Influence of Imposed Strain on Weldability of Dievar Alloy.

The presented work is focused on the influence of imposed strain on the weldability of Dievar alloy. Two mechanisms affecting the microstructure and thus imparting changes in the mechanical properties were applied-heat treatment (hardening and tempering), and rotary swaging. The processed workpieces were further subjected to welding with various welding currents. In order to characterize the effects of welding on the microstructure, especially in the heat-affected zone, and determine material stability under elevated temperatures, samples for uniaxial hot compression testing at temperatures from 600 to 900 °C, optical and scanning electron microscopy, and microhardness testing were taken. The testing revealed that, although the rotary swaged and heat-treated samples featured comparable microhardness, the strength of the swaged material was approximately twice as high as that of the heat-treated one-specifically 1350 MPa. Furthermore, it was found that the rotary swaged sample exhibited favorable welding behavior when compared to the heat-treated one, when the higher welding current was applied.

Structural Phenomena Introduced by Rotary Swaging: A Review.

Rotary swaging is an industrially applicable intensive plastic deformation method. Due to its versatility, it is popular, especially in the automotive industry. Similar to the well-known methods of severe plastic deformation (SPD), rotary swaging imparts high shear strain into the swaged materials and thus introduces grain refinement down to a very fine, even ultra-fine, level. However, contrary to SPD methods, one of the primary characteristics of which is that they retain the shapes and dimensions of the processed sample, rotary swaging enables the imparting of required shapes and dimensions of workpieces (besides introducing structure refinement and the consequent enhancement of properties and performance). Therefore, under optimized conditions, swaging can be used to process workpieces of virtually any metallic material with theoretically any required dimensions. The main aim of this review is to present the principle of the rotary swaging method and its undeniable advantages. The focus is primarily on assessing its pros and cons by evaluating the imparted microstructures.

Effect of Stacking Sequence on Mechanical Properties and Microstructural Features within Al/Cu Laminates.

The study presents a method to prepare Al/Cu laminated conductors featuring two different stacking sequences using rotary swaging, a method of intensive plastic deformation. The primary focus of the work was to perform detailed characterization of the effects of room temperature swaging on the development of microstructures, including the Al/Cu interfaces, and internal misorientations pointed to the presence of residual stress within the laminates. The results revealed that both the Al and Cu components of the final laminates with 5 mm in diameter featured fine, more or less equiaxed, grains with no dominating preferential texture orientations (the maximum observed texture intensity was 2.3 × random for the Cu components of both the laminates). This fact points to the development of dynamic restoration processes during swaging. The analyses of misorientations within the grains showed that residual stress was locally present primarily in the Cu components. The Al components did not feature a substantial presence of misorientations, which confirms the dynamic recrystallization. Tensile testing revealed that the laminates with both the designed stacking sequences exhibited comparable UTS (ultimate tensile strength) of almost 280 MPa. However, notable differences were observed with regard to the plasticity (~3.5% compared to less than 1%). The laminate consisting of Al sheath and Cu wires exhibited very low plasticity as a result of significant work hardening of Al; this hypothesis was also confirmed with microhardness measurements. Observations of the interfaces confirmed satisfactory bonding of both the metallic components.

High Pressure Torsion of Copper; Effect of Processing Temperature on Structural Features, Microhardness and Electric Conductivity.

By optimizing the fabrication method, copper components featuring (typically contradicting) advantageous electric conductivity and favorable mechanical properties can be acquired. In this study, we subjected conventional electroconductive copper to a single revolution of high pressure torsion (HPT) at room temperature (RT), searched for the conditions which would yield comparable structure characteristics (grain size) when deformed at a cryogenic temperature, and finally compared the mechanical and electric behaviors to assess specific differences and correlate them with the (sub)structural development. 180° revolution of cryo-HPT imparted structure refinement comparable to 360° revolution of room temperature HPT, i.e., the average grain size at the periphery of both the specimens was ~7 µm. The 360° RT HPT specimen exhibited preferential (111)||SD (shear direction) texture fiber in all the examined regions, whereas the 180° cryo-HPT specimen exhibited more or less randomly oriented grains of equiaxed shapes featuring substantial substructure development of a relatively homogeneous character and massive occurrence of (nano)twins. These structural features resulted in the increase in microhardness to the average value of 118.2 HV0.2 and the increase in the electric conductivity to 59.66 MS·m-1 (compared to 105 HV0.2 and 59.14 MS·m-1 acquired for the 360° RT HPT specimen). The deformation under the cryogenic conditions also imparted higher homogeneity of microhardness distribution when compared to RT processing.

