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1.
Materials (Basel) ; 17(12)2024 Jun 14.
Artículo en Inglés | MEDLINE | ID: mdl-38930287

RESUMEN

This work presents issues related to selected errors accompanying spatial measurements of surface roughness using contact profilometry. The influence of internal heat sources, such as engines or control electronics, on the thermal expansion of the drive responsible for the measurement probe's movement in the X-axis direction was investigated. In terms of starting measurements on a thermally unstable device, the synchronization error of individual profile paths was 16.1 µm. Based on thermographic studies, the time required for full thermal stabilization of this drive was determined to be 6-12 h from when the device was turned on. It was demonstrated that thermal stabilization of the profilometer significantly reduced positioning errors of the measurement probe on the X-axis. Thermal stabilization time should be determined individually for a specific device variant. This research also determined how changes in the center of gravity caused by the measurement probe's movement affected the overall rigidity of the profilometer structure and the leveling of the tested surface. Laser interferometry was used for this purpose. The determined vulnerability of the profilometer structure was 0.8 µm for a measurement section of 25 mm. Understanding the described relationships will reduce errors associated with conducting measurements and preparing equipment for tests. Additionally, it will enable the correct evaluation of surface geometry.

2.
Materials (Basel) ; 16(4)2023 Feb 17.
Artículo en Inglés | MEDLINE | ID: mdl-36837339

RESUMEN

Osteoporosis is the most common metabolic disease of the skeletal system and is characterized by impaired bone strength. This translates into an increased risk of low-energy fractures, which means fractures caused by disproportionate force. This disease is quite insidious, its presence is usually detected only at an advanced stage, where treatment with pharmaceuticals does not produce sufficient results. It is obligatory to replace the weakened bone with an implant. For this reason, it is necessary to look at the possibilities of surface modification used in tissue engineering, which, in combination with the drugs for osteoporosis, i.e., bisphosphonates, may constitute a new and effective method for preventing the deterioration of the osteoporotic state. To achieve this purpose, titanium implants coated with magnesium or zinc zeolite were prepared. Both the sorption and release profiles differed depending on the type of ion in the zeolite structure. The successful release of risedronate from the materials at a low level was proven. It can be concluded that the proposed solution will allow the preparation of endoprostheses for patients with bone diseases such as osteoporosis.

3.
Materials (Basel) ; 16(3)2023 Jan 31.
Artículo en Inglés | MEDLINE | ID: mdl-36770206

RESUMEN

In the article, the new concept of plasma-sprayed coatings for the cylinder liner was presented. The new type of powder containing WC-CrC-Ni with a 5 and 10 wt. % addition of nano-YSZ powder was plasma-sprayed on aluminum 2017 alloy samples. The selection of optimal plasma-spraying parameters was made taking into account the thickness, porosity, and hardness of the coatings. For the coatings obtained according to the developed parameters, the analysis of their microstructure, chemical, and phase composition was performed. At the next stage, the friction coefficient of the developed coatings was tested and compared with the properties of a classic cast-iron cylinder liner. The obtained results suggest that the developed type of coating might be used for cylinder liner applications after a deeper friction analysis.

4.
Materials (Basel) ; 16(14)2023 Jul 12.
Artículo en Inglés | MEDLINE | ID: mdl-37512235

RESUMEN

The aim of this research was to analyze the effect of inorganic additives on the tribological properties of the high-density polyethylene (HDPE) matrix composite surface. Titanium (Ti) and hexagonal boron nitride (hBN) were added in different mass fractions. The samples were produced by pressing a pre-prepared mixture of granules. The composite samples with the following mass fractions of additives were fabricated: 5% hBN, 10% hBN, 28% Ti-2% hBN, 23% Ti-7% hBN, and 20% Ti-10% hBN. An even distribution of individual additives' concentrations was confirmed. Observations of morphology, surface topography, hardness, and tribological measurements were conducted using reciprocating motion tests with the "pin-on-flat" and rotational tests with the "pin-on-disc" configuration. Subsequently, microscopic observations and measurements of the wear track profile were carried out. Additionally, geometry parameters of the contacting elastic body were calculated for various counter-samples. It was found that the Shore D hardness of samples containing Ti and hBN increased with the Ti content, while the coefficient of friction (COF) value decreased. The addition of hBN alone did not significantly affect the hardness, regardless of the ratio, while the COF increased with the increasing hBN content. The COF value doubled with the addition of 10% hBN (COF = 0.22), whereas the addition of 90% Ti-10% hBN resulted in a decrease in the COF value, to COF = 0.83. The highest hardness value was obtained for the sample containing 28% Ti-2% hBN (66.5), while the lowest was for the sample containing 10% hBN (63.2). The wear track analysis, including its height and width caused by deformation, was detected using a focal differentiation microscope and scanning electron microscopy. Additionally, EDS maps were generated to determine the wear characteristics of the composite.

