Thermal, structural, antimicrobial, and physicochemical characterisation of thyme essential oil encapsulated in ß- and γ-cyclodextrin.

The present work aimed to encapsulate the thyme essential oil (TEO) in ß-cyclodextrin (BCD) and γ-cyclodextrin (GCD) complexes in two selected cyclodextrin (CD) to TEO ratios (85/15 and 80/20 w/w) and compare the physicochemical, antioxidant, and antimicrobial properties of the encapsulated powders. The inclusion complexes between CD and TEO were prepared by blending aqueous CD and TEO in ethanol followed by freeze-drying. The powder properties were assessed by measuring particle size and microstructure using SEM, FTIR, and XRD. The median values of the particle sizes (GCD: 92.0 ± 4.69 and BCD: 46.2 ± 2.56-mm) significantly influenced the encapsulation efficiency, resulting in a higher encapsulation efficiency of the GCD (92.02 ± 10.79%) than that of the BCD (56.30 ± 12.19%). The encapsulated GCD/TEO (80/20) showed higher antioxidant activity and an antimicrobial inhibitory effect against Listeria monocytogenes and Salmonella enterica sv. typhimurium. Overall, the GCD acts as a superior wall material to the BCD in the TEO encapsulation.

A comprehensive overview of functional and rheological properties of aloe vera and its application in foods.

Aloe vera catches attention of food industry due to its various health benefits like emollient, anti-inflammatory, purgative, anti-microbial, aphrodisiac, antifungal, and antioxidant. Aloe vera gel has excellent functional and nutritional properties and its incorporation into food can increase its functional and nutritional value of the food. However, both the pulp and aloe gel contain a lot of insoluble polymer particles, which affect the rheological behaviour and physical stability mechanisms of the suspensions during storage and processing. While many researchers have explored the application of aloe vera juice in the food products, no literature review of food applications of aloe vera along with their rheological properties have been complied. Hence, the present review aimed to focus on the utilization of aloe vera in the various sectors of food processing and gives insights on the rheological and flow behaviour of aloe vera juice which is a critical parameter for its food application.

Dry granulation of vitamin D3 and iron in corn starch matrix: Powder flow and structural properties.

In this work, a twin-screw dry granulation (TSDG) was adopted to produce vitamin D3 (VD3) and iron blended dry granules using corn starch as an excipient. Response surface methodology was applied to determine the effect of the formulation compositions (VD3 and iron) on granule properties [tapped bulk density, oil holding capacity, and volumetric mean particle size (Dv50)]. Results indicated that the model fitted well, and responses, in particular flow properties, were significantly affected by the composition. The Dv50 was only influenced by the addition of VD3. The flow properties were characterized by the Carr index and Hausner ratio, which indicated very poor flow of the granules. Scanning electron microscopy with energy dispersive spectroscopy confirm the presence and distribution of Fe++ and VD3 in the granules. Overall, TSDG was proven to be a simple alternative method for the preparation of dry granules of VD3 and iron in a blend.

High-pressure treatment of water-filled co-extruded polylactide films: Effect on microstructure, barrier, thermal, and rheological properties.

The impact of high-pressure treatments (450 and 600 MPa) on the morphological, thermal, structural, and barrier properties of commercial coextruded polylactide (PLA) packaging films has been explored to evaluate their applicability in food processing. Pouches filled with water as a food simulant were subjected to high-pressure treatment for 15 min at ambient temperature. Results indicated no significant changes in the visual appearance, color, integrity, or water barrier properties of the post-process pouches. However, high-pressure treatment affected mechanical property results. Thermal analysis of the film showed endothermic double melting peaks (165.12 and 170.55°C), which did not change with the pressurization; however, the exothermic crystallization peak (118.08°C) varied significantly. Both SEM and AFM micrographs demonstrated that the surface morphology and roughness parameters (arithmetic mean [Sa ] and root mean square height [Sq ]) of the films were significantly affected by the HP treatment, which is further complemented by the FTIR spectra and XRD diffractogram. Melt rheology (175-205°C) of the pressure-treated films showed a significant drop (20-30%) in mechanical rigidity (G') when compared to the untreated sample. Changes in the microstructure/crystallinity in the PLA films were indicated by van Gurp and Palmen plot. PRACTICAL APPLICATION: The results reported here can help to improve the design of the coextruded packaging materials so that it can be successfully implemented to high-pressure processing and high pressure-assisted thermal processing of food.

Effect of high pressure processing on structural and functional properties of canned aquafaba.

Aquafaba is chickpea cooking water. It has great functional properties since it consists of starch and protein. High pressure processing (HPP) is proven to modify the functionality of starch by keeping its integrity. The objective of this study was to check if HPP can improve structural and functional properties of canned aquafaba. HPP treatments were given at pressure levels: 200, 259, 400, 542, and 600 MPa with holding time between 5 and 30 min. After HPP, part of the samples was freeze dried for crystallinity and particle size analysis and the fresh part used for rheological, functional properties, and colour. HPP enhanced functional properties, mostly foaming stability which increased from 50.5 to 67 min. Rheological properties were enhanced mainly for consistency coefficient from 0.6 to 1.4 Pa.s. Crystallinity dropped slightly compared to control sample, while the colour got brighter, from 27.5 to 49.6. Processing time and pressure intensity did not contribute in increasing particle size. The combination of high intensity and long pressurization time resulted the smallest particle size (90 µm).