Affecting Microstructure and Properties of Additively Manufactured AISI 316L Steel by Rotary Swaging.

The presented work focused on the development of the microstructural and mechanical properties of a AISI 316L stainless steel workpiece prepared through additive manufacturing and subsequently processed by hot rotary swaging. In order to characterize the effects of swaging on the structural development, samples were taken for electron microscopy scanning and microhardness measurements were taken after each swaging reduction. The as-built and final swaged pieces were also subjected to tensile testing at room temperature and at 900 °C. The structural analyses showed that the hot swaging introduced a substructural formation; low angle grain boundaries prevailed over high angle ones after each pass. The swaging also imparted an almost complete elimination of the porosity and significant grain size; the average grain area decreased from the original value of 365.5 µm2 to 4.4 µm2 after the final swaging pass. The changes in the texture between the passes were negligible, however, the grain refinement went hand in hand with the microhardness increase (up to almost 300 HV1). The results of the tensile testing confirmed that the mechanical properties of the swaged pieces which improved dramatically and remained favorable up to high temperatures.

Grain Structure Engineering of NiTi Shape Memory Alloys by Intensive Plastic Deformation.

To explore an effective route of customizing the superelasticity (SE) of NiTi shape memory alloys via modifying the grain structure, binary Ni55Ti45 (wt) alloys were fabricated in as-cast, hot swaged, and hot-rolled conditions, presenting contrasting grain sizes and grain boundary types. In situ synchrotron X-ray Laue microdiffraction and in situ synchrotron X-ray powder diffraction techniques were employed to unravel the underlying grain structure mechanisms that cause the diversity of SE performance among the three materials. The evolution of lattice rotation, strain field, and phase transformation has been revealed at the micro- and mesoscale, and the effect of grain structure on SE performance has been quantified. It was found that (i) the Ni4Ti3 and NiTi2 precipitates are similar among the three materials in terms of morphology, size, and orientation distribution; (ii) phase transformation happens preferentially near high-angle grain boundary (HAGB) yet randomly in low-angle grain boundary (LAGB) structures; (iii) the smaller the grain size, the higher the phase transformation nucleation kinetics, and the lower the propagation kinetics; (iv) stress concentration happens near HAGBs, while no obvious stress concentration can be observed in the LAGB grain structure during loading; (v) the statistical distribution of strain in the three materials becomes asymmetric during loading; (vi) three grain lattice rotation modes are identified and termed for the first time, namely, multi-extension rotation, rigid rotation, and nondispersive rotation; and (vii) the texture evolution of B2 austenite and B19' martensite is not strongly dependent on the grain structure.

Characterising Correlations between Electric Conductivity and Structural Features in Rotary Swaged Al/Cu Laminated Conductors.

This study aims to characterize the correlations between electric characteristics and selected structural features of newly designed Al/Cu laminated conductors manufactured via room temperature rotary swaging. After swaging, the laminates with diameters of 15 mm were subjected to two different post-process annealing treatments. Structure analyses performed to evaluate the effects of thermomechanical processing were performed via scanning and transmission electron microscopies. Electric conductivity and resistivity of the laminates were experimentally measured and numerically simulated using models designed according to the real conditions. The results showed that the electric resistivity was affected by the grain size, bimodal grains' distribution (where observed), the presence of twins, and, last but not least, dislocation density. Among the influencing factors were the area fractions of Al and Cu at the cross-sections of the of the laminated conductors, too. The results revealed that fabrication of the laminate via the technology of rotary swaging introduced more advantageous combinations of electric and mechanical properties than fabrication by conventional manufacturing techniques. The lowest specific electric resistivity of 20.6 Ωm × 10-9 was measured for the laminated conductor subjected to the post-process annealing treatment at 350 °C, which imparted significant structure restoration (confirmed by the presence of fine, equiaxed, randomly oriented grains).

Influence of (Sub) Structure Development within Rotary Swaged Al-Cu Clad Conductors on Skin Effect during Transfer of Alternating Current.

