In Operando Monitoring the Stress Evolution of Silicon Anode Electrodes during Battery Operation via Optical Fiber Sensors.

Silicon (Si) anode has attracted broad attention because of its high theoretical specific capacity and low working potential. However, the severe volumetric changes of Si particles during the lithiation process cause expansion and contraction of the electrodes, which induces a repeatedly repair of solid electrolyte interphase, resulting in an excessive consuming of electrolyte and rapid capacity decay. Clearly known the deformation and stress changing at µÎµ resolution in the Si-based electrode during battery operation provides invaluable information for the battery research and development. Here, an in operando approach is developed to monitor the stress evolution of Si anode electrodes via optical fiber Bragg grating (FBG) sensors. By implanting FBG sensor at specific locations in the pouch cells with different Si anodes, the stress evolution of Si electrodes has been systematically investigated, and Δσ/areal capacity is proposed for stress assessment. The results indicate that the differences in stress evolution are nested in the morphological changes of Si particles and the evolution characteristics of electrode structures. The proposed technique provides a brand-new view for understanding the electrochemical mechanics of Si electrodes during battery operation.

Strain measurement with adaptive local feature extraction method based on special fiber OFDR system.

The optical fiber distributed strain sensor based on the optical frequency domain reflectometer (OFDR) preserves its dominant position in short-distance measurement fields with high spatial resolution, such as biomedical treatment, soft robot, etc. However, owing to the weak intensity of the Rayleigh backscattered signal (RBS) in the single-mode fiber (SMF) and complex computation, the large strain changes cannot be precisely and rapidly demodulated by the traditional cross-correlation method. In this work, the OFDR with backscattering enhanced optical fiber (BEOF) is proposed and demonstrated for fast and large strain measurement. By enhancing the RBS amplitude, the signal-to-noise ratio (SNR) is improved, resulting in a higher similarity between the reference signal and test signal, which is beneficial for the expansion of the strain measurement range. Moreover, the adaptive local feature extraction and matching (ALFEM) algorithm is presented and demonstrated, which replaces the traditional cross-correlation method for strain demodulation and fast measurement. On account of the enhancement ratio of BEOF, the dominant characteristic data segment can be extracted from whole wavelength data. In the experiments, the enhancing ratio of BEOF is designed as 10, resulting in the spatial resolution reaches 400µm and the strain measurement range is greatly increased to 4800µÉ›. Further, the effectiveness of the ALFEM algorithm has been verified, in which the strain demodulation time is approximately 25% of that of the traditional method. This scheme fully exploits the enhancement characteristic of the BEOF and is also applicable to the systems based on other types of BEOF, different strain changes and sensing distances.

Investigations on diverse dynamics of soliton triplets in mode-locked fiber lasers.

Optical soliton molecules exhibiting behaviors analogous to matter molecules have been the hotspot in the dissipative system for decades. Based on the dispersion Fourier transformation technique, the real-time spectral interferometry has become the popular method to reveal the internal dynamics of soliton molecules. The rising degrees of freedom in pace with the increased constitutes of soliton molecules yield more intriguing sights into the internal motions. Yet the soliton molecules with three or more pulses are rarely investigated owing to the exponentially growing complexity. Here, we present both experimental and theoretical studies on the soliton molecules containing three solitons. Different assemblies of the constitutes are categorized as different types of soliton triplet akin to the geometric isomer, including equally-spaced triplet and unequally-spaced triplet. Typical soliton triplets with different dynamics including regular internal motions, hybrid phase dynamics and complex dynamics involving separation evolution are experimentally analyzed and theoretically simulated. Specifically, the energy difference which remains elusive in experiments are uncovered through the simulation of diverse triplets with plentiful dynamics. Moreover, the multi-dimensional interaction space is proposed to visualize the internal motions in connection with the energy exchange, which play significant roles in the interplays among the solitons. Both the experimental and numerical simulations on the isomeric soliton triplets would release a larger number of degrees of freedom and motivate the potentially artificial configuration of soliton molecules for various ultrafast applications, such as all-optical buffering and multiple encoding for telecommunications.

SNR enhancement of quasi-distributed weak acoustic signal detection by elastomers and MMF integrated Φ-OTDR.

