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OBJECTIVE: The aim of this study was to assess the effect of opaque stain application to the intaglio surface of lithium disilicate glass ceramics on the masking ability of discolored substrates and bond strength to a resin-based luting agent (depending on etching time); the stain film-thickness was also assessed. MATERIALS AND METHODS: Ceramic specimens were produced with CAD-CAM blocks of lithium disilicate (IPS e.max CAD). Two opaque stains were tested at ceramic intaglio surface: opaque glassy stain for titanium frameworks (OP-ti) and low-fusion glassy stain for ceramic characterization (LFG-iv). Non-stained ceramic specimens served as controls. For optical and colorimetric analyses, A2-shaded ceramics of medium and low-translucencies were tested, in thicknesses of 1.0- and 1.5-mm (n = 10), with two coupling agents (non-shaded-glycerin and A2-shaded try-in paste). CIEDE2000 formula was used for calculation of translucency parameter (TP00) and color differences (ΔE00). Whiteness index for dentistry (WID) was also reported. ΔE00 were assessed over discolored substrates (tooth-shaded A2-reference, A4, C3, and C4; coppery metal, silvery metal, white zirconia, and PEEK). Microshear bond strength of stained and non-stained ceramic specimens to a resin-based luting agent was evaluated. Film-thickness of stains was assessed by scanning electron microscopy. RESULTS: The application of opaque stains to the intaglio surface of lithium disilicate ceramics resulted in significant reduction of TP00 (p < 0.001) and WID (p < 0.001) and differences in L*, C*, and ho color coordinates (especially with OP-ti) (p < 0.001). ΔE00 was significantly reduced in stained ceramic groups in comparison with the control, for all discolored substrates (p < 0.001). Acceptable color matching was obtained with stained ceramic specimens for all discolored substrates, depending on the type of stain, ceramic thickness, ceramic translucency, and coupling agent. The application of stains to the ceramic intaglio surface was not detrimental to bond strength to a resin-based luting agent, but depended on the time of hydrofluoric acid-etching (20 s for OP-ti and 60 s for LFG-iv) (p < 0.001). Film-thickness of stains presented mean values <70 µm. CONCLUSION: The application of opaque stains to the intaglio surface of lithium disilicate glass ceramics was effective to mask severely discolored substrates, presenting adequate bond strength to the luting agent and thin film-thicknesses. CLINICAL SIGNIFICANCE: For indirect restorations over severely discolored substrates, the application of opaque stain to the intaglio surface of lithium disilicate glass ceramic ensures acceptable color matching, with adequate bond strength to resin-based luting agents and clinically acceptable stain film-thickness.
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OBJECTIVE: To investigate the effect of ceramic thickness and dental substrate (enamel vs. dentin/enamel) on the survival rate and failure load of non-retentive occlusal veneers. MATERIALS AND METHODS: Human maxillary molars (n = 60) were divided into five test-groups (n = 12). The groups (named DE-1.5, DE-1.0, DE-0.5, E-1.0, E-0.5) differed in their dental substrate (E = enamel, DE = dentin/enamel) and restoration thickness (standard: 1.5 mm, thin: 1.0 mm, ultrathin: 0.5 mm). All teeth were prepared for non-retentive monolithic lithium-disilicate occlusal veneers (IPS e.max Press, Ivoclar). Restorations were adhesively cemented (Syntac Classic/Variolink II, Ivoclar) and exposed to thermomechanical fatigue (1.2 million cycles, 1.6 Hz, 49 N/ 5-55°C). Single load to failure was performed using a universal testing-machine. A linear-regression model was applied, pairwise comparisons used the Student-Newman-Keuls method (p < 0.05). RESULTS: Three dentin-based occlusal veneers (one DE-1.0, two DE-0.5) revealed cracks after fatigue exposure, which corresponds to an overall-survival rate of 95%. Load to failure resulted in the following ranking: 2142 N(DE-0.5) > 2105 N(E-1.0) > 2075 N(E-0.5) > 1440 N(DE-1.5) > 1430 N(DE-1.0). Thin (E-1.0) and ultrathin enamel-based occlusal veneers (E-0.5) revealed high failure loads and surpassed the standard thickness dentin-based veneers (DE-1.5) significantly (p = 0.044, p = 0.022). CONCLUSION: All tested monolithic lithium disilicate occlusal veneers obtained failure loads above physiological chewing forces. Thin and ultrathin enamel-based occlusal veneers outperformed the standard thick dentin-based occlusal veneers. CLINICAL SIGNIFICANCE: Minimally invasive enamel-based occlusal veneer restorations with non-retentive preparation design may serve as a conservative treatment option.
