Kinetic of Light Transmission during Setting and Aging of Modern Flowable Bulk-Fill Composites.

The current development of dental materials aims to improve their properties and expand their clinical application. New flowable bulk-fill composites have been released which, unlike what was previously common in this material category, are intended to be used alone and without a top layer, in various cavities. The study compares their kinetic of light transmission during monomer-to-polymer conversion on a laboratory-grade spectrometer, as well as their elastoplastic and aging behavior under simulated clinical conditions. Major differences in the kinetic of light transmission was observed, which is related to the degree of mismatch between the refractive indices of filler and polymer matrix during polymerization and/or the type of initiator used. Compared to the literature data, the kinetic of light transmission do not always correlate with the kinetic of functional group conversion, and therefore should not be used to assess polymerization quality or to determine an appropriate exposure time. Furthermore, the initial mechanical properties are directly related to the volumetric amount of filler, but degradation during aging must be considered as a multifactorial event.

Shrinkage and Creep Properties of Low-Carbon Hybrid Cement.

Hybrid cements combine clinker with large amount of supplementary cementitious materials while utilizing hydration and alkali activation processes. This paper summarizes shrinkage and creep properties of industrially produced H-cement, containing only 20% of Portland clinker. In comparison with a reference cement CEM II/B-S 32.5 R, autogenous shrinkage is smaller after 7 days, and drying shrinkage is similar at similar times. A different capillary system of H-cement leads to faster water mass loss during drying. Basic and total creep of concrete remains in the standard deviation of B4 and EC2 creep models. The results demonstrate that shrinkage and creep properties of concrete made from H-cement have similar behavior as conventional structural concrete or high-volume fly ash concrete.

Machine learning-based predictions and analyses of the creep rupture life of the Ni-based single crystal superalloy.

The evaluation of creep rupture life is complex due to its variable formation mechanism. In this paper, machine learning algorithms are applied to explore the creep rupture life span as a function of 27 physical properties to address this issue. By training several classical machine learning models and comparing their prediction performance, XGBoost is finally selected as the predictive model for creep rupture life. Moreover, we introduce an interpretable method, Shapley additive explanations (SHAP), to explain the creep rupture life predicted by the XGBoost model. The SHAP values are then calculated, and the feature importance of the creep rupture life yielded by the XGBoost model is discussed. Finally, the creep fracture life is optimized by using the chaotic sparrow optimization algorithm. We then show that our proposed method can accurately predict and optimize creep properties in a cheaper and faster way than other approaches in the experiments. The proposed method can also be used to optimize the material design across various engineering domains.

Age-dependence of semitendinosus tendon properties used for anterior cruciate ligament reconstruction differs in males and females.

BACKGROUND: The semitendinosus tendon is one of the most used autografts in anterior cruciate ligament reconstruction. Although recent evidence indicates that young patients, especially in females, may experience high rates of revision and residual instability, the reasons for the inferior outcomes in these patients remain unclear. To address this issue, we aimed to compare the mechanical properties of the semitendinosus tendon used for anterior cruciate ligament reconstruction in male and female patients of various ages. METHODS: The semitendinosus tendons harvested from 31 male and 29 female patients who underwent anterior cruciate ligament reconstruction surgery using the semitendinosus tendon autografts were used in this study. Using the distal part of the harvested semitendinosus tendon, the extent of cyclic loading-induced elongation (i.e., the extent of the increase in slack length) and the Young's modulus were measured during cyclic tensile testing. FINDINGS: Spearman correlation analyses revealed that the Young's modulus (|ρ| = 0.725, P < 0.001), but not elongation (|ρ| ≤ 0.036, P ≥ 0.351) positively correlated with the patient age in male tendon samples. In contrast, for female tendon samples, the elongation (|ρ| ≥ 0.415, P ≤ 0.025), but not the Young's modulus (|ρ| = 0.087, P = 0.655) negatively correlated with the patient age. INTERPRETATION: These results indicate that the semitendinosus tendon used for anterior cruciate ligament reconstruction in young male patients is compliant, whereas that in young female patients is susceptible to elongation induced by cyclic loading.

