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In this paper, a ratiometric approach to sensing temperature variations is shown using specialty fiber optic devices. We analyzed the transmission response of cascaded segments of multicore fibers (MCFs), and dissimilar lengths were found to generate an adequate scheme for ratiometric operation. The perturbation of optical parameters in the MCFs translates to a rich spectral behavior in which some peaks increase their intensity while others decrease their intensity. Thus, by selecting opposite-behavior peaks, highly sensitive ratiometric measurements that provide robustness against spurious fluctuations can be performed. We implemented this approach using seven-core fiber (SCF) segments of 5.8 cm and 9.9 cm. To test the system's response under controlled perturbations, we heated one of the segments from ambient temperature up to 150 °C. We observed defined peaks with opposite behavior as a function of temperature. Two pairs of peaks within the interrogation window were selected to perform ratiometric calculations. Ratiometric measurements exhibited sensitivities 6-14 times higher than single-wavelength measurements. A similar trend with enhanced sensitivity in both peak pairs was obtained. In contrast to conventional interferometric schemes, the proposed approach does not require expensive facilities or micrometric-resolution equipment. Moreover, our approach has the potential to be realized using commercial splicers, detectors, and filters.
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A ratiometric fiber optic temperature sensor based on a highly coupled seven-core fiber (SCF) is proposed and experimentally demonstrated. A theoretical analysis of the SCF's sinusoidal spectral response in transmission configuration is presented. The proposed sensor comprises two SCF devices exhibiting anti-phase transmission spectra. Simple fabrication of the devices is shown by just splicing a segment of a 2 cm long SCF between two single-mode fibers (SMFs). The sensor proved to be robust against light source fluctuations, as a standard deviation of 0.2% was registered in the ratiometric measurements when the light source varied by 12%. Its low-cost detection system (two photodetectors) and the range of temperature detection (25 °C to 400 °C) make it a very attractive and promising device for real industrial applications.
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In this Letter, we report a novel, to the best of our knowledge, and simple approach for passive quadrature-phase demodulation of relatively long multiplexed interferometers based on two-channel coherence correlation reflectometry. Two-wavelength channels are generated using a single unmodulated CW-DFB diode laser and an acousto-optic frequency shifter. The introduced frequency shift determines the optical lengths of the interferometers. In our experiments, all interferometers have the same optical length of 32â cm corresponding to the π/2 phase difference between channel signals. An additional fiber delay line was introduced between channels to destroy coherence between initial and frequency-shifted channels. Demultiplexing of channels and sensors was performed using correlation-based signal processing. Amplitudes of cross correlation peaks obtained for both channels were used to extract the interferometric phase for each interferometer. Phase demodulation of relatively long multiplexed interferometers is experimentally demonstrated. Experimental results prove that the proposed technique is suitable for interrogating a serial array of relatively long interferometers dynamically modulated with phase excursions exceeding 2π. Simultaneous interrogation and phase demodulation were experimentally demonstrated using an in-line array of low-finesse Fabry-Perot interferometric sensors.
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In this paper, we propose a highly sensitive temperature sensor based on two cascaded Mach-Zehnder interferometers (MZIs) that work using the Vernier effect. The all-fiber MZIs were assembled by splicing a segment of capillary hollow-core fiber (CHCF) between two sections of multimode fibers (MMFs). This cascaded configuration exhibits a temperature sensitivity of 1.964 nm/°C in a range from 10 to 70 °C, which is ~67.03 times higher than the sensitivity of the single MZI. Moreover, this device exhibits a high-temperature resolution of 0.0153 °C. A numerical analysis was carried out to estimate the devices' temperature sensitivity and calculate the magnification of the sensitivity produced by the Vernier effect. The numerical results have an excellent agreement with the experimental results and provide a better insight into the working principle of the MZI devices. The sensor's performance, small size, and easy fabrication make us believe that it is an attractive candidate for temperature measurement in biological applications.
