Crystal structure of 3,9,9-trimethyl-2,3,3a,4,9,9a-hexa-hydro-1H-cyclo-penta[b]quinolin-4-ium chloride.
Acta Crystallogr E Crystallogr Commun
; 71(Pt 7): o525-6, 2015 Jul 01.
Article
em En
| MEDLINE
| ID: mdl-26279944
ABSTRACT
The title mol-ecular salt, C15H22N(+)·Cl(-), arose as an unexpected product of the reaction between aniline and melanol in the presence of HCl. The central heterocyclic ring has a half-chair conformation and the five-membered ring has an envelope conformation, with the C atom linked to the N atom as the flap. In the crystal, the ions are linked by N-Hâ¯Cl hydrogen bonds, generating chains propagating in the [100] direction. The crystal studied was a merohedral twin with a 0.64â
(3)0.36â
(3) domain ratio.
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MEDLINE
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En
Ano de publicação:
2015
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Article