Effect of supplemental milk replacer and liquid starter diet for 4 and 11 days postweaning on intestinal parameters of weaned piglets and growth to slaughter.

Reduced piglet feed intake immediately postweaning (pw) leads to disruption of small intestine structure and function and reduced growth. Our objective was to evaluate the effect of providing supplemental milk or liquid starter diet for either 4 or 11 days pw, on intestinal parameters of newly weaned piglets and growth to slaughter. At weaning (28 ± 0.6 days old), five hundred and eighty-seven piglets ((Large White × Landrace) × Duroc) were divided into 59 pen groups, each containing 9-10 same sex (entire male or female) piglets. The pen groups were blocked by sex and weaning weight and provided with ad-libitum access to one of five dietary treatments: (1) Dry pelleted starter diet (control; CON); (2) CON+liquid milk replacer for 4 days pw (M4); (3) CON+liquid milk replacer for 11 days pw (M11); (4) CON+liquid starter diet for 4 days pw (S4) and (5) CON+liquid starter diet for 11 days pw (S11). Pen groups were weighed at weaning, days 11, 20, 28, and 47 pw and at target sale weight. Feed disappearance (on a DM basis) was recorded on each weighing day. On day 7 pw, 10 piglets per treatment were euthanised to collect small intestine tissue samples for determination of villus height (VH), crypt depth and brush-border membrane enzyme activity. Data were analysed using SAS-version 9.4. Between days 0 and 11 pw, M11 increased average daily feed intake by 48% and average daily gain (ADG) by 57% compared to CON (P < 0.05), and increased ADG by 54% (P < 0.05) compared to S4. Piglets on M11 also had improved feed conversion efficiency compared with CON piglets between days 0 and 11 pw. Treatment did not affect growth performance after day 28 pw, or carcass parameters at slaughter. At day 7 pw, M11 piglets had 37% higher jejunal VH than CON piglets (P < 0.05) and S11 piglets had 28% higher ileal VH than S4 piglets (P < 0.05). M11 piglets had up to 150% higher ileal sucrase activity than M4, S4 and S11 piglets (P < 0.05) and 180% higher ileal maltase activity than S4 piglets (P < 0.05). In conclusion, M11 reduced the immediate negative effects of weaning, as it was associated with increased feed intake, growth, brush-border membrane enzyme activity and improved intestinal structure early pw. However, there were no carryover effects of any of the liquid supplements on growth or feed efficiency or carcass weight at slaughter.

Cyclic Mechanism Affects Lumbar Spine Creep Response.

PURPOSE: This study aims to explore how cyclic loading influences creep response in the lumbar spine under combined flexion-compression loading. METHODS: Ten porcine functional spinal units (FSUs) were mechanically tested in cyclic or static combined flexion-compression loading. Creep response between loading regimes was compared using strain-time histories and linear regression. High-resolution computed tomography (µCT) visualized damage to FSUs. Statistical methods, ANCOVA and ANOVA, assessed differences in behavior between loading regimes. RESULTS: Cyclic and static loading regimes exhibited distinct creep response patterns and biphasic response. ANCOVA and ANOVA analyses revealed significant differences in slopes of creep behavior in both linear phases. Cyclic tests consistently showed endplate fractures in µCT imaging. CONCLUSION: The study reveals statistically significant differences in creep response between cyclic and static loading regimes in porcine lumbar spinal units under combined flexion-compression loading. The observed biphasic behavior suggests distinct phases of tissue response, indicating potential shifts in load transfer mechanisms. Endplate fractures in cyclic tests suggest increased injury risk compared to static loading. These findings underscore the importance of considering loading conditions in computational models and designing preventive measures for occupations involving repetitive spinal loading.

Study on the fractional creep model of roadway filling paste under the coupling effect of pore water pressure and stress.