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Cerâmica , Porcelana Dentária , Humanos , Taxa de Sobrevida , Dente Molar , Teste de Materiais , Análise do Estresse Dentário , Facetas Dentárias , Falha de Restauração DentáriaRESUMO
OBJECTIVES: To evaluate minimally invasive restorations' capacity to mask discolored teeth and explore the impact of ceramic thickness, translucency, and cement color. MATERIALS AND METHODS: Twenty-four assessment pairs of naturally colored and discolored bovine dentin samples were formed, using lithium disilicate specimens in six different thicknesses (0.3-0.8 mm), two different translucencies (high, low), and two cements (transparent, tooth-colored). Evaluators assessed the color differences in each assessment pair, and the threshold for detecting a color difference was determined using sequential testing and the Bonferroni-Holm method. RESULTS: A thickness of 0.6 mm effectively masked color differences using high translucent ceramic with transparent cement, detectable differences were still observed at 0.7/0.8 mm. A threshold thickness of 0.4 mm was seen using high translucent ceramic and tooth-colored cement, with color differences still discernible at 0.5 and 0.8 mm. A threshold thickness of 0.4 mm was detected using low translucent ceramic and transparent cement, while detectable differences persisted at 0.5, 0.7, and 0.8 mm. A 0.5 mm threshold thickness was observed when using low translucent ceramic and tooth-colored cement, and no detectable color differences were detected beyond this thickness. CONCLUSIONS: Masking can be achieved with a thickness of 0.4-0.5 mm using a low translucent material and tooth-colored cement. CLINICAL SIGNIFICANCE: Understanding the impact of ceramic thickness, translucency, and cement color can aid clinicians in making informed decisions for achieving the best esthetic outcomes while preserving tooth structure. Effective masking can be accomplished with ceramic thicknesses starting at 0.4 mm, especially when employing a low translucent material and tooth-colored cement. However, clinicians should be aware that discolorations may still be detectable in certain scenarios when using minimally invasive lithium disilicate restorations.
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Cerâmica , Porcelana Dentária , Animais , Bovinos , Porcelana Dentária/química , Cimentos Dentários , Cimentos de Ionômeros de Vidro , Teste de Materiais , Cor , Propriedades de SuperfícieRESUMO
Since the removal of resin-luted all-ceramic restorations is a challenge, the use of Er:YAG lasers has become popular. The aim of this study was to determine the removal time of monolithic lithium disilicate crowns in different thicknesses and heat transmission to pulp using Er:YAG laser. Forty-five full-coverage monolithic lithium disilicate crowns in 1 mm (n = 15), 1.5 mm (n = 15), and mixed thickness (n = 15) were resin luted on relevant extracted human maxillary first premolars and subjected to Er:YAG laser irradiation for crown removal after 24 h. Laser parameters for each thickness, respectively, were 5 W, 5.6 W, and 5.9 W (10 Hz). The removal time and temperature change values were recorded for each sample. The statistical evaluations were performed using one-way ANOVA variance and post hoc Duncan and Tamhane's T2 tests (p < 0.05), and Pearson correlation coefficient was used to examine the significance within each group and without group discrimination. All crowns were laser-debonded successfully. The removal time (min:s) at the succeeding laser parameter for each group is as follows: between 2:30 and 4:45 at 5 W power for 1-mm samples, between 5:00 and 11:15 at 5.9 W power for 1.5-mm samples, and between 8:45 and 15:00 at 5.9 W power for samples in mixed thickness. Moreover, it was observed that the temperature changes in the pulp chamber did not exceed the critical value of 5.5 °C for any sample. Er:YAG laser irradiation is an effective and safe method for removal of all-ceramic crowns when appropriate laser parameters are used according to thickness.