We have proposed and demonstrated a weak acoustic signal detection technology based on phase-sensitive optical time-domain reflectometry (Φ-OTDR). Non-contact acoustic signals transmitting through air gap between the sound source and the receiver are difficult to detect due to fast attenuation. In order to improve the detection ability of non-contact weak acoustic signals, we demonstrate that multi-mode fiber (MMF) is a better solution than single-mode fiber (SMF) benefiting from its larger core and higher Rayleigh backscattering (RBS) capture coefficient. The frequency signal-to-noise ratio (SNR) has been enhanced by 9.26 dB. Then, with the help of 3D printing technology, elastomers have been designed to further enhance the detection ability due to the high-sensitive response to acoustic signals. Compared with the previous reported "I" type elastomer, the location and frequency SNR enhancement caused by our new proposed "n" type elastomer are 8.39 dB and 11.02 dB in SMF based system. The values are further improved to 10.51 dB and 13.38 dB in MMF and "n" type elastomer integrated system. And a phase-pressure sensitivity of -94.62 dB re rad/µPa has been achieved at 2.5 kHz. This non-contact weak acoustic signal detection technique has great application potential in the quasi-distributed partial discharge (PD) detection of smart grid.

Fiber Bragg grating displacement sensor based on synchronous deformation sensing for real-time monitoring of a tunnel lining.

A fiber Bragg grating (FBG) displacement sensor based on synchronous sensing is developed for real-time monitoring of a tunnel lining. The sensing principle and mechanical structure of the proposed sensor are analyzed and simulated, and its sensitization effectiveness and temperature compensation are verified. Equivalent model tests show that the sensor has a good linear sensitivity of 19.48 pm/mm and an excellent precision of 5.13×10-2 m m in the displacement range of 0-25 mm, which is basically consistent with the simulation results. The key traffic parameters of the train were successfully obtained by real-time monitoring of the tunnel lining in a field trial, which shows the superior capability of micro-displacement measurement of the sensor. Furthermore, good stability and excellent creep resistance have also been demonstrated. Our results provide theoretical guidance for the fabrication and package of the FBG displacement sensor, which is valuable for structure health monitoring (SHM) in civil engineering applications.

Diffraction characteristics of radiated tilted fiber grating and its spectrometer application.

We have numerically and experimentally presented the diffraction characteristics of radiated tilted fiber grating (RTFG) in terms of the spectrum, bandwidth, degree of polarization, angular dispersion, and temperature crosstalk. The theoretical and experimental results have shown that the polarization property, bandwidth, and dispersion of RTFG highly depended on the tilt angle of RTFG, and the RTFG has ultra-low temperature crosstalk. We have simulated the transmission spectrum of the RTFG with different tilt angles (25°, 31°, 38°, 45°, and 54°), in which the results show that the larger tilt angle has the wider bandwidth. The RTFGs with the tilt angle of 25°, 31°, 38°, 45°, and 54° have the 3dB bandwidth of 110 nm, 144 nm, 182 nm, 242 nm, and 301 nm, respectively. Besides, the degree of polarization (DOP) of the radiated light from RTFG with the different tilt angles are 0.876, 0.944, 0.967, 0.998, and 0.970, respectively, and the RTFG has the maximum DOP at the tilt angle of 45°, which could be used as single-polarization diffraction device. The experimental results show that with further increase or decrease of the tilt angle, the DOP of radiated light of RTFG would decrease. Both the theoretical and experimental results show that the smaller tilt angle could greatly improve the diffraction angular dispersion of RTFG, in which the 25°, 31°, 38°, and 45° RTFG have the angular dispersion of 0.2288 °/nm, 0.1026 °/nm, 0.0714 °/nm, and 0.0528 °/nm, respectively. Due to the broad working bandwidth, the diffraction angles of RTFG have ultra-low temperature crosstalk, where -0.00042, -0.00054, -0.00064, and -0.00099 degree / °C at the tilt angle of 25°, 31°, 38°, and 45°. Finally, we have demonstrated a miniaturized spectrometer integrated by a 25° RTFG, which has a high spectral resolution of 0.08 nm. The proposed RTFG would be an ideal in-fiber diffraction device and widely applied in spectral analysis, space optical communication, and Lidar areas.

High-precision distributed detection of rail defects by tracking the acoustic propagation waves.

Nowadays, early defect detection plays a significant role for the railway safety warning. However, the existing methods cannot satisfy the requirements of real-time and high-precision detection. Here, a high-precision, distributed and on-line method for detecting rail defect is proposed and demonstrated. When a train goes through defects, the instantaneous elastic waves will be excited by the wheel-rail interaction, which will further propagate along railway tracks bidirectionally. Through mounting the backscattering enhanced optical fiber on the railway as sensors, the fiber optic distributed acoustic sensing system can record the propagation trace precisely. Further, the acoustic propagation fitting method is applied onto the propagation data to detect and locate defects along the long-distance railway. Especially, the dual-frequency joint-processing algorithm is proposed to improve the location accuracy. The field test proves that multiple defects along the railway can be successfully identified and located with a standard deviation of 0.314m. To the best of our knowledge, this work is the first report of distributed rail defect detection, which will bring a breakthrough for high-precision structural damage detection in the infrastructures such as the railway, pipeline and tunnel.

Spatio-temporal joint oversampling-downsampling technique for ultra-high resolution fiber optic distributed acoustic sensing.

In order to suppress the noise of the coherent fiber distributed acoustic sensing (DAS) system, the spatio-temporal joint oversampling-downsampling technique is proposed. The spatial oversampling is used for artificially dense sampling, whose spacing is far less than the target spatial resolution. Then the spatial downsampling performed by the average of multiple differential sub-vectors is utilized to reduce the influence of noise vectors, which could completely eliminate the interfere fading without increasing any system complexity and introducing any crosstalk. Meanwhile, the temporal oversampling-downsampling is analyzed from the perspective of theory and simulation, demonstrating that the noise floor will decrease with the increase of downsampling coefficient. The temporal oversampling is carried out to expand the noise distribution bandwidth and ensure the correct quantization of the noise frequency. Then the temporal downsampling of differential phase reconstruction is utilized to recover the target bandwidth and reduce the out-of-band noise. The experimental results prove that the noise floor is inversely correlated with the spatiotemporal downsampling factors. The strain resolution of the DAS system with the proposed scheme can reach 2.58pε/√Hz@100Hz-500Hz and 9.47pε/√Hz@10Hz under the condition of DC-500Hz target bandwidth, as well as the probability of the large-noise sensing channels is greatly reduced from 44.32% to 0%. Moreover, the demodulated SNR of dynamic signal is improved by 20.8dB compared with the traditional method. Without any crosstalk, the noise floor is optimized 8dB lower than the averaging technique. Based on the proposed method, the high-performance DAS system has significant competitiveness in the applications with the demand of high-precision and high-sensitivity, such as passive-source seismic imaging and VSP exploration.

Multi-channel parallel ultrasound detection based on a photothermal tunable fiber optic sensor array.

A multi-channel parallel ultrasound detection system based on a photothermal tunable fiber optic sensor array is proposed. The resonant wavelength of the ultrasound sensor has a quadratic relationship with the power of a 980-nm heating laser. The maximum tuning range is larger than 15 nm. Through photothermal tuning, the inconsistent operating wavelengths of the Fabry-Perot (FP) sensor array can be solved, and then a multiplexing capacity of up to 53 can be theoretically realized, which could greatly reduce the time required for data acquisition. Then, a fixed wavelength laser with ultra-narrow linewidth is used to interrogate the sensor array. The interrogation system demonstrates a noise equivalent pressure (NEP) as low as 0.12 kPa, which is 5.5-times lower than the commercial hydrophone. Furthermore, a prototype of a four-channel ultrasound detection system is built to demonstrate the parallel detection capability. Compared with the independent detection, the SNR of parallel detection does not deteriorate, proving that the parallel detection system and the sensor array own very low cross talk characteristics. The parallel detection technique paves a way for real-time photoacoustic/ultrasound imaging.

In-fiber duplex optical antenna and its programmable spectral filter application.

In this Letter, we have proposed an in-fiber duplex optical antenna based on a 45° radiated titled fiber grating (RTFG), in which the 45° RTFG not only radiates the light from the fiber core to the free space, but also harvests the light from the free space back into the fiber core. Using the finite difference time domain method, we have theoretically analyzed the light recoupling efficiency of the RTFG. The simulated results have shown that the RTFG-based optical antennas have a maximum coupling efficiency of 10%. The recoupling wavelength and efficiency are related to the grating period and horizontal incidence angle. Furthermore, we demonstrate a programmable spectral filtering system based on the 45° RTFG antennas, which could achieve filtering with arbitrary spectral shapes. The spectral resolution is 0.4 nm and the insertion loss is around 20 dB. The proposed programmable spectral filtering system has a compact structure compared with the traditional filter.

In-fiber duplex optical antenna and its programmable spectral filter application: publisher's note.

This publisher's note contains corrections to Opt. Lett.47, 4937 (2022)10.1364/OL.468940.

High resolution and large sensing range liquid level measurement using phase-sensitive optic distributed sensor.