Filling paste in deep roadways is significantly affected by groundwater, especially high pore water pressure, which increases the complexity and variability of the filling paste's mechanical properties. To explore the creep characteristics and long-term stability of filling paste under varying pore water pressure, the MTS815.03 test system is used to conduct creep tests under different pore water pressures and stress. Then the creep deformation of the filling paste under the complex pressure field of static pore water pressures is analyzed. Finally, through the one-to-one correspondence between the numerical simulation of the creep model and the characteristic points of the creep curve, a method for determining the creep parameters under the complex pressure field of static pore water pressures is proposed. Results show that the creep test curves of filling paste under different pore water pressures and stress are in good agreement with the model curves. This shows that the creep constitutive model in this research can better reflect the whole process of creep deformation of filling paste. The result also verifies the rationality of the proposed method to determine creep model parameters. The newly proposed creep model can effectively compensate for the traditional Nishihara model, which is inability to reflect the acceleration of creep and can more accurately describe the creep characteristics of the primary and steady-state creep stages.

"Unmasking a Looming Crisis: Escalating MIC of Last Resort Drugs against MRSA Isolates from a Tertiary Hospital in Central India."

PURPOSE: The Centers for Disease Control and Prevention has classified methicillin-resistant S aureus (MRSA) as a serious public health threat. The escalating minimum inhibitory concentration (MIC) of standard anti-methicillin-resistant S aureus (MRSA) drugs within the susceptible range, known as "MIC creep," jeopardizes their effectiveness against MRSA infections, posing additional challenges in managing MRSA infections. This cross-sectional study was conducted in a tertiary care hospital in Central India to assess the susceptibility trends of clinical MRSA isolates against commonly used anti-MRSA drugs and to observe MIC creep, if any, over three years (2020-2022). METHODS: The study included 158 non-repetitive clinical MRSA isolates. The MICs of vancomycin, teicoplanin, and linezolid were determined in MRSA strains using agar dilution, while the MIC of daptomycin was performed by broth microdilution. MIC creep was assessed by calculating MIC50, MIC90, Modal MIC, G-mean MIC, and susceptible and resistant percentages for the fiscal years 2020, 2021, and 2022. RESULTS: Of the 158 MRSA isolates, none were resistant to vancomycin, teicoplanin, and daptomycin, but two showed resistance to linezolid (LRSA). However, fifteen isolates showed intermediate resistance to vancomycin (VISA), and five showed intermediate resistance to teicoplanin (TISA). MIC of these anti-MRSA drugs increased in 2021 and 2022 compared to 2020. G-mean MIC for vancomycin, teicoplanin, and linezolid in MRSA strains increased significantly over the study period, while daptomycin MIC remained relatively stable, with a slight increase in 2021 and 2022. There was a high resistance rate for clindamycin, doxycycline, and chloramphenicol among VISA, TISA, and LRSA isolates compared to MRSA. CONCLUSIONS: During the three years of the study, "MIC creep" was observed in vancomycin, teicoplanin, and linezolid and, to some extent, for daptomycin in MRSA strains. The recovery of VISA, TISA, and linezolid-resistant MRSAs is worrisome, suggesting possible MRSA treatment failure and being a forerunner of resistant strains.

Nanoindentation Creep Behavior of Additively Manufactured H13 Steel by Utilizing Selective Laser Melting Technology.

Nowadays, H13 hot work steel is a commonly used hot work die material in the industry; however, its creep behavior for additively manufactured H13 steel parts has not been widely investigated. This research paper examines the impact of volumetric energy density (VED), a critical parameter in additive manufacturing (AM), and the effect of post heat-treatment nitrification on the creep behavior of H13 hot work tool steel, which is constructed through selective laser melting (SLM), which is a powder bed fusion process according to ISO/ASTM 52900:2021. The study utilizes nanoindentation tests to investigate the creep response and the associated parameters such as the steady-state creep strain rate. Measurements and observations taken during the holding phase offer a valuable understanding of the behavior of the studied material. The findings of this study highlight a substantial influence of both VED and nitrification on several factors including hardness, modulus of elasticity, indentation depth, and creep displacement. Interestingly, the creep strain rate appears to be largely unaltered by these parameters. The study concludes with the observation that the creep stress exponent (n) shows a decreasing trend with an increase in VED and the application of nitrification treatment.

Comprehensive rheological and mechanistic evaluation of an asphalt binder and mixture modified with warm mix additives.