The nature of alternating current transfer via metallic materials is specific, since the current density tends to be inhomogeneous across the cross-section of the conductor and the skin effect tends to occur. However, the influence of this effect on the behaviour of the conductor can be optimized via the design and fabrication procedures. The study presents innovative design of an Al-Cu clad conductor, which is supposed to affect favourably the influence of the skin effect. The clad conductors of various diameters (20 mm, 15 mm, and 10 mm) were fabricated via rotary swaging at room temperature, and their electric characteristics were subsequently examined both experimentally and via numerical simulations. Structure analyses performed to document the effects of the swaging technology on the development of substructure and characteristic structural features were carried out by scanning electron microscopy (electron backscatter diffraction analyses), and transmission electron microscopy. The results showed that the design of the composite has a favourable effect on decreasing the power losses during alternating current transfer and that the substructure development affected favourably the electric resistance of the conductor. The highest electric resistance was measured for the composite conductor with the diameter of 20 mm (1.8% increase compared to electric resistance during transfer of direct current). This value then decreased to 0.6%, and 0.1% after swaging down to the diameters of 15 mm, and 10 mm; the 10 mm composite featured the finest grains, partially restored structure, and texture randomization compared to the 20 mm and 15 mm composites. Manufacturing of the clad composite via rotary swaging imparted advantageous combinations of both the electric and mechanical properties, as swaging also introduced increased microhardness.

Determining Johnson-Cook Constitutive Equation for Low-Carbon Steel via Taylor Anvil Test.

Tristal steel is low-carbon construction-type steel widely used in the automotive industry, e.g., for braking components. Given the contemporary demands on the high-volume production of such components, these are typically fabricated using automatic sequential machines, which can produce components at strain rates up to 103 s-1. For this reason, characterising the behaviour of the used material at high strain rates is of the utmost importance for successful industrial production. This study focuses on the characterisation of the behaviour of low-carbon steel via developing its material model using the Johnson-Cook constitutive equation. At first, the Taylor anvil test is performed. Subsequently, the acquired data together with the results of observations of structures and properties of the tested specimens are used to fill the necessary parameters into the equation. Finally, the developed equation is used to numerically simulate the Taylor anvil test and the predicted data is correlated with the experimentally acquired one. The results showed a satisfactory correlation of the experimental and predicted data; the deformed specimen region featured increased occurrence of dislocations, as well as higher hardness (its original value of 88 HV increased to more than 200 HV after testing), which corresponded to the predicted distributions of effective imposed strain and compressive stress.

Structural Factors Inducing Cracking of Brass Fittings.

Cu-Zn-Pb brasses are popular materials, from which numerous industrially and commercially used components are fabricated. These alloys are typically subjected to multiple-step processing-involving casting, extrusion, hot forming, and machining-which can introduce various defects to the final product. The present study focuses on the detailed characterization of the structure of a brass fitting-i.e., a pre-shaped medical gas valve, produced by hot die forging-and attempts to assess the factors beyond local cracking occurring during processing. The analyses involved characterization of plastic flow via optical microscopy, and investigations of the phenomena in the vicinity of the crack, for which we used scanning and transmission electron microscopy. Numerical simulation was implemented not only to characterize the plastic flow more in detail, but primarily to investigate the probability of the occurrence of cracking based on the presence of stress. Last, but not least, microhardness in specific locations of the fitting were examined. The results reveal that the cracking occurring in the location with the highest probability of the occurrence of defects was most likely induced by differences in the chemical composition; the location the crack in which developed exhibited local changes not only in chemical composition-which manifested as the presence of brittle precipitates-but also in beta phase depletion. Moreover, as a result of the presence of oxidic precipitates and the hard and brittle alpha phase, the vicinity of the crack exhibited an increase in microhardness, which contributed to local brittleness.

Special Issue: Selected Papers from Experimental Stress Analysis 2020.

The contemporary way of living brings about increasing demands on materials used in our everyday lives [...].

Monotonic Tension-Torsion Experiments and FE Modeling on Notched Specimens Produced by SLM Technology from SS316L.

