Your browser doesn't support javascript.
loading
Efficient Route for the Preparation of Composite Resin Incorporating Silver Nanoparticles with Enhanced Antibacterial Properties.
Beery, Drake; Mottaleb, Mohammad Abdul; Meziani, Mohammed J; Campbell, James; Miranda, Isabella Pires; Bellamy, Michael.
Afiliação
  • Beery D; Department of Natural Sciences, Northwest Missouri State University, 800 University Drive, Maryville, MO 64468, USA.
  • Mottaleb MA; Center for Innovation and Entrepreneurship, Northwest Missouri State University, 800 University Drive, Maryville, MO 64468, USA.
  • Meziani MJ; Institute of Drug & Biotherapeutic Innovation (IDBI), Office of the Vice President for Research Doisy Research Center (DRC), Saint Louis University, 1100 South Grand Blvd, Saint Louis, MO 63104, USA.
  • Campbell J; Department of Natural Sciences, Northwest Missouri State University, 800 University Drive, Maryville, MO 64468, USA.
  • Miranda IP; Center for Innovation and Entrepreneurship, Northwest Missouri State University, 800 University Drive, Maryville, MO 64468, USA.
  • Bellamy M; Department of Natural Sciences, Northwest Missouri State University, 800 University Drive, Maryville, MO 64468, USA.
Nanomaterials (Basel) ; 12(3)2022 Jan 29.
Article em En | MEDLINE | ID: mdl-35159816
ABSTRACT
An efficient and facile route for the immobilization of silver (Ag) nanoparticles (NPs) in anion exchange resin beads with different silver loading is proposed. In this method, BH4- ions were first introduced into chloride-form resin through an ion exchange process with Cl- ions, followed by in-situ chemical reduction of Ag+ ions at the surface of the resin to form metallic Ag nanoparticles. Morphology and structure of the resulting Ag-resin nanocomposites were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), energy dispersive spectroscopy (EDS), Fourier transform infra-red (FTIR), inductively coupled plasma-optical emission spectrometry (ICP-OES), and thermogravimetry analysis (TGA). The results confirmed the presence of smaller diameter Ag NPs incorporated into the resin beads having an average diameter on the order of 10 nm with a few Ag NP clusters of 20-100 nm. The nanoparticles were homogeneously distributed throughout the resin. There were no dramatic increases in average particle sizes even at very high Ag loadings. The resin retained its structure and stability, allowing higher stability of immobilized AgNPs than the colloidal ones. The Ag-loaded resins made with 50 mM AgNO3 were tested for antibacterial activity in vitro against Escherichia coli (E. coli) as a model microbial contaminant in water. Results showed greater than 99% bacterial inhibition within 3 h of exposure. The resin form offers greater ease of handling, long-term storage at room temperature, reusability in repeated reactions, and reduces the risk of environmental contamination.
Palavras-chave

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Revista: Nanomaterials (Basel) Ano de publicação: 2022 Tipo de documento: Article País de afiliação: Estados Unidos

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Revista: Nanomaterials (Basel) Ano de publicação: 2022 Tipo de documento: Article País de afiliação: Estados Unidos