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1.
Molecules ; 20(1): 1676-85, 2015 Jan 20.
Artigo em Inglês | MEDLINE | ID: mdl-25608855

RESUMO

In order to find and develop new botanical pesticides against tobacco storage pests, bioactivity screening was performed. The essential oil obtained from the aerial parts of Liriope muscari was investigated by GC/MS and GC/FID. A total of 14 components representing 96.12% of the oil were identified and the main compounds in the oil were found to be methyl eugenol (42.15%) and safrole (17.15%), followed by myristicin (14.18%) and 3,5-dimethoxytoluene (10.60%). After screening, the essential oil exhibit potential insecticidal activity. In the progress of assay, it showed that the essential oil exhibited potent contact toxicity against Tribolium castaneum, Lasioderma serricorne and Liposcelis bostrychophila adults, with LD50 values of 13.36, 11.28 µg/adult and 21.37 µg/cm2, respectively. The essential oil also exhibited strong repellency against the three stored product insects. At the same concentrations, the essential oil was more repellent to T. castaneum than to L. serricorne adults. The results indicate that the essential oil of Liriope muscari has potential to be developed into a natural insecticide or repellent for controlling insects in stored tobacco and traditional Chinese medicinal materials.


Assuntos
Besouros/efeitos dos fármacos , Repelentes de Insetos/toxicidade , Liriope (Planta)/química , Nicotiana/parasitologia , Óleos Voláteis/toxicidade , Controle Biológico de Vetores , Animais , Óleos Voláteis/química
2.
Molecules ; 20(12): 21939-45, 2015 Dec 08.
Artigo em Inglês | MEDLINE | ID: mdl-26670226

RESUMO

The essential oil obtained by hydrodistillation from Alpinia kwangsiensis rhizomes was investigated by GC-MS. A total of 31 components representing 92.45% of the oil were identified and the main compounds in the oil were found to be camphor (17.59%), eucalyptol (15.16%), ß-pinene (11.15%) and α-pinene (10.50%). These four compounds were subsequently isolated and the essential oil and four isolated compounds exhibited potent insecticidal activity against Lasioderma serricorne adults. During the assay, it was shown that the essential oil exhibited both potential contact (LD50 = of 24.59 µg/adult) and fumigant (LC50 = of 9.91 mg/L air) toxicity against Lasioderma serricorne. The study revealed that the insecticidal activity of the essential oil can be attributed to the synergistic effects of its diverse major components, which indicates that oil of Alpinia kwangsiensis and its isolated compounds have potential to be developed into natural insecticides to control insects in stored grains and traditional Chinese medicinal materials.


Assuntos
Alpinia/química , Besouros/efeitos dos fármacos , Inseticidas/química , Inseticidas/farmacologia , Óleos Voláteis/química , Óleos Voláteis/farmacologia , Rizoma/química , Animais , Cromatografia Gasosa-Espectrometria de Massas , Inseticidas/isolamento & purificação , Óleos Voláteis/isolamento & purificação
3.
Nat Prod Res ; 34(10): 1360-1365, 2020 May.
Artigo em Inglês | MEDLINE | ID: mdl-30398378

RESUMO

Two new compounds, versicolones A and B (1 and 2), and three known pyrone derivatives (3-5) were isolated from the insect-associated fungus Aspergillus versicolor. Their structures were elucidated through a combination of HRESIMS and NMR spectroscopic analysis. Versicolone A (1) was revealed as a coumarin derivative with the rare 5-alkyl side chain substitution. Compound 5 exhibited significant antioxidant activity with EC50 value of 8.0 µM in the ABTS (2,2-azino-bis-3-ethylbenzothiazoline-6-sulfonic acid) assay, which was more than 2-fold potency of the positive control trolox.


Assuntos
Antioxidantes/isolamento & purificação , Aspergillus/química , Cumarínicos/isolamento & purificação , Pironas/isolamento & purificação , Animais , Antioxidantes/química , Antioxidantes/farmacologia , Cumarínicos/química , Cumarínicos/farmacologia , Fungos/química , Insetos/microbiologia , Espectroscopia de Ressonância Magnética , Estrutura Molecular , Pironas/química , Pironas/farmacologia
4.
J Oleo Sci ; 66(4): 399-405, 2017 Apr 03.
Artigo em Inglês | MEDLINE | ID: mdl-28239059

RESUMO

The contact toxicity and repellent activities of the essential oil extracted from the rhizomes of Zingiber zerumbet (L.) Smith (Zingiberaceae) was evaluated against cigarette beetles (Lasioderma serricorne). The essential oil obtained by hydrodistillation was investigated by GC-FID and GC-MS. The main constituents of the essential oil were zerumbone (40.2%), α-caryophyllene (8.6%), humulene epoxide II (7.3%), camphene (5.9%) and fenchene (4.7%). Zerumbone and its analogues totally are accounting for 60.3% of the essential oil. It was found that the essential oil possessed contact toxicity against L. serricorne adults with a LD50 value of 48.3 µg/adult. α-Caryophyllene (LD50 = 13.1 µg/adult) exhibited stronger contact toxicity against L. serricorne than humulene oxide (LD50 = 31.2 µg/adult), ß-caryophyllene (LD50 = 35.5 µg/adult) and zerumbone (LD50 = 42.4 µg/adult). Moreover, α-caryophyllene possessed strong repellent activity (Class IV and V, respectively) against the beetles at 78.63 nL/cm2, after 2 and 4 h treatment. The results indicate that zerumbone and its analogues might be developed into natural insecticides or repellents for control of cigarette beetles, but their bioactivities are affected by their structures.


Assuntos
Besouros , Repelentes de Insetos , Inseticidas , Óleos de Plantas , Sesquiterpenos , Animais , Monoterpenos/isolamento & purificação , Óleos de Plantas/isolamento & purificação , Sesquiterpenos/isolamento & purificação , Zingiberaceae
5.
Zhongguo Zhong Yao Za Zhi ; 30(5): 340-3, 2005 Mar.
Artigo em Zh | MEDLINE | ID: mdl-15806964

RESUMO

A processing method to enhance thrombolytic effect of Carthamus tinctorius using a fermentation technology with bacillus sp. C2-13 was investigated. The fibrinolysis and anticoagulation activity of thrombolytic extracts from an optimized fermentation process was studied using a carrageenan induced mice model. The fermented extracts resulted in significantly better thrombolytic activity, suggesting that the process was promising for use in the study and preparation of nature medicines.


Assuntos
Bacillus , Carthamus tinctorius/química , Medicamentos de Ervas Chinesas/farmacologia , Fibrinólise/efeitos dos fármacos , Fibrinolíticos/farmacologia , Animais , Carthamus tinctorius/microbiologia , Medicamentos de Ervas Chinesas/isolamento & purificação , Feminino , Fermentação , Masculino , Camundongos , Tempo de Tromboplastina Parcial , Tempo de Protrombina , Ratos , Ratos Sprague-Dawley , Tempo de Trombina
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