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Lasers de Estado Sólido , Humanos , Lasers de Estado Sólido/uso terapêutico , Temperatura , Porcelana Dentária , CerâmicaRESUMO
OBJECTIVE: the aim of this study was to evaluate the effect of resin composite layering on discolored substrates to obtain masking ability with monolithic ceramics. MATERIALS AND METHODS: Four groups (n = 8) of computer-aided design/computer aided manufacturing (CAD/CAM) monolithic ceramics, shade A1, with thicknesses of 1.0 and 1.5 mm, were tested: feldspathic (FC), leucite-reinforced (LC), lithium disilicate-reinforced (LD), and translucent zirconia (5YSZ). Five substrates were used: A1 (used as reference), A3.5, C4, and coppery and silvery metals. The substrates were separated as non-layered or layered (with flowable opaque resin composite (FL), white opaque restorative resin composite (WD), and A1-shaded opaque restorative resin composite (A1D)). Resin composite layers of 0.5 and 1.0 mm were tested. The try-in paste, shade A1, was used as a luting agent. Translucency parameter (TP00 ) was assessed for the ceramics. Color differences (∆E00 ) were assessed for the restorative ceramics and resin composite layers over discolored substrates with the CIEDE2000 formula. The results were compared statistically, and descriptively with acceptability (AT, 1.77) and perceptibility (PT, 0.81) thresholds. RESULTS: Feldspathic showed the highest TP00 (for both ceramic thicknesses) and LD the lowest (for 1.5 mm of ceramic thickness) (P < 0.001). For substrate A3.5, layering with 1.0 mm of A1D or WD ensured ∆E00 below PT for all ceramics tested (P < 0.001). The use of 0.5 mm of FL or 1.0 mm of A1D associated with ceramics LC, LD, and 5YSZ ensured ∆E00 below AT for substrates C4 and coppery metal (P < 0.001). Silvery background layered with 0.5 mm of FL presented ∆E00 below AT for all ceramics and ∆E00 below PT for lithium disilicate of 1.0 mm of thickness (∆E00 = 0.72). CONCLUSIONS: Layering severely discolored substrates with selected opaque resin composites ensures masking ability for restoration with CAD/CAM monolithic ceramics. CLINICAL SIGNIFICANCE: Severely discolored substrates are predictably restored with monolithic CAD/CAM ceramics by performing a previous layering of the substrate with opaque resin composite.
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Cerâmica , Porcelana Dentária , Cor , Cimentos Dentários , Desenho Assistido por Computador , Teste de Materiais , Propriedades de SuperfícieRESUMO
The adhesive cementation of ceramic inlays may increase pulpal temperature (PT) and induce pulpal damage due to heat generated by the curing unit and the exothermic reaction of the luting agent (LA). The aim was to measure the PT rise during ceramic inlay cementation by testing different combinations of dentin and ceramic thicknesses and LAs. The PT changes were detected using a thermocouple sensor positioned in the pulp chamber of a mandibular molar. Gradual occlusal reduction obtained dentin thicknesses of 2.5, 2.0, 1.5, and 1.0 mm. Light-cured (LC) and dual-cured (DC) adhesive cements and preheated restorative resin-based composite (RBC) were applied to luting of 2.0, 2.5, 3.0, and 3.5 mm lithium disilicate ceramic blocks. Differential scanning calorimetry was used to compare the thermal conductivity of dentin and ceramic slices. Although ceramic reduced heat delivered by the curing unit, the exothermic reaction of the LAs significantly increased it in each investigated combination (5.4-7.9 °C). Temperature changes were predominantly influenced by dentin thickness followed by LA and ceramic thickness. Thermal conductivity of dentin was 24% lower than that of ceramic, and its thermal capacity was 86% higher. Regardless of the ceramic thickness, adhesive inlay cementation can significantly increase the PT, especially when the remaining dentin thickness is <2 mm.