5.
Materials (Basel) ; 16(15)2023 Jul 29.
Artículo en Inglés | MEDLINE | ID: mdl-37570052

RESUMEN

The performance of a heat sink is significantly influenced by the type of cooling used: passive or active (forced), the shape of the heat sink, and the material from which it is made. This paper presents a review of the literature on the influence of geometry and surface parameters on effective heat transfer in heat sinks. The results of simulation studies for three different heat sink fin geometries and cooling types are presented. Furthermore, the influence of the surface texture of the heat sink fins on the heat transfer efficiency was determined. It was shown that the best performance in terms of geometries was that of a wave fin heat sink. When the surface texture was analyzed, it was found that an increase in the amplitude values of the texture decreases the heat dissipation efficiency in the case of active cooling, while for passive cooling, an increase in these parameters has a beneficial effect and increases the effective heat transfer to the surroundings. The cooling method was found to be the most important factor affecting heat dissipation efficiency. Forced airflow results in more efficient heat transfer from the heat sink fins to the surroundings.

6.
Materials (Basel) ; 16(18)2023 Sep 15.
Artículo en Inglés | MEDLINE | ID: mdl-37763511

RESUMEN

The use of thermoplastic materials has had significant growth in recent years. However, with great mechanical requirements, thermoplastics have limitations to their use. To improve these restrictions, these materials are reinforced to obtain better properties. Polypropylene is one of the most versatile polymers and is used in almost all modern industries. Thus, the aim of this study is to create composite materials that offer performance for various industrial fields using carbon fiber fabric reinforcement, which is an inexpensive material widely used by the aerospace, automotive, and marine industries. The samples are produced by the over-injection molding of polypropylene. The investigation is focused on the impact of two critical control parameters in the injection molding process: temperature and pressure. Twelve experiments have therefore been considered, taking into account the combination of three factors: the presence or absence of carbon fiber fabric reinforcement, three levels of temperature (200 °C, 220 °C, and 240 °C), and two injection pressures (5000 kPa and 10,000 kPa). To evaluate the influence of these factors, three analyses were carried out: first, on the samples' shrinkage using a portable metrology-grade 3D laser scanner; second, on the internal defects using computed tomography (CT); and third, on the mechanical properties with tensile tests. From the results obtained, it is observed that the mold shrinkage fell slightly when PP samples were reinforced with carbon fiber, with both materials (PP and carbon-fiber-reinforced PP) having linear behavior with temperature. It is also noticed that polypropylene behaves as a crystalline material when processed at higher temperatures and pressures. From tests on the mechanical properties, it is concluded that the mean yield strength of PP-CF for injection temperatures of 220 °C and 240 °C represents an increase of 43% compared to the non-reinforced material.

7.
Scanning ; 36(1): 170-83, 2014.
Artículo en Inglés | MEDLINE | ID: mdl-23878095

RESUMEN

Several random surface topographies were analyzed. They were measured by optical (Talysurf CCI Lite) method. They represent one- and two-process anisotropic and isotropic surfaces. These surfaces were rotated of ± 1° and ± 2° by two methods: on the plane table (before measurement) and virtually (after measurement) using the software TalyMap Gold. After each measurement or surface rotation, each surface was levelled. Then, the forms were removed using polynomial of the 3rd degree. Areal surface topography parameters from standard ISO 25178 were calculated. The relative deviations of parameters were determined. The tendency of surface topography changes characteristic to various surface types were analyzed. It was found that change in orientation to the measurement direction of both isotropic and anisotropic surfaces could be substantial source of the measurement uncertainty. Functional parameter Smr and also feature parameters Sda, Sha, Sdv, Shv, and Spd are the mostly sensitive on measurement orientation. Statistical amplitude parameters Sa and Sq are more stable than parameters describing maximum surface height, like Sz, Sp, and Sv. The effect of surface orientation to measurement direction on values of functional parameters from V group was small. It was shown that changes of Sdq, Sdr, and Spc parameters describing hybrid properties due to surface rotation before measurement were smaller than those caused by change in surface orientation after measurement.

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