Liquid level sensor with large sensing range and high-resolution is essential for the application of industry monitoring. In this work, a distributed optical fiber liquid level sensor is proposed and demonstrated based on phase-sensitive optical time domain reflectometry (φ-OTDR). In the basic of the thermal optic effect, the temperature change will induce the fluctuation of the effective refractive indexes of the fiber core, as well as the fluctuation of the optical path of the light transmitting in the fiber. Therefore, the φ-OTDR can detect the liquid level with a large measurement range by interrogating the phase information along the fiber due to the temperature difference between the liquid and air. Further, the scattering enhanced optical fiber (SEOF) is used as the sensing fiber to improve the signal to noise ratio (SNR) of the phase signal. Moreover, a high sensitivity liquid level sensing head by wrapping the SEOF on a heat conductive cylinder is designed and optimized to improve the sensing resolution. In the experiment, the proposed distributed liquid level sensor presents a high sensitivity of 73.4 rad/mm, corresponding to a competitive liquid level resolution of 142µm based on the noise floor of 10.4 rad within 160 s. The field test validates a large sensing range of 20 cm which is limited by the cylinder length, while a potential sensing range could reach 320 m with the sensing fiber of 40 km, proving a dynamic range of 127.1 dB. The proposed liquid level sensor with large dynamic range and high sensing resolution can benefit potential application in smart industry platforms and biomedicine monitoring.

In-service crosstalk monitoring in multicore fibers based on precoded DMT system.

In-service crosstalk monitoring based on the precoding technique in a discrete multitone (DMT) system is proposed and validated experimentally. The method relies on the ability of time-frequency domain equalization of precoded DMT. Experiments on a 20 GBaud 16 quadrature amplitude modulation DMT system over seven-core weakly coupled multicore fibers (MCFs) are conducted. The inter-core instantaneous average crosstalk (IAXT) is gathered and evaluated in a period as short as 10 µm without disturbing the signal transmission. Such IAXT has a high correlation with the bit error ratio (BER), and a transmission performance evaluation strategy of the MCF transmitting system is developed according to the relationship between IAXT and BER.

In-situ DNA hybridization detection based on a reflective microfiber probe.

A label-free biosensor based on a reflective microfiber probe for in-situ real-time DNA hybridization detection is proposed and experimentally demonstrated. The microfiber probe is simply fabricated by snapping a non-adiabatic biconical microfiber through closing the oxyhydrogen flame during fiber stretching. Assisted with the Fresnel reflection at the end of microfiber, a reflective microfiber modal interferometer is realized. The in-situ DNA hybridization relies on the surface functionalization of a monolayer of Poly-L-lysine (PLL) and synthetic DNA sequences that bind to a given target with high specificity. The detection processes of DNA hybridization in various concentration of target DNA solutions are monitored in real-time and the experimental results present a minimum detectable concentration of 10pM with good repeatability. Additionally, the detection specificity is also investigated by immersing the microfiber probe into the non-complementary ssDNA solutions and observing the spectral variation. The proposed biosensor has advantages of high sensitivity, compact size, ease of use and simple fabrication, which makes it has great potential to be applied in a lot of fields such as disease diagnosis, medicine, and environmental science.

Stationary and pulsating vector dissipative solitons in nonlinear multimode interference based fiber lasers.

Rapid progress in real-time spectroscopy uncovers the spatio-spectral scenarios of ultrashort pulses in dissipative systems. Varieties of transient soliton dynamics on different timescales have been revealed. Here, we report on an experimental observation of stationary and pulsating vector dissipative solitons in a nonlinear multimode interference (NL-MMI) based fiber laser with net normal dispersion. Polarization non-discrimination of the NL-MMI mode-locking facilitates the dissipative soliton trapping process. Two orthogonally polarized components are coupled together through oppositely shifting their central frequencies to form the group-velocity-locked vector dissipative solitons (GVLVDSs). Dispersive Fourier transform (DFT) based polarization resolved measurement enables insights into the transient polarization dynamics and the long-term evolution. Particularly, both stationary and pulsating GVLVDSs are obtained with appropriate parameter settings. It is found that the quasi-stationary pulsating manner is accompanied with recurrent spectral breathing and energy oscillation; the two orthogonally polarized components possess synchronous pulsating manners due to the cross-phase modulation induced trapping mechanism and the similar formation process. Additionally, chaotic pulsation is also captured in sense that the spectra cannot recover to their original profiles despite of the harmonic energy oscillation. All these findings can enhance our understanding towards soliton pulsation with the freedom of vectorial degree.