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Resinas Compostas , Colagem Dentária , Resinas Compostas/química , Dentina , Restaurações Intracoronárias , Temperatura , Cimentos de Resina/química , Cerâmica/química , Teste de MateriaisRESUMO
OBJECTIVE: To evaluate the effect of ceramic thicknesses, bonding surface (enamel vs. dentin), and preparation design (box vs. no box) on the fatigue survival and failure load of minimally invasive full-veneer restorations. MATERIALS AND METHODS: Human-premolars (n = 60) were divided into five test groups (n = 12). All teeth received full-veneer preparation with the following occlusal/labial thicknesses: standard: 1.5/0.8 mm; thin: 1.0/0.6 mm; ultrathin 0.5/0.4 mm. Preparations for each ceramic thickness were refined in enamel (E-1.0 and E-0.5) or dentin (D-1.5, D-1.0, and D-0.5). Control groups DB-1.5, EB-1.0, and EB-0.5 received box preparations. Monolithic lithium disilicate restorations (IPS-e.max-Press, Ivoclar Vivadent) were adhesively cemented (Syntac-Classic/Variolink-II, Ivoclar Vivadent) and subjected to cyclic mechanical loading (F = 49 N, 1.2 million cycles) with simultaneous thermocycling (5-55°C). All specimens were exposed to single load-to-failure. Pair-wise differences were calculated by using a linear regression model and Student-Newman-Keuls method (p < 0.05). RESULTS: All full-veneers of group D-1.5, E-1.0, E-0.5, DB-1.5, EB-1.0, and EB-0.5 survived fatigue. Two full-veneers (D-1.0 and D-0.5) revealed cracks during fatigue, resulting in an overall fatigue survival rate of 98.1%. Mean load-to-failure values (N) were as followed: 1005 (D-1.5); 866 (D-1.0); 816 (D-0.5); 1495 (E-1.0); 1279 (E-0.5); 1129 (DB-1.5); 1087 (EB-1.0); and 833 (EB-0.5). Irrespective of ceramic thicknesses, enamel-based full-veneers resulted in higher failure loads than dentin-based restorations. Box preparation reduced the failure loads of thin and ultrathin enamel-based restorations. CONCLUSION: All tested monolithic lithium disilicate full-veneer restorations exceeded physiological masticatory forces. Minimally invasive full-veneer restorations with enamel as a bonding surface and a non-retentive preparation design showed superior performance. CLINICAL SIGNIFICANCE: Enamel-based non-retentive full-veneers made of monolithic lithium disilicate may serve as a reliable and esthetical minimally invasive treatment option for premolars.
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Porcelana Dentária , Facetas Dentárias , Cerâmica , Esmalte Dentário , Falha de Restauração Dentária , Análise do Estresse Dentário , Humanos , Teste de MateriaisRESUMO
OBJECTIVES: The purpose of this study was to evaluate the effect of the tooth color, ceramic color, and ceramic thickness on the final color parameters of a feldspathic computer-aided design (CAD)/computer-aided manufacturing (CAM) ceramic material. MATERIALS AND METHODS: Resin specimens (12 × 14 × 4 mm) were prepared from six shades, namely, 0M1S, 1M1S, 2M3S, 3M2S, 4M3S, and 5M3S, to simulate tooth color. Ceramic slices with thicknesses of 0.3, 0.5, 0.7, and 1 mm were sectioned from Vitablocs Mark II (12 × 14 × 18 mm) in 10 shades-OM1C, 1M1C, 1M2C, 2M1C, 2M2C, 2M3C, 3M1C, 3M2C, 3M3C, and 4M2C. An intraoral spectrophotometer was used and three axes of Commission Internationale de l'Eclairage (CIE) LAB color space (CIE L* a* b*) and chroma (C) and hue (H) values were obtained. RESULTS: The a* and b* values showed a decrease with increasing thickness. Generally, C decreased with the increasing ceramic thickness. The effect of ceramic thickness on H changed depending on the block and substructure color. The change of ceramic thickness resulted in changes in the lightness parameter (L*) of the ceramics. Generally, with an increase in the thickness, the L* value increased. The univariate analysis of variance (ANOVA) indicated a significant interaction between ceramic thickness and substructure color (P <. 005) and ceramic thickness and ceramic color (P <. 005). CONCLUSION: The final color parameters of a feldspathic CAD/CAM block were significantly affected by the changes in the ceramic thickness and substructure color.
