Headspace single-drop microextraction gas chromatography mass spectrometry for the analysis of volatile compounds from herba asari.
J Anal Methods Chem
; 2013: 380705, 2013.
Article
en En
| MEDLINE
| ID: mdl-23607049
ABSTRACT
A rapid headspace single-drop microextraction gas chromatography mass spectrometry (SDME-GC-MS) for the analysis of the volatile compounds in Herba Asari was developed in this study. The extraction solvent, extraction temperature and time, sample amount, and particle size were optimized. A mixed solvent of n-tridecane and butyl acetate (1 1) was finally used for the extraction with sample amount of 0.750 g and 100-mesh particle size at 70°C for 15 min. Under the determined conditions, the pound samples of Herba Asari were directly applied for the analysis. The result showed that SDME-GC-MS method was a simple, effective, and inexpensive way to measure the volatile compounds in Herba Asari and could be used for the analysis of volatile compounds in Chinese medicine.
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Bases de datos:
MEDLINE
Idioma:
En
Revista:
J Anal Methods Chem
Año:
2013
Tipo del documento:
Article
País de afiliación:
China