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Interferometria , Refratometria , Temperatura Alta , TemperaturaRESUMO
In this paper, we propose and experimentally demonstrate a simple technique to enhance the curvature sensitivity of a bending fiber optic sensor based on anti-resonant reflecting optical waveguide (ARROW) guidance. The sensing structure is assembled by splicing a segment of capillary hollow-core fiber (CHCF) between two single-mode fibers (SMF), and the device is set on a steel sheet for measuring different curvatures. Without any surface treatment, the ARROW sensor exhibits a curvature sensitivity of 1.6 dB/m-1 in a curvature range from 0 to 2.14 m-1. By carefully coating half of the CHCF length with polydimethylsiloxane (PDMS), the curvature sensitivity of the ARROW sensor is enhanced to -5.62 dB/m-1, as well as an increment in the curvature range (from 0 to 2.68 m-1). Moreover, the covered device exhibits a low-temperature sensitivity (0.038 dB/°C), meaning that temperature fluctuations do not compromise the bending fiber optic sensor operation. The ARROW sensor fabricated with this technique has high sensitivity and a wide range for curvature measurements, with the advantage that the technique is cost-effective and easy to implement. All these features make this technique appealing for real sensing applications, such as structural health monitoring.
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An all-fiber approach is presented to measure surface tension. The experimental realization relies on the use of a specialty fiber, a so-called two-hole fiber (THF), which serves a two-fold purpose: providing a capillary channel to produce bubbles while having the means to measure the power reflected at the end facet of the fiber core. We demonstrate that provided a controlled injection of gas into the hollow channels of the THF, surface tension measurements are possible by simply tracking the Fresnel reflection at the distal end of the THF. Our results show that the characteristic times involved in the bubble formation process, from where the surface tension of the liquids under test is retrieved, can be measured from the train of pulses generated by the continuous formation and detachment of bubbles.
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This study presents the optical improvement of a high flux solar simulator (HFSS) with controllable flux-spot capabilities developed for researching solar thermal and thermochemical processes. The HFSS is comprised of seven 2.5 kWel Xenon arc lamps coupled with ellipsoidal reflectors, a servo-controlled attenuator curtain, and three-axes linear test bench. Different attenuators were designed and tested in order to identify the best curtain geometry to improve the HFSS modulation with the lowest possible radiative losses. The optical design improvement was performed with the aid of TracePro, a Monte Carlo ray-tracing software. From simulation results, radiative peak flux from 1700 to 480 kWm-2 from the focal plane to 300 mm further back was estimated without curtains. By using the attenuators, flux levels from 1570 to 92 kWm-2 at the focal plane were also estimated. An experimental validation was achieved with a single lamp-reflector unit obtaining peak flux distributions from 200±20 kWm-2 to 97±9.7 kWm-2 from the focal plane to 300 mm behind. Flux modulation from 170 to 1.5 kWm-2 was also measured at the focal plane using a servo-controlled curtain from fully-open slats (0°) to partially closed (60°). With this attenuator, introduced as the shutter of the system, the use of several lamps or electronic rectifiers is avoided and the radiative flux is modulated with high resolution in an optomechatronical form.
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The integration of carbon nanotubes (CNTs) into optical fibers allows the application of their unique properties in robust and versatile devices. Here, we present a laser-induced technique to obtain the deposition of CNTs onto the fiber optics tips of multimode interference (MMI) devices. An MMI device is constructed by splicing a section of no-core fiber (NCF) to a single-mode fiber (SMF). The tip of the MMI device is immersed into a liquid solution of CNTs and laser light is launched into the MMI device. CNTs solutions using water and methanol as solvents were tested. In addition, the use of a polymer dispersant polyvinylpyrrolidone (PVP) in the CNTs solutions was also studied. We found that the laser-induced deposition of CNTs performed in water-based solutions generates non-uniform deposits. On the other hand, the laser-induced deposition performed with methanol solutions generates uniform deposits over the fiber tip when no PVP is used and deposition at the center of the fiber when PVP is present in the CNTs solution. The results show the crucial role of the solvent on the spatial features of the laser-induced deposition process. Finally, we register and study the reflection spectra of the as-fabricated CNTs deposited MMI devices.
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In this paper we demonstrate the passive, material-based athermalization of all-fiber architectures by cascading multimode interference (MMI) devices. In-line thermal compensation is achieved by including a liquid-core multimode section of variable length that allows ensuring temperature-independent operation while preserving the inherent filter-like spectral response of the MMI devices. The design of the temperature compensation unit is straightforward and its fabrication is simple. The applicability of our approach is experimentally verified by fabricating a wavelength-locked MMI laser with sensitivity of only -0.1 pm/°C, which is at least one order of magnitude lower than that achieved with other fiber optics devices.