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Cerâmica/química , Desenho Assistido por Computador , Materiais Dentários/química , CorRESUMO
OBJECTIVE: The aim of this study was to evaluate the micro-mechanical properties of a light-cured resin cement in four different shades when polymerized through a leucite-reinforced glass-ceramic in different shades and thicknesses. MATERIALS AND METHODS: A light-cured resin cement in four different shades (HV+1, HV+3, LV-1 and LV-3) was selected for this study. The specimens were cured by using a LED-unit (Bluephase®, IvoclarVivadent) for 20 s under a leucite-reinforced glass-ceramic (IPS Empress® CAD, IvoclarVivadent) in two different shades (A1 and A3) of different thicknesses (1 and 2 mm). Specimens cured directly, without an intermediate ceramic, served as control. The specimens were stored after curing for 24 h at 37°C by maintaining moisture conditions with distilled water. Micro-mechanical properties (indentation modulus, E; Hardness, HV; creep, Cr) of the resin cements were measured with an automatic microhardness indenter (Fisherscope H100C, Germany). Twenty groups were included (n = 3), while 10 measurements were performed on each specimen. Data were statistically analyzed by using one-way ANOVA and Tukey's post-hoc test, as well as a multivariate analysis to test the influence of the study parameters. RESULTS: Significant differences were observed between the micromechanical properties of the tested resin cements (p < 0.05). The resin cement shade showed the highest effect on the micromechanical properties (Partial-eta squared (ηP(2))-E = 0.45, ηP(2)-HV = 0.59, ηP(2)-Cr = 0.29) of the resin cement, followed by ceramic thickness (ηP(2)-E = 0.38, ηP(2)-HV = 0.3, ηP(2)-Cr = 0.04) and ceramic shade (ηP(2)-E = 0.2, ηP(2)-HV = 0.26). CONCLUSIONS: Resin cement shade is an important factor influencing the mechanical properties of the material. Light shades of a resin cement express higher E and HV as well as lower Cr values compared with the darker ones.
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Porcelana Dentária/química , Cura Luminosa de Adesivos Dentários , Cimentos de Resina/química , Silicatos de Alumínio/química , Cerâmica/química , Cor , Lâmpadas de Polimerização Dentária/classificação , Módulo de Elasticidade , Dureza , Humanos , Cura Luminosa de Adesivos Dentários/instrumentação , Teste de Materiais , Polimerização , Estresse Mecânico , Propriedades de Superfície , Temperatura , Fatores de Tempo , Água/químicaRESUMO
Preparation of porcelain restorations that match the natural dentition has been a subject of great concern for many years. An understanding of the process by which the colour and translucency of fixed restorations are planned and obtained so as to replicate the colour of its adjacent teeth is important for achieving an esthetic restoration. This study was done to study the effect of fabrication procedures such as ceramic thickness and number of firing cycles on the colour of metal ceramic restorations. Metal ceramic samples with three different ceramic thicknesses; 0.5, 1 and 1.5 mm (N = 30, n = 10 per group) were fabricated. A3 shade of [VMK 95, VITA Zahnfabrik, Bad Sackingen, Germany] ceramic was used for the fabrication of samples. Samples were subject to multiple firing cycles and colour was measured after 2nd, 3rd, 4th, 6th, 8th and 10th firing cycle. Colour measurement was done objectively using spectrolino (Gretag Macbeth Inc., Germany) spectrophotometer. 'Repeated measures ANOVA' test was used for doing statistical analysis. No significant change was noticed in any of the four colour parameters between the baseline reading after second firing uptil the tenth firing for any of the three groups with different ceramic thicknesses. There was a consistent rise in L* or lightness of colour as the thickness of ceramic increased. Between group I and group III there was a consistent shift of a* axis towards the blue green side and there was a consistent shift in b* axis towards purple-blue with an increase in ceramic thickness. It was observed that there was a change in ΔE with a change in ceramic thickness. There was a change of about two units between group I and group II and a change of about one unit between group II and group III. Change in ΔE between group I and group III was the most significant, being about three units. It was concluded from the study that multiple firing cycles during fabrication of metal ceramic restorations do not have any effect on colour while colour varies with change in ceramic thickness.