Though warm mix asphalt (WMA) technology has been introduced for a long time, there is still reluctance in the industry to utilize it in practice. In regions like India, where WMA incorporation into road construction has been limited over the past two decades, building confidence in local binders is imperative for widespread adoption. Thus, the present study appraises the effect of three commonly used WMA additives in India, namely Sasobit®, Evotherm®, and Zycotherm®, with base binder VG-30 on the rheological and mixture performance parameters. Three dosages of each WMA additive were blended with the control binder to give ten binder combinations. Different binder evaluations such as Superpave grading and parameters, frequency sweep testing, multiple stress creep recovery test, and linear amplitude sweep test were conducted for comparative dynamic mechanical analysis. Based on the binder testing results, suitable dosages of WMA additives were established, and mixture testing was carried out using these specific additive dosages. Binder evaluations showed improvement in high-temperature characteristics with Sasobit® and better fatigue performance with Evotherm®, while Zycotherm® did not alter binder properties significantly. The asphalt mixture testing results indicated satisfactory performance with the three additives based on Marshall stability and flow testing. The WMA additives also showed enhancement in moisture susceptibility based on the modified Lottman test with Zycotherm® demonstrating the best performance. Overall, the study underscores promising effects of the three WMA additives across different parameters, signaling their potential for widespread application in real-world scenarios.

An experimental and theoretical study on the creep behavior of silt soil in the Yellow River flood area of Zhengzhou City.

We took the silt soil in the Yellow River flood area of Zhengzhou City as the research object and carried out triaxial shear and triaxial creep tests on silt soil with different moisture contents (8%, 10%, 12%, 14%) to analyze the effect of moisture content on silt soil. In addition, the influence of moisture contents on soil creep characteristics and long-term strength was analyzed. Based on the fractional derivative theory, we established a fractional derivative model that can effectively describe the creep characteristics of silt soil in all stages, and used the Levenberg-Marquardt algorithm to inversely identify the relevant parameters of the fractional derivative creep model. The results show that the shear strengths of silt soil samples with moisture contents of 8%, 10%, 12% and 14% are 294 kPa, 236 kPa, 179 kPa and 161 kPa, respectively. The shear strength of silt soil decreases with increasing moisture content. When the moisture content increases, the cohesion of the silt soil decreases. Under the same deviatoric stress, the higher the moisture content of the silt soil, the greater the deformation will be. The long-term strength of silt soil decreases exponentially with the increase of moisture content. If the moisture content is 12%, the long-term strength loss rate of silt soil is the smallest, with a value of 32.96%. The calculated values of our creep model based on fractional derivatives have a high goodness of fit with the experimental results. This indicates that our model can better simulate the creep characteristics of silt soil. This study can provide a theoretical basis for engineering construction and geological disaster prevention in silt soil areas in the Yellow River flood area.

Creep Failure Characteristics and Mathematical Modeling of High-Density Polyethylene Geomembranes under High Stress Levels.

To explore the creep characteristics of geomembrane under different tensile stresses, a series of creep tests were carried out on high-density polyethylene (HDPE) geomembrane specimens. For the interpretation and fitting of the experimental data, refined approximation functions were proposed. Particular attention was paid to the creep failure behavior under high tensile stresses, i.e., 70%, 80%, and 90% of maximum peak stress. To investigate the effects of size on the mechanical response, experiments with two different membrane thicknesses were conducted. The results obtained under high stress levels were compared with creep tests at medium and low stress levels. Depending on load level, different creep characteristics can be distinguished. In the secondary creep state, the creep velocity is higher for higher load levels. In contrast to the medium and low load levels, the geomembrane under high stresses underwent the tertiary creep stage after instantaneous deformation and primary and secondary creep stages. In some tests, it was observed that under very high stress levels, creep velocity does not necessarily follow the expected trend and creep rupture can occur within a short time. For numerical simulation, an improved mathematical model was proposed to reproduce in a unified manner the experimental data of the whole non-linear evolution of creep elongation under different stress levels.

The Effects of Combined Treatments of Laser Engraving, Plasma Spraying and Resin Pre-Coating on Improving the Bonding Strength of Titanium Alloy and Carbon Fiber-Reinforced Polymer.

