A Staggered Vane-Shaped Slot-Line Slow-Wave Structure for W-Band Dual-Sheet Electron-Beam-Traveling Wave Tubes.

A staggered vane-shaped slot-line slow-wave structure (SV-SL SWS) for application in W-band traveling wave tubes (TWTs) is proposed in this article. In contrast to the conventional slot-line SWSs with dielectric substrates, the proposed SWS consists only of a thin metal sheet inscribed with periodic grooves and two half-metal enclosures, which means it can be easily manufactured and assembled and has the potential for mass production. This SWS not only solves the problem of the dielectric loading effect but also improves the heat dissipation capability of such structures. Meanwhile, the SWS design presented here covers a -15 dB S11 frequency range from 87.5 to 95 GHz. The 3-D simulation for a TWT based on the suggested SWS is also investigated. Under dual-electron injection conditions with a total voltage of 17.2 kV and a total current of 0.3 A, the maximum output power at 90 GHz is 200 W, with a 3 dB bandwidth up to 4 GHz. With a good potential for fabrication using microfabrication techniques, this structure can be a good candidate for millimeter-wave TWT applications.

Adaptation of an IRAM W-Band SIS Receiver to the INAF Sardinia Radio Telescope: A Feasibility Study and Preliminary Tests.

Radio telescopes are used by astronomers to observe the naturally occurring radio waves generated by planets, interstellar molecular clouds, galaxies, and other cosmic objects. These telescopes are equipped with radio receivers that cover a portion of the radio frequency (RF) and millimetre-wave spectra. The Sardinia Radio Telescope (SRT) is an Italian instrument designed to operate between 300 MHz and 116 GHz. Currently, the SRT maximum observational frequency is 26.5 GHz. A feasibility study and preliminary tests were performed with the goal of equipping the SRT with a W-band (84-116 GHz) mono-feed radio receiver, whose results are presented in this paper. In particular, we describe the adaptation to the SRT of an 84-116 GHz cryogenic receiver developed by the Institute de Radio Astronomie Millimétrique (IRAM) for the Plateau de Bure Interferometer (PdBI) antennas. The receiver was upgraded by INAF with a new electronic control system for the remote control from the SRT control room, with a new local oscillator (LO), and with a new refrigeration system. Our feasibility study includes the design of new receiver optics. The single side band (SSB) receiver noise temperature measured in the laboratory, Trec ≈ 66 K at 86 GHz, is considered sufficiently low to carry out the characterisation of the SRT active surface and metrology system in the 3 mm band.

Shadow Effect for Small Insect Detection by W-Band Pulsed Radar.

In radar entomology, one primary challenge is detecting small species (smaller than 5 cm) since these tiny insects reflect radiation that can be poorly observable and, therefore, difficult to interpret. After a literature search on radar entomology, this research found few works where it has been possible to sense insects with dimensions smaller than 5 cm using radars. This paper describes different methodologies to detect Mediterranean fruit flies with 5-6 mm sizes using a pulsed W-band radar and presents the experimental results that validate the procedures. The article's main contribution is the successful detection of Mediterranean fruit flies employing the shadow effect on the backscattered radar signal, achieving an 11% difference in received power when flies are present. So far, according to the information available and the literature search, this work is the first to detect small insects less than 1 cm long using a pulsed radar in W-Band. The results show that the proposed shadow effect is a viable alternative to the current sensors used in smart traps, as it allows not only detection but also counting the number of insects in the trap.

A 78.8-84 GHz Phase Locked Loop Synthesizer for a W-Band Frequency-Hopping FMCW Radar Transceiver in 65 nm CMOS.

A W-band integer-N phase-locked loop (PLL) for a frequency hopping frequency modulation continuous wave (FMCW) radar is implemented in 65-nm CMOS technology. The cross-coupled voltage-controlled oscillator (VCO) was designed based on a systematic analysis of the VCO combined with its push-pull buffer to achieve high efficiency and high output power. To provide a frequency hopping functionality without any overhead in the implementation, the center frequency of the VCO is steeply controlled by the gate voltage of the buffer, which effectively modifies the susceptance of the VCO load. A stand-alone VCO with the proposed architecture is fabricated, and it achieves an output power of 13.5 dBm, a peak power efficiency of 9.6%, and a tuning range of 3.5%. The phase noise performance of the VCO is -92.6 dBc/Hz at 1-MHz and -106.1 dBc/Hz at 10 MHz offset. Consisting of a third-order loop filter and a divider chain with a total modulus of 48, the locking range of the implemented PLL with the cross-coupled VCO is recorded from 78.84 GHz to 84 GHz, and its phase noise is -85.2 dBc/Hz at 1-MHz offset.

W-Band 4th Order Waveguide Filter Based on Double Layer SU8 Microfabrication.

This paper investigates the fabrication accuracy of the W-band SU-8 photoresist micromachined 4th order waveguide bandpass filters (BPF). The designed filter based on cylindrical resonators is excited in TM010 mode. It is ideally suitable for the layered SU-8 micromachining process as the height of the resonator is much smaller than one wavelength, the electromagnetic fields remain unchanged in the thickness direction. The filter is composed of three silver-coated SU-8 layers based on a double-layer overlay process. Excellent manufacturing tolerances can be controlled within 4 µm in the thickness direction, around 10 µm in double-layer stacking accuracy, and an average of 1° in vertical angle deviation. Various challenges encountered in the SU-8 process are investigated while corresponding general solutions are proposed for machining high-precision devices. The measured results show a return loss of 12.4 dB and a minimum insertion loss of 0.8 dB, which are in agreement with the simulated one. Stress and deformation analysis are also conducted to confirm the maximum pressure that the filter can withstand and maintain good transmission performance.

A 90 GHz Broadband Balanced 8-Way Power Amplifier for High Precision FMCW Radar Sensors in 65-nm CMOS.

We present a W-band 8-way wideband power amplifier (PA) for a high precision frequency modulated continuous wave (FMCW) radar in 65-nm CMOS technology. To achieve a broadband operation with an improved output power for a high range resolution and high distance coverage of FMCW radar sensors, a balanced architecture is employed with the Lange coupler which naturally combines the output powers from two 4-way push-pull PAs. By utilizing a transformer-based push-pull structure with a cross-coupled capacitive neutralization technique, the gate-drain capacitance of the 4-way PA is compensated for the stabilization with an improved power gain. Interstage matching was performed with transformers for a reduced loss from the matching network and minimal area occupation. The implemented balanced 8-way PA achieved a saturated output power (Psat) of 16.5 dBm, a 1-dB compressed output power (OP1dB) of 13.3 dBm, a power-added efficiency (PAE) of 9.9% at 90 GHz and 3-dB power bandwidth was 20.4 GHz (79.2-99.6 GHz).

Spin-label W-band EