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Low-budget 3D-printed equipment for continuous flow reactions.
Neumaier, Jochen M; Madani, Amiera; Klein, Thomas; Ziegler, Thomas.
Afiliação
  • Neumaier JM; Institute of Organic Chemistry, University of Tübingen, Auf der Morgenstelle 18, 72076 Tübingen, Germany.
  • Madani A; Institute of Organic Chemistry, University of Tübingen, Auf der Morgenstelle 18, 72076 Tübingen, Germany.
  • Klein T; Institute of Organic Chemistry, University of Tübingen, Auf der Morgenstelle 18, 72076 Tübingen, Germany.
  • Ziegler T; Institute of Organic Chemistry, University of Tübingen, Auf der Morgenstelle 18, 72076 Tübingen, Germany.
Beilstein J Org Chem ; 15: 558-566, 2019.
Article em En | MEDLINE | ID: mdl-30873240
ABSTRACT
This article describes the development and manufacturing of lab equipment, which is needed for the use in flow chemistry. We developed a rack of four syringe pumps controlled by one Arduino computer, which can be manufactured with a commonly available 3D printer and readily available parts. Also, we printed various flow reactor cells, which are fully customizable for each individual reaction. With this equipment we performed some multistep glycosylation reactions, where multiple 3D-printed flow reactors were used in series.
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Texto completo: 1 Temas: ECOS / Financiamentos_gastos Bases de dados: MEDLINE Tipo de estudo: Health_economic_evaluation Idioma: En Revista: Beilstein J Org Chem Ano de publicação: 2019 Tipo de documento: Article País de afiliação: Alemanha

Texto completo: 1 Temas: ECOS / Financiamentos_gastos Bases de dados: MEDLINE Tipo de estudo: Health_economic_evaluation Idioma: En Revista: Beilstein J Org Chem Ano de publicação: 2019 Tipo de documento: Article País de afiliação: Alemanha