The aim of this work was to monitor the mechanical behavior of 316L stainless steel produced by 3D printing in the vertical direction. The material was tested in the "as printed" state. Digital Image Correlation measurements were used for 4 types of notched specimens. The behavior of these specimens under monotonic loading was investigated in two loading paths: tension and torsion. Based on the experimental data, two yield criteria were used in the finite element analyses. Von Mises criterion and Hill criterion were applied, together with the nonlinear isotropic hardening rule of Voce. Subsequently, the load-deformation responses of simulations and experiments were compared. Results of the Hill criterion show better correlation with experimental data. The numerical study shows that taking into account the difference in yield stress in the horizontal direction of printing plays a crucial role for modeling of notched geometries loaded in the vertical direction of printing. Ductility of 3D printed specimens in the "as printed" state is also compared with 3D printed machined specimens and specimens produced by conventional methods. "As printed" specimens have 2/3 lower ductility than specimens produced by a conventional production method. Machining of "as printed" specimens does not affect the yield stress, but a significant reduction of ductility was observed due to microcracks arising from the pores as a microscopic surface study showed.

The Effect of Predeformation on Creep Strength of 9% Cr Steel.

Martensitic creep-resistant P92 steel was deformed by different methods of severe plastic deformation such as rotation swaging, high-pressure sliding, and high-pressure torsion at room temperature. These methods imposed significantly different equivalent plastic strains of about 1-30. It was found that rotation swaging led to formation of heterogeneous microstructures with elongated grains where low-angle grain boundaries predominated. Other methods led to formation of ultrafine-grained (UFG) microstructures with high frequency of high-angle grain boundaries. Constant load tensile creep tests at 873 K and initial stresses in the range of 50 to 300 MPa revealed that the specimens processed by rotation swaging exhibited one order of magnitude lower minimum creep rate compared to standard P92 steel. By contrast, UFG P92 steel is significantly softer than standard P92 steel, but differences in their strengths decrease with increasing stress. Microstructural results suggest that creep behavior of P92 steel processed by severe plastic deformation is influenced by the frequency of high-angle grain boundaries and dynamic grain coarsening during creep.

Fundamental Improvement of Creep Resistance of New-Generation Nano-Oxide Strengthened Alloys via Hot Rotary Swaging Consolidation.

New-generation oxide dispersion-strengthened (ODS) alloys with a high volume fraction of nano-oxides of 5% are intended to become the leading creep- and oxidation-resistant alloys for applications at 1100-1300 °C. Hot consolidation of mechanically alloyed powders by intensive plastic deformation followed by heat treatment of the alloys are the key aspects for achieving top creep properties, typically ensured by a coarse-grained microstructure strengthened with homogeneously dispersed, very stable yttrium nano-oxides. The rotary swaging method proves to be favourable for hot consolidation of the new-generation ODS alloy presented. Compared to specimens consolidated by hot rolling, consolidation by hot rotary swaging predetermines the formation of coarse grains with a very high aspect ratio during subsequent secondary recrystallization. Such a grain morphology increases the creep strength of the new-generation ODS alloy considerably.

Special Issue: Mechanical Properties in Progressive Mechanically Processed Metallic Materials.

The research and development of modern metallic materials imparts not only the introduction of innovative alloys and compounds, but also the increasing lifetime of existing materials via optimized deformation processing. Among the essential features of progressive metallic materials used for modern applications are enhanced mechanical properties, but also other high-level functional characteristics, such as thermal-physical parameters, corrosion rate, and electric resistance. The properties of materials and alloys ensue from their structures, which can primarily be affected by the preparation/production process. The Special Issue "Mechanical Properties in Progressive Mechanically Processed Metallic Materials" was established to present recent developments and innovations particularly in the engineering field. The Special Issue comprises papers dealing with modern materials, such as metallic composites and pseudoalloys, as well as developments in various processing technologies.

Structure Characteristics Affected by Material Plastic Flow in Twist Channel Angular Pressed Al/Cu Clad Composites.

The study focuses on structure analyses, texture analyses in particular, of an Al/Cu clad composite manufactured by single and double pass of the twist channel angular pressing (TCAP) method. Microscopic analyses were supplemented with numerical predictions focused on the effective imposed strain and material plastic flow, and microhardness measurements. Both the TCAP passes imparted characteristic texture orientations to the reinforcing Cu wires, however, the individual preferential grains' orientations throughout the composite differed and depended on the location of the particular wire within the Al sheath during extrusion, i.e., on the dominant acting strain path. The second TCAP pass resulted in texture homogenization; all the Cu wires finally exhibited dominant A fiber shear texture. This finding was in accordance with the homogenization of the imposed strain predicted after the second TCAP pass. The results also revealed that both the component metals exhibited significant deformation strengthening (which also caused bending of the ends of the Cu wires within the Al sheath after extrusion). The average microhardness of the Cu wires after the second pass reached up to 128 HV, while for the Al sheath the value was 86 HV.

