fotônica/instrumentação , Robótica/instrumentação , Síncrotrons/instrumentação , Desenho de Equipamento , França
9.
Rev. cient. (Bogotá) ; 1(2): 12-13, jul.-dic. 1995.
Artigo em Espanhol | LILACS | ID: lil-385965

RESUMO

El legado histórico de nuestra cultura expone una serie de circunstancias que evidencian el manejo práctico y ritual de las piezas dentales como parte de una concepción integrada de elementos cosmogónicos necesarios para la sobrevivencia. La conquista y la colonia representaron un período de presencias y ausencias en la cultura nacional que marcaron los intereses por la explotación de los recursos humanos y naturales, que por otra parte, hoy nos muestra los vacíos en la retribución a nuestro pueblo.


Assuntos
Odontologia
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