Experimental observation of shaking soliton molecules in a dispersion-managed fiber laser.

Recent progress in real-time spectral interferometry enables access to the internal dynamics of optical multisoliton complexes. Here, we report on the first, to the best of our knowledge, experimental observation of shaking soliton molecules by means of the dispersive Fourier transform technique. Beyond the simplex vibrating soliton pairs, multiple oscillatory motions can jointly involve in the internal dynamics, reminiscent of the shaking soliton pairs. Both quasi-periodically and chaotically evolving phase oscillations are approached in the sense of different oscillatory frequencies. In addition, the shaking soliton pair combined with sliding phase dynamics is also observed, and is interpreted as the superposition of two different internal motions. All of these results shed new light on the internal dynamics of soliton molecules with higher degrees of freedom, as well as enrich the framework toward multisoliton complexes.

Sensitivity Characterization of Cascaded Long-Period Gratings Operating near the Phase-Matching Turning Point.

We characterized a cascaded long-period gratings (LPGs)-based sensor that was operating at the phase-matching turning point (PMTP). The cascaded LPGs constructed an in-fiber Mach-Zehnder interferometer (MZI), which exhibited a series of high-quality-factor (Q) narrow-bandwidth resonance peaks. As the LPG operated at the PMTP, the proposed sensor showed an ultrahigh refractive index (RI) and temperature sensitivity, and high measurement precision. In this study, we took an in-depth look at the effects of grating separation on Q-factor and sensitivity. The results showed that the sensitivity to the surrounding refractive index (SRI) reached 4741.5 nm/RIU at 1.4255 and 2138 nm/RIU, over the range of 1.335-1.373. In addition, the temperature sensitivity was around 4.84 nm/°C. With a 0.02 nm wavelength resolution, the RI and temperature sensing limits were 9.3 × 10-6 RIU and 5.5 × 10-3 °C.

Excessively tilted fiber grating-based vector magnetometer.

A compact optic-fiber vector magnetometer is proposed and experimentally demonstrated, which is based on an excessively tilted fiber grating (Ex-TFG) assistant with the magnetic fluid (MF). Without any complicated processing, the cladding mode resonances of the bare Ex-TFG packaged by the MF show high sensitivity to slight perturbations by the magnetic field. Due to the excellent magneto-optical properties of the MF and the azimuth-dependent refractive index sensitivity of the Ex-TFG, such a magnetometer can achieve the magnetic field intensity sensitivity of 2.45 nm/mT and the orientation sensitivity of 0.41 nm/deg. In addition, based on the spectral interrogation, the detection limit of the magnetic field intensity could reach around 8.1 µT at the minimum wavelength measurement accuracy of 0.02 nm.

Real-time access to the coexistence of soliton singlets and molecules in an all-fiber laser.

Recent progress in time-stretch spectroscopy accelerates the exploration of ultrafast dynamics in mode-locked lasers through mapping the spectral information into time domain. Here, we report on real-time access to the coexistence of soliton singlets and molecules in an all-fiber laser mode-locked by a 45° tilted fiber grating. By virtue of the dispersive Fourier transform process, spectral information of the pulse trains under multi-pulse states can be resolved. It is identified that soliton singlets and soliton molecules coexist in one cavity roundtrip with different assembling forms. In addition, consecutive recordings of the shot-to-shot spectra further enable insight into the transient dynamics of soliton molecules. Particularly, varieties of internal motions, including the diverging/oscillating phase evolution and the temporal separation vibration, are validated loosely bound intra-soliton molecules. All of these findings unveil the scenarios of multi-soliton phenomena in fiber lasers, as well as highlight the significance of pulse interaction towards both scientific research and practical applications.

In-fiber single-polarization diffraction grating based on radiant tilted fiber grating.

In this Letter, we propose an in-fiber single-polarization diffraction grating based on a radiant tilted fiber grating (TFG), in which the s-polarization light could be diffracted from the fiber core to free space with the wavelength-dependent diffraction angle. For the first time, we have presented the theoretical model of angular dispersion of a radiant TFG by employing the Fourier optics analysis method. The angular dispersion of the radiant TFG has been numerically characterized in terms of tilt angle, period, and wavelength. In the experiment, we have measured the diffraction angles and angular dispersion of the radiant TFGs with tilt angles of 41°, 45°, and 47° UV-inscribed into single-mode fiber, where the experimental results matched well with the simulation results. The simulation and experimental results have indicated that the diffraction light of radiant TFGs has a linear polarization state with over 0.99 degree of polarization at the tilt angle range from 41° to 47°.