RESUMO
The AZ91 magnesium alloy was subjected to a complex treatment involving age hardening (supersaturation and artificial aging) and simultaneous surface layer modification. The specimens were supersaturated in contact with a mixture containing varying concentrations of zinc chloride, followed by cooling either in air or water. After supersaturation, the specimens were subjected to artificial aging and then air-cooled. This process resulted in the formation of a surface layer made of zinc-rich phases. The thickness and microstructure of the surface layer were influenced by the process parameters, namely, the zinc chloride content in the mixture and the cooling rate during supersaturation. The treated specimens exhibited favorable tensile strength and greater elongation compared to the as-cast AZ91 alloy, with values comparable to those of the alloy subjected to standard T6 tempering. No cracking of the layer was observed under moderate deformation, though greater deformation resulted in the formation of cracks, primarily in the areas containing the Mg5Al2Zn2 intermetallic phase. The produced layer demonstrated strong metallurgical bonding to the AZ91 substrate.
RESUMO
Continuous cooling transformation (CCT) diagrams are widely used when heat treating steels and represent which type of phase will occur in a material as it is cooled at different cooling rates. CCT diagrams are constructed on the basis of dilatometry measurements on relatively small testing samples (cylindrical shape with diameter of 4mm and length of 11 mm in this study). The main aim of this work was to demonstrate the possibility of evaluating the tensile test properties using mini-tensile tests from miniature volumes (1.4 × 10-7 m3 for one sample) subsequent to determination of the CCT diagram and to extend a standard CCT diagram with information about strength, ductility and the estimated value of the work-hardening coefficient. Mini-tensile tests (MTT) were recently developed due to the low availability of experimental material and have already been successfully used for local mechanical property characterization of metals. CCT diagrams were constructed for 42CrMo4 steel prepared by the laser-directed energy deposition (L-DED) process, for commercially available 42CrMo4 steel conventionally manufactured (for comparison of traditional processing and AM preparation) and for H13 tool steel deposited by the selective laser melting (SLM) process.
RESUMO
An ultrafine-grained EN AW 6082 aluminum alloy was prepared by continuous serve plastic deformation (i.e., thermo-mechanical equal channel angular pressing (ECAP)-Conform process). A miniaturized tensile testing technique was used for estimating local mechanical properties with the aim to reveal the inhomogeneity of elastic and plastic properties in a workpiece volume. These inhomogeneities may appear due to the irregular shear strain distribution in a Conformed wire. Miniaturized samples for tensile testing were cut from the Conformed workpiece. Elongation of miniaturized samples was measured with a 2D digital image correlation technique as the optical extensometer. Tensile test characteristics, such as the yield strength and ultimate tensile strength, were consequently compared with results of conventional and hardness tests. The microstructure of Conformed bars was studied in the cross-section perpendicular and parallel to the extrusion direction using scanning electron microscope (SEM) and electron backscatter diffraction (EBSD) analysis. The microstructure of samples exhibits pronounced inhomogeneity, which is reflected by the hardness and tensile test results. Estimated distinctions between peripheral and central parts of the Conformed wires are probably a consequence of the significant strain differences realized in the upper and bottom wire parts.