This study focused on effective methods of laser engraving treatment (LET), plasma spraying, and resin pre-coating (RPC) to manufacture the reinforced adhesive joints of titanium alloy and carbon fiber-reinforced polymer (TA-CFRP) composites. The combined treatments contributed to the creation of a better adhesive bonding condition and offer a vertical gap between circular protrusions to form epoxy pins and carbon nanotube (CNT)-reinforced epoxy pins. The bonding strength of the TA-CFRP composite was reinforced by 130.6% via treatments with a twice-engraving unit of 0.8 mm, plasma spraying, and RPC. The original debonding failure on the TA surface was changed into the cohesive failure of the epoxy adhesive and delamination-dominated failure of the CFRP panel. Overall, laser engraving has been confirmed as an effective and controllable treatment method to reinforce the bonding strength of the TA-CFRP joint combined with plasma spraying and RPC. It may be considered as an alternative in industry for manufacturing high-performance metal-CFRP composites.

Research on the bearing creep characteristics and constitutive model of gangue filling body.

The creep characteristics and potential deformation patterns of gangue backfill material are crucial in backfill mining operations. This study utilizes crushed gangue from the Gangue Yard in Fuxin City as the research material. An in-house designed, large-scale, triaxial gangue compaction test system was used. Triaxial compaction creep tests were conducted on gangue materials with varying particle size distributions. Analysis was performed based on different particle sizes, stresses, and confinement pressures. The study investigates the creep characteristics of the gangue under different conditions and explores the underlying causes. It reveals the relationship between the creep deformation of gangue materials and the passage of time. Mathematical methods are applied to develop a triaxial compaction creep power law model for gangue backfill materials. Finally, the creep results are fitted using an empirical formula approach.

Analytical Calculation of Relationship Temperature and Fatigue and Creep Strength Based on Thermal Activation.

The purpose of this study was to formulate a mathematical expression for the temperature dependence of adhesive strength using various parameters. Adhesive structures are typically exposed to a broad temperature range, spanning from low to high temperatures; therefore, understanding how their strength depends on temperature is crucial. The strength was measured through tensile, fatigue, and creep tests at temperatures ranging from -60 °C to 135 °C. The properties of these test types were thoroughly investigated by analyzing the strength of the test results from a thermal activity perspective. The results demonstrate that there is a clear relationship between temperature and strength. The intensity decreased with temperature according to the exponential function and could be accurately represented using the parameters of thermal activity. The temperature at which the strength begins to decrease in the fatigue test was higher than in the static tests. Consequently, we were able to accurately express the relationship between the temperature and intensity using certain parameters. Few studies successfully developed a precise nonlinear relationship between temperature and intensity using approximate expressions.

Recent Progress in Creep-Resistant Aluminum Alloys for Diesel Engine Applications: A Review.

Diesel engines in heavy-duty vehicles are predicted to maintain a stable presence in the future due to the difficulty of electrifying heavy trucks, mine equipment, and railway cars. This trend encourages the effort to develop new aluminum alloy systems with improved performance at diesel engine conditions of elevated temperature and stress combinations to reduce vehicle weight and, consequently, CO2 emissions. Aluminum alloys need to provide adequate creep resistance at ~300 °C and room-temperature tensile properties better than the current commercial aluminum alloys used for powertrain applications. The studies for improving creep resistance for aluminum casting alloys indicate that their high-temperature stability depends on the formation of high-density uniform dispersoids with low solid solubility and low diffusivity in aluminum. This review summarizes three generations of diesel engine aluminum alloys and focuses on recent work on the third-generation dispersoid-strengthened alloys. Additionally, new trends in developing creep resistance through the development of alloy systems other than Al-Si-based alloys, the optimization of manufacturing processes, and the use of thermal barrier coatings and composites are discussed. New progress on concepts regarding the thermal stability of rapidly solidified and nano-structured alloys and on creep-resistant alloy design via machine learning-based algorithms is also presented.

Forward and inverse problems for creep models in viscoelasticity.