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Ceramic thickness and technicians' manipulative variables are critical factors affecting the resultant shade of dental ceramo-metallic restorations. This study investigated the effect of the following variables on shade duplication of ceramo-metallic specimens: (a) ceramic thickness; (b) differences between several technicians (inter-technician variability); and (c) the ability of each technician to repeat the resultant shade (intra-technician variability). Ninety ceramo-metallic specimens were prepared and divided into three main groups (n = 30/gp) according to the different technicians who built up the veneering ceramic of the specimens. Each group was further subdivided into three subgroups (n = 10/subgroup) according to the thickness of the ceramic (1, 1.5, and 2 mm built over a 0.5 mm-thick metal substructure). Three different technicians were asked to follow the same protocol as regards the same ceramic batch (Shade 3M2, Vita VM13, Zahnfabrik, Germany), firing temperature, and number of firing cycles. Meanwhile, each technician followed his own protocol with regard to other ceramic manipulative variables. The duplicated shades of the specimens were investigated using the Vita Easyshade spectrophotometer by using the verify shade mode. Color difference (∆E) values were calculated between the target shade (3M2) and the duplicated shades of the specimens automatically by the Vita Easyshade spectrophotometer (Vita, Zahnfabrik, Germany). The effect of ceramic thickness and inter- and intra-technician variability on the duplication of the target shade was investigated. The results showed that the effect of ceramic thickness on the duplicated shades depended on inter-technician variability. High inter-technician variability (∆E = 2-6.4) was noticed in contrast to low intra-technician variability (∆E = 0.2-1.5). It could be concluded that proper shade-duplication of ceramo-metallic restoration was a cumulative technique intimately related to manipulative variables and ceramic thickness.
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OBJECTIVE: To compare the translucency and masking of zirconia-reinforced lithium silicate with lithium disilicate glass-ceramic and hybrid composite. MATERIALS AND METHODS: One hundred and twenty disc-shaped specimens were fabricated using Enamic, Celtra Duo, IPS E.max CAD, and Suprinity. Twelve groups were prepared according to material type and thickness (0.5, 1.0, and 1.5 mm). The specimens were tested over five substrates: composite resin-A3.5 shade (A3.5 control group), zirconia-A1 shade (ZR), nickel-chromium alloy (NC), black (B), and white (W). A spectrophotometer operating at wavelengths from 360 to 750 nm and a view-area size of 9.53 mm was used for color measurement. RESULTS: Mean color difference values (ΔΕ) were found to be lowest in Suprinity and highest in IPS E.max. CAD. Color difference values were significantly related to substrate shade. The A3.5 substrate revealed the significantly lowest ΔΕ values of all the substrates (P = 0.05). Regarding the translucency parameters for ceramics of different thicknesses, a significant difference was observed among all groups except in Suprinity. CONCLUSIONS: Different ceramic types with different thicknesses and substrate strongly affect translucency and masking. CLINICAL SIGNIFICANCE: Fabricating durable aesthetic restorations that also meets patients' expectations is among the most significant challenges in dentistry. With high demand for more natural restorations, ceramics based on computer-aided design (CAD) and computer-aided manufacture (CAM) became popular and exhibited excellent results. However, various factors such as abutment shade, luting cement color, and ceramic type, thickness, and translucency may affect the prosthesis shade. The objective of this study was to evaluate the effects of these factors on the final shades of CAD/CAM-based ceramic restorations.
