1.
Rev Sci Instrum
; 93(7): 073902, 2022 Jul 01.
Artigo
em Inglês
| MEDLINE
| ID: mdl-35922329
RESUMO
A proof of concept is shown for the design of a high pressure heterogeneous catalysis reaction cell suitable for surface sensitive x-ray diffraction and x-ray reflectometry over planar samples using high energy synchrotron radiation in combination with mass spectrometry. This design enables measurements in a pressure range from several tens to hundreds of bars for surface investigations under realistic industrial conditions in heterogeneous catalysis or gaseous corrosion studies.