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A novel fiber optic temperature sensor based on a liquid-core multimode interference device is demonstrated. The advantage of such structure is that the thermo-optic coefficient (TOC) of the liquid is at least one order of magnitude larger than that of silica and this, combined with the fact that the TOC of silica and the liquid have opposite signs, provides a liquid-core multimode fiber (MMF) highly sensitive to temperature. Since the refractive index of the liquid can be easily modified, this allows us to control the modal properties of the liquid-core MMF at will and the sensor sensitivity can be easily tuned by selecting the refractive index of the liquid in the core of the device. The maximum sensitivity measured in our experiments is 20 nm/°C in the low-temperature regime up to 60 °C. To the best of our knowledge, to date, this is the largest sensitivity reported for fiber-based MMI temperature sensors.
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Tecnologia de Fibra Óptica/métodos , Desenho de Equipamento/métodos , TemperaturaRESUMO
A universal pH indicator is used to fabricate a fiber optic ammonia sensor. The advantage of this pH indicator is that it exhibits sensitivity to ammonia over a broad wavelength range. This provides a differential response, with a valley around 500 nm and a peak around 650 nm, which allows us to perform ratiometric measurements. The ratiometric measurements provide not only an enhanced signal, but can also eliminate any external disturbance due to humidity or temperature fluctuations. In addition, the indicator is embedded in a hydrophobic and gas permeable polyurethane film named Tecoflex®. The film provides additional advantages to the sensor, such as operation in dry environments, efficient transport of the element to be measured to the sensitive area of the sensor, and prevent leakage or detachment of the indicator. The combination of the universal pH indicator and Tecoflex® film provides a reliable and robust fiber optic ammonia sensor.
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Amônia/análise , Tecnologia de Fibra Óptica/instrumentação , Concentração de Íons de Hidrogênio , Fibras Ópticas , Processamento de Sinais Assistido por Computador , Análise EspectralRESUMO
In this work we demonstrate efficient quality control of a variety of gasoline and ethanol (gasohol) blends using a multimode interference (MMI) fiber sensor. The operational principle relies on the fact that the addition of ethanol to the gasohol blend reduces the refractive index (RI) of the gasoline. Since MMI sensors are capable of detecting small RI changes, the ethanol content of the gasohol blend is easily determined by tracking the MMI peak wavelength response. Gasohol blends with ethanol contents ranging from 0% to 50% has been clearly identified using this device, which provides a linear response with a maximum sensitivity of 0.270 nm/% EtOH. The sensor can also distinguish when water incorporated in the blend has exceeded the maximum volume tolerated by the gasohol blend, which is responsible for phase separation of the ethanol and gasoline and could cause serious engine failures. Since the MMI sensor is straightforward to fabricate and does not require any special coating it is a cost effective solution for real time and in-situ monitoring of the quality of gasohol blends.
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We report on an all-fiber setup capable of generating complex intensity patterns using interference of few guided modes. Comprised by a few-mode fiber (FMF) spliced to a multimodal interference (MMI) fiber device, the setup allows for obtaining different output patterns upon adjusting the phases and intensities of the modes propagating in the FMF. We analyze the output patterns obtained when exciting two family modes in the MMI device using different phase and intensity conditions for the FMF modal base. Using this simple experimental arrangement we are able to produce complex intensity patterns with radial and azimuthal symmetry. Moreover, our results suggest that this approach provides a means to generate beams with orbital angular momentum (OAM).
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A simple and compact fiber optic sensor based on a two-core fiber is demonstrated for high-performance measurements of refractive indices (RI) of liquids. In order to demonstrate the suitability of the proposed sensor to perform high-sensitivity sensing in a variety of applications, the sensor has been used to measure the RI of binary liquid mixtures. Such measurements can accurately determine the salinity of salt water solutions, and detect the water content of adulterated alcoholic beverages. The largest sensitivity of the RI sensor that has been experimentally demonstrated is 3,119 nm per Refractive Index Units (RIU) for the RI range from 1.3160 to 1.3943. On the other hand, our results suggest that the sensitivity can be enhanced up to 3485.67 nm/RIU approximately for the same RI range.