This study examines a class of time-dependent constitutive equations used to describe viscoelastic materials under creep in solid mechanics. In nonlinear elasticity, the strain response to the applied stress is expressed via an implicit graph allowing multi-valued functions. For coercive and maximal monotone graphs, the existence of a solution to the quasi-static viscoelastic problem is proven by applying the Browder-Minty fixed point theorem. Moreover, for quasi-linear viscoelastic problems, the solution is constructed as a semi-analytic formula. The inverse viscoelastic problem is represented by identification of a design variable from non-smooth measurements. A non-empty set of optimal variables is obtained based on the compactness argument by applying Tikhonov regularization in the space of bounded measures and deformations. Furthermore, an illustrative example is given for the inverse problem of isotropic kernel identification. This article is part of the theme issue 'Non-smooth variational problems with applications in mechanics'.

Alpha-expansins: more than three decades of wall creep and loosening in fruits.

Expansins are proteins without catalytic activity, but able to break hydrogen bonds between cell wall polysaccharides hemicellulose and cellulose. This proteins were reported for the first time in 1992, describing cell wall extension in cucumber hypocotyls caused particularly by alpha-expansins. Although these proteins have GH45 and CBM63 domains, characteristic of enzymes related with the cleavage of cell wall polysaccharides, demonstrating in vitro that they extend plant cell wall. Its participation has been associated to molecular processes such as development and growing, fruit ripening and softening, tolerance and resistance to biotic and abiotic stress and seed germination. Structural insights, facilitated by bioinformatics approaches, are highlighted, shedding light on the intricate interactions between alpha-expansins and cell wall polysaccharides. After more than thirty years of its discovery, we want to celebrate the knowledge of alpha-expansins and emphasize their importance to understand the phenomena of disassembly and loosening of the cell wall, specifically in the fruit ripening phenomena, with this state-of-the-art dedicated to them.

Cumulative creep response of viscoelastic lumbar tissue as a function of work-rest schedule.

We explore the effect of stress-recovery schedule on the cumulative creep response of lumbar tissues. Twelve participants performed a 48-minute protocol that consisted of 12 min of full trunk flexion and 36 min of upright standing. Two stress-recovery (work-rest) schedules were considered: a) three minutes of full trunk flexion followed by twelve minutes of upright standing (3:12), and b) one minute of full trunk flexion followed by four minutes of upright standing (1:4). Lumbar kinematics and EMG activity of erector spinae muscles were collected. Cumulative creep deformation was explored by considering the changes in peak lumbar flexion angles during full flexion and changes in the angles of flexion-relaxation (EMG-off) of the lumbar extensor musculature after the 48-minute protocol. The results of time-dependent lumbar flexion angle during full flexion revealed a noticeable creep response in both work-rest schedules, but the cumulative creep response was significantly greater in the 3:12 schedule (Δ3.5°) than in the 1:4 schedule (Δ1.6°). Similarly, the change in the EMG-off lumbar flexion angle in the 3:12 schedule was significantly greater than in the 1:4 schedule (Δ2.5° vs -Δ0.2°, respectively). These results indicate that the passive lumbar tissues recover their force producing capability more rapidly with shorter cycle times.

Realizing the Creep and Damage Effect on Masonry Panel Design Based on Reliability Analysis.

In this study, a masonry panel under a high compressive stress to strength ratio is considered. The panel is modeled as a composite structure by considering a repeated unit cell of mortar and brick. Load redistributions due to creep in mortar and brick as composite materials are accounted for. A step-by-step in-time analysis is performed to calculate the load redistribution in the composite masonry. Time-dependent system reliability analysis of the masonry panel is performed by defining the component and system limit state functions at each time step. While the reliability index of ductile materials depends on the load level in each part of masonry, the reliability index of brittle materials depends only on the overall load. By proposing the reliability index of quasi-brittle materials being between these two reliability index bounds, the reliability index of quasi-brittle materials depends on both the load level in each part and the overall load. Using the proposed reliability index of quasi-brittle materials, partial safety factors for masonry panel design considering creep and damage are calibrated based on the Hasofer and Lind method. A design example using the proposed partial safety factor is presented.