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Zhong Yao Cai ; 38(11): 2321-3, 2015 Nov.
Artigo em Chinês | MEDLINE | ID: mdl-27356384

RESUMO

OBJECTIVE: To study the chemical constituents of Mongolian medicine Halenia corniculata. METHODS: Positive phase and reversed phase silica gel, as well as Sephadex LH-20 methods were used to separate and purify. The structure of the isolated constituents was identified according to the NMR spectroscopy data and the literature data. RESULTS: Nine compounds were isolated from 95% ethanol extracts of petroleum ether part of Halenia corniculata and identified as: 1-hydroxy-2,3,4,6-tetramethoxyxanthone (1), 1-hydroxy-2,3, 5-trimethoxyxanthone (2) 1-hydroxy-3,7-dimethoxyxanthone (3), 1-hydroxy-3,5,6,7,8-pentamethoxyxanthone (4), 1-hydroxy-2,3,4, 7-tetramethoxyxanthone (5), 1-hydroxy-3,5-dimethoxyxanthone (6),1-hydroxy-2,3,4,5,7-pentamethoxyxanthone (7), palmitic acid (8) and ß-sitosterol (9). CONCLUSION: Compounds 3, 4 and 8 are isolated from this genus for the first time, Compound 1 is isolated from this plant for the first time.


Assuntos
Gentianaceae/química , Compostos Fitoquímicos/análise , Extratos Vegetais/química , Alcanos , Medicina Tradicional da Mongólia , Compostos Fitoquímicos/isolamento & purificação , Sitosteroides/análise , Sitosteroides/isolamento & purificação , Solventes , Xantonas/análise , Xantonas/isolamento & purificação
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