Measurement of (15)N enrichment of glutamine and urea cycle amino acids derivatized with 6-aminoquinolyl-N-hydroxysuccinimidyl carbamate using liquid chromatography-tandem quadrupole mass spectrometry.

Nakamura, Hidehiro; Karakawa, Sachise; Watanabe, Akiko; Kawamata, Yasuko; Kuwahara, Tomomi; Shimbo, Kazutaka; Sakai, Ryosei

Nakamura, Hidehiro; Karakawa, Sachise; Watanabe, Akiko; Kawamata, Yasuko; Kuwahara, Tomomi; Shimbo, Kazutaka; Sakai, Ryosei.

Afiliação

Nakamura H; Institute for Innovation, Ajinomoto, Kawasaki-ku, Kawasaki-shi 210-8681, Japan.
Karakawa S; Institute for Innovation, Ajinomoto, Kawasaki-ku, Kawasaki-shi 210-8681, Japan.
Watanabe A; Institute for Innovation, Ajinomoto, Kawasaki-ku, Kawasaki-shi 210-8681, Japan.
Kawamata Y; Institute for Innovation, Ajinomoto, Kawasaki-ku, Kawasaki-shi 210-8681, Japan.
Kuwahara T; Institute for Innovation, Ajinomoto, Kawasaki-ku, Kawasaki-shi 210-8681, Japan.
Shimbo K; Institute for Innovation, Ajinomoto, Kawasaki-ku, Kawasaki-shi 210-8681, Japan.
Sakai R; Institute for Innovation, Ajinomoto, Kawasaki-ku, Kawasaki-shi 210-8681, Japan. Electronic address: ryosei_sakai@ajinomoto.com.

Anal Biochem ; 476: 67-77, 2015 May 01.

Article em En | MEDLINE | ID: mdl-25681567

Assuntos

Aminoácidos/química; Aminoquinolinas/química; Carbamatos/química; Cromatografia Líquida/métodos; Glutamina/química; Espectrometria de Massas em Tandem/métodos; Animais; Masculino; Ratos; Ratos Endogâmicos F344

Palavras-chave

Isotopic enrichment; LCMS/MS; Urea cycle amino acids

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Texto completo: 1 Base de dados: MEDLINE Assunto principal: Carbamatos / Cromatografia Líquida / Espectrometria de Massas em Tandem / Aminoácidos / Glutamina / Aminoquinolinas Idioma: En Ano de publicação: 2015 Tipo de documento: Article

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