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Tecnologia de Fibra Óptica/instrumentação , Refratometria/instrumentação , Reologia/instrumentação , Soluções/química , Transdutores , Desenho de Equipamento , Análise de Falha de Equipamento , Reprodutibilidade dos Testes , Sensibilidade e EspecificidadeRESUMO
We report the fabrication of a saturable absorber based on SU8 single wall carbon nanotube (SWCNT) composite material. Thin films with a controllable thickness can be fabricated using a simple and reliable process. These films can be inserted between two FC/APC connectors in order to have an inline saturable absorber. A passive mode-locked laser was built by interleaving the fiberized saturable absorber in an erbium-doped fiber (L-band) ring cavity laser. The laser produces 871 fs pulses with a repetition rate of 21.27 MHz and a maximum average power of 1 mW.
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Tecnologia de Fibra Óptica/instrumentação , Lasers , Nanotecnologia/instrumentação , Nanotubos de Carbono/química , Desenho de Equipamento , Análise de Falha de EquipamentoRESUMO
We demonstrate optical fiber sensors based on highly coupled multicore fibers operating with the optical Vernier effect. The sensors are constructed using a simple device incorporating single-mode fibers (SMFs) and a segment of a multicore fiber. In particular, we evaluated the performance of a sensor based on a seven-core fiber (SCF) spliced at both ends to conventional SMFs, yielding a versatile arrangement for realizing Vernier-based fiber sensors. The SMF-SCF-SMF device can be fabricated using standard splicing procedures and serve as a "building block" for both, reflection and transmission sensing configurations. As demonstrated with our experimental results, the Vernier arrangements can yield a ten-fold increase in sensitivity for temperature measurements compared to a conventional single SMF-SCF-SMF device, thereby confirming the enhanced sensitivity that can be attained with this optical effect. Furthermore, through theoretical analysis, we obtain the relevant parameters that must be optimized in order to achieve an optimal sensitivity for a specific application. Our findings thus provide the necessary guidelines for constructing Vernier-based sensors with all-fiber devices based on highly coupled multicore optical fibers, which constitutes an ideal framework to develop highly sensitive fiber sensors for different applications.
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The applications of serology tests to the virus SARS-CoV-2 are diverse, ranging from diagnosing COVID-19, understanding the humoral response to this disease, and estimating its prevalence in a population, to modeling the course of the pandemic. COVID-19 serology assays will significantly benefit from sensitive and reliable technologies that can process dozens of samples in parallel, thus reducing costs and time; however, they will also benefit from biosensors that can assess antibody reactivities to multiple SARS-CoV-2 antigens. Here, we report a high-throughput microfluidic device that can assess antibody reactivities against four SARS-CoV-2 antigens from up to 50 serum samples in parallel. This semi-automatic platform measures IgG and IgM levels against four SARS-CoV-2 proteins: the spike protein (S), the S1 subunit (S1), the receptor-binding domain (RBD), and the nucleocapsid (N). After assay optimization, we evaluated sera from infected individuals with COVID-19 and a cohort of archival samples from 2018. The assay achieved a sensitivity of 95% and a specificity of 91%. Nonetheless, both parameters increased to 100% when evaluating sera from individuals in the third week after symptom onset. To further assess our platform's utility, we monitored the antibody titers from 5 COVID-19 patients over a time course of several weeks. Our platform can aid in global efforts to control and understand COVID-19.
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Anticorpos Antivirais/sangue , COVID-19/diagnóstico , Imunoensaio/métodos , SARS-CoV-2/imunologia , Área Sob a Curva , COVID-19/virologia , Proteínas do Nucleocapsídeo de Coronavírus/imunologia , Humanos , Imunoensaio/instrumentação , Imunoglobulina G/sangue , Imunoglobulina G/imunologia , Imunoglobulina M/sangue , Imunoglobulina M/imunologia , Dispositivos Lab-On-A-Chip , Estudos Longitudinais , Fosfoproteínas/imunologia , Domínios Proteicos/imunologia , Curva ROC , SARS-CoV-2/isolamento & purificação , Sensibilidade e Especificidade , Glicoproteína da Espícula de Coronavírus/química , Glicoproteína da Espícula de Coronavírus/imunologiaRESUMO
We report the first observation of discrete Talbot revivals in one-dimensional waveguide arrays. Unlike continuous systems where the Talbot self-imaging effect always occurs irrespective of the pattern period, in discrete configurations this process is only possible for a specific set of periodicities. Recurrence of different input periodic patterns is observed in good agreement with theory.