Effects of Sintering Conditions on Structures and Properties of Sintered Tungsten Heavy Alloy.

Probably the most advantageous fabrication technology of tungsten heavy alloys enabling the achievement of required performance combines methods of powder metallurgy and processing by intensive plastic deformation. Since the selected processing conditions applied for each individual processing step affect the final structures and properties of the alloys, their optimization is of the utmost importance. This study deals with thorough investigations of the effects of sintering temperature, sintering time, and subsequent quenching in water on the structures and mechanical properties of a 93W6Ni1Co tungsten heavy alloy. The results showed that sintering at temperatures of or above 1525 °C leads to formation of structures featuring W agglomerates surrounded by the NiCo matrix. The sintering time has non-negligible effects on the microhardness of the sintered samples as it affects the diffusion and structure softening phenomena. Implementation of quenching to the processing technology results in excellent plasticity of the green sintered and quenched pieces of almost 20%, while maintaining the strength of more than 1000 MPa.

Correlating Microstrain and Activated Slip Systems with Mechanical Properties within Rotary Swaged WNiCo Pseudoalloy.

Due to their superb mechanical properties and high specific mass, tungsten heavy alloys are used in demanding applications, such as kinetic penetrators, gyroscope rotors, or radiation shielding. However, their structure, consisting of hard tungsten particles embedded in a soft matrix, makes the deformation processing a challenging task. This study focused on the characterization of deformation behavior during thermomechanical processing of a WNiCo tungsten heavy alloy (THA) via the method of rotary swaging at various temperatures. Emphasis is given to microstrain development and determination of the activated slip systems and dislocation density via neutron diffraction. The analyses showed that the grains of the NiCo2W matrix refined significantly after the deformation treatments. The microstrain was higher in the cold swaged sample (44.2 × 10-4). Both the samples swaged at 20 °C and 900 °C exhibited the activation of edge dislocations with <111> {110} or <110> {111} slip systems, and/or screw dislocations with <110> slip system in the NiCo2W matrix. Dislocation densities were determined and the results were correlated with the final mechanical properties of the swaged bars.

Affecting Structure Characteristics of Rotary Swaged Tungsten Heavy Alloy Via Variable Deformation Temperature.

This study focuses on numerical prediction and experimental investigation of deformation behaviour of a tungsten heavy alloy prepared via powder metallurgy and subsequent cold (20 °C) and warm (900 °C) rotary swaging. Special emphasis was placed on the prediction of the effects of the applied induction heating. As shown by the results, the predicted material behaviour was in good correlation with the real experiment. The differences in the plastic flow during cold and warm swaging imparted differences in structural development and the occurrence of residual stress. Both the swaged pieces exhibited the presence of residual stress in the peripheries of W agglomerates. However, the NiCO matrix of the warm-swaged piece also exhibited the presence of residual stress, and it also featured regions with increased W content. Testing of mechanical properties revealed the ultimate tensile strength of the swaged pieces to be approximately twice as high as of the sintered piece (860 MPa compared to 1650 MPa and 1828 MPa after warm and cold swaging, respectively).

Analysis of Deformation Behaviour and Residual Stress in Rotary Swaged Cu/Al Clad Composite Wires.

Both copper and aluminum are widely applicable throughout a variety of industrial and commercial branches, however, joining them in a composite provides the possibility of combining all their advantageous properties in one material. This study investigates uniquely sequenced copper-aluminum clad composite wires, fabricated via rotary swaging technology. The composites were processed at 20 °C and 250 °C to a diameter of 5 mm. Structural observations and the determination of residual stress within both elements of the swaged wires were performed via electron microscopy; the experimental results were correlated with numerical predictions. As shown in the results, both the applied swaging force and temperature affected the plastic flow, which had a direct influence on residual stress and texture development; the Alsheath elements exhibited ideal rolling textures, whereas the Cuwires elements featured ideal shear texture orientation. The grains within both the Alsheath elements of the 5 mm composite wire were refined down to sub-micron size. Structural restoration also had a positive influence on residual stress.