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OBJECTIVES: In-vitro evaluation of the influence of preparation design and thickness of ceramic veneers on the interfacial bond using optical coherence tomography (OCT). METHODS: Sixty-four central incisors were randomly assigned to four preparation designs differing from no to complete dentine exposure (n = 16 each): non-prep (NP), minimal-invasive (MI, no dentine exposure), semi-invasive (SI, 50% dentine) and invasive (I, 100% dentine). Ceramic veneers (IPS InLine Veneer) of two thicknesses (0.2-0.5 mm (T1) and > 0.5-1.2 mm (T2)) were etched, silanized, and adhesively luted (Optibond FL, Variolink Veneer). After water storage (37 °C, 21d), thermocycling (2000 cycles, 5°-55 °C), and mechanical loading (2 + 1 million cycles, 50 + 100 N) specimens were imaged by spectral-domain OCT (Telesto II, Thorlabs). Adhesive defects at the ceramic-composite and tooth-composite interfaces were quantified on 35 equidistantly distributed OCT B-scans (length, %). Statistical differences were verified with Wilcoxon-/Mann-Whitney-U-test (α = 0.05). RESULTS: Adhesive defects appeared in all groups at both interfaces, albeit to differing extents (0.1 - 31.7%). NP and MI veneers showed no significant differences at the interfaces (pi > 0.05). In groups, SI and I, significantly more adhesive defects appeared at the tooth-composite compared to the veneer-composite interface (pi ≤ 0.039). The following preparation designs and veneer thicknesses showed differences (pi ≤ 0.021): Veneer-composite: NP-T1 < I-T1, MI-T1 < I-T1, I-T1 > I-T2; Tooth-composite: NP-T1 < SI-T1, NP-T1 < I-T1, NP-T2 > MI-T2, MI-T1 < SI-T1, MI-T1 < I-T1, SI-T1 < I-T1, MI-T2 < SI-T2, MI-T2 < I-T2. SIGNIFICANCE: The interface adhesion of ceramic veneers was influenced by the preparation design and the veneer thickness. A ceramic thickness of at least 0.5 mm and a preparation without exposing dentine is advantageous for the interfacial bond.
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Porcelana Dentária , Facetas Dentárias , Cerâmica , Teste de Materiais , Cimentos de Resina , Tomografia de Coerência ÓpticaRESUMO
OBJECTIVES: The purpose of this laboratory study was to evaluate the influence of bonding method and type of dental bonding surface on fracture resistance and survival rate of resin bonded occlusal veneers made from lithium disilicate ceramic after cyclic loading. METHODS: Fourty-eight extracted molars were divided into three groups (N=16) depending on the preparation: within enamel, within dentin/enamel or within enamel/composite resin filling. Lithium disilicate occlussal veneers were fabricated with a fissure-cusp thickness of 0.3-0.6mm. Restorations were etched (5% HF), silanated and adhesively luted using a dual-curing luting composite resin. Test groups were divided into two subgroups, one using a only a self-etching primer, the other additionally etching the enamel with phosphoric acid. After water storage (37°C; 21d) and thermocycling (7500 cycles; 5-55°C), specimens were subjected to dynamic loading in a chewing simulator (600,000 cycles; 10kg/2Hz). Surviving specimens were loaded until fracture using a universal testing machine. RESULTS: All specimens survived artificial aging, several specimens showed some damage. ANOVA revealed that enamel etching provided statistically significantly (p≤0.05) higher fracture resistance than self-etching when bonding to enamel and dentin. Self-etching provided statistically significant (p≤0.05) higher fracture resistance for the enamel-composite group than for the enamel group. Enamel etching provided statistically significant (p≤0.05) higher fracture resistance for the enamel and dentin group than for groups enamel and enamel-composite. SIGNIFICANCE: Etching enamel improved the fracture resistance of occlusal veneers when bonding to dentin and enamel and increased the survival rate when bonding to enamel.
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Colagem Dentária , Porcelana Dentária , Cerâmica , Análise do Estresse Dentário , Teste de Materiais , Cimentos de Resina , Propriedades de Superfície , Taxa de SobrevidaRESUMO
PURPOSE: The aim of this study was to evaluate the effect of thickness of zirconia on curing efficiency of resin cements. MATERIALS AND METHODS: Four discs with 4.0 mm in diameter were prepared from non-HIP translucent zirconia blocks using a CAD/CAM system and feldspathic ceramic was layered onto discs. Thus, 4 ceramic disc samples were fabricated: (G) 0.5 mm zirconia- as a control group, (G1) 0.5 mm zirconia and 0.5 mm feldspathic, (G2) 1.0 mm zirconia and 0.5 mm feldspathic and (G3) 2.0 mm zirconia and 0.5 mm feldspathic ceramic layer. 2 different dual cure cements were polymerized using a LED curing unit. Degree of conversion was evaluated using Vickers Hardness Test and depths of cure of samples were measured. Data were analyzed statistically using One-way ANOVA and Tukey's HSD test (p<0.05). RESULTS: Microhardness and depth of cure values were different under same thickness of ceramic discs for two resin cements. As the thickness of the zirconia discs increased, the microhardness values and depth of cure decreased. CONCLUSION: Photocuring time cannot be the same for all clinical conditions, under thicker zirconia restorations (>2.0 mm), an extended period of light curing or a light unit with a high irradiance should be used.
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OBJECTIVES: The purpose of this in-vitro study was to evaluate the influence of ceramic thickness and type of dental bonding surface on the fracture resistance of non-retentive full-coverage adhesively retained occlusal veneers made from lithium disilicate ceramic. METHODS: Seventy-two extracted molars were divided into three test groups (N=24) depending on the location of the occlusal veneer preparation: solely within enamel, within enamel and dentin or within enamel and an occlusal composite resin filling. For each test group, occlusal all-ceramic restorations were fabricated from lithium disilicate ceramic blocks (IPS e.max CAD) in three subgroups with different thicknesses ranging from 0.3 to 0.7mm in the fissures and from 0.6 to 1.0mm at the cusps. The veneers were etched (5% HF), silanated and adhesively luted using a self etching primer and a composite luting resin (Multilink Primer A/B and Multilink Automix). After water storage at 37°C for 3 days and thermal cycling for 7500 cycles at 5-55°C, specimens were subjected to dynamic loading in a chewing simulator with 600,000 loading cycles at 10kg combined with thermal cycling. Unfractured specimens were loaded until fracture using a universal testing machine. Statistical analysis was performed using Kruskal-Wallis and Wilcoxon tests with Bonferroni-Holm correction for multiple testing. RESULTS: Only specimens in the group with the thickest dimension (0.7mm in fissure, 1.0mm at cusp) survived cyclic loading without any damage. Survival rates in the remaining subgroups ranged from 50 to 100% for surviving with some damage and from 12.5 to 75% for surviving without any damage. Medians of final fracture resistance ranged from 610 to 3390N. In groups with smaller ceramic thickness, luting to dentin or composite provided statistically significant (p≤0.05) higher fracture resistance than luting to enamel only. The thickness of the occlual ceramic veneers had a statistically significant (p≤0.05) influence on fracture resistance. SIGNIFICANCE: The results suggest to use a thickness of 0.7-1mm for non-retentive full-coverage adhesively retained occlusal lithium disilicate ceramic restorations.