Combining J-edited and correlation spectroscopies within a multi-dimensional spatial frequency encoding: toward fully resolved 1Hâ
NMR spectra.
Chemistry
; 19(37): 12221-4, 2013 Sep 09.
Article
em En
| MEDLINE
| ID: mdl-24167822
J-resolved at a glance: Passive coupling refocusing-COSY experiments based on a frequency encoding of the sample along two directions of space are presented. It allows various spin evolutions to be triggered in different parts of the sample in a selective and fully controlled manner. This yields 2D spectra in which the whole proton network appears as a series of fully resolved and straightforwardly assignable doublets, triplets or quartets (see figure).
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Base de dados:
MEDLINE
Idioma:
En
Ano de publicação:
2013
Tipo de documento:
Article