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1.
J Synchrotron Radiat ; 20(Pt 2): 219-25, 2013 Mar.
Article in English | MEDLINE | ID: mdl-23412477

ABSTRACT

A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the `golden value'. The analysis showed that the slope error owing to anticlastic bending is less than the Darwin width. The X-rays were focused two-dimensionally using the crystal and a tangentially bent mirror. The observed profiles of the focal spot agreed well with the results of a ray-tracing calculation in the energy range from 8 to 17.5 keV. X-ray diffraction measurements with a high signal-to-noise ratio using this focusing system were demonstrated for a small protein crystal.


Subject(s)
Muramidase/chemistry , X-Ray Diffraction/methods , Animals , Crystallization/instrumentation , Equipment Design , Synchrotrons
2.
Phys Rev B Condens Matter ; 34(10): 6690-6694, 1986 Nov 15.
Article in English | MEDLINE | ID: mdl-9939309
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