Electrochemical Direct Synthesis of <i>N</i>-Sulfenylimines from Amines in the Presence of Thiophenols.

Shalamu, Maidina; Saimi, Naibijiang; Luo, Shiwei; Maihemuti, Mailikezhati; Abudu Rexit, Abulikemu

Electrochemical Direct Synthesis of N-Sulfenylimines from Amines in the Presence of Thiophenols.

Shalamu, Maidina; Saimi, Naibijiang; Luo, Shiwei; Maihemuti, Mailikezhati; Abudu Rexit, Abulikemu.

Afiliación

Shalamu M; Department of Chemistry, Xinjiang Normal University, Urumqi 830054, China.
Saimi N; Department of Chemistry, Xinjiang Normal University, Urumqi 830054, China.
Luo S; Department of Chemistry, University of Science and Technology of China, Hefei 230026, China.
Maihemuti M; School of Chemical Engineering, Xinjiang University, Urumqi 830046, China.
Abudu Rexit A; Department of Chemistry, Xinjiang Normal University, Urumqi 830054, China.

J Org Chem ; 89(6): 3696-3701, 2024 Mar 15.

Article en En | MEDLINE | ID: mdl-38393326

ABSTRACT

ABSTRACT

N-Sulfenylimines are important molecules owing to their value in organic synthesis. Herein, we developed an electrochemical oxidative cross-coupling reaction between amines and thiols to synthesize N-sulfenylimines without a transition-metal catalyst and external oxidant. Various amines and thiols were compatible, generating the desired products in up to 86% yield.

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Texto completo: 1 Colección: 01-internacional Banco de datos: MEDLINE Idioma: En Revista: J Org Chem Año: 2024 Tipo del documento: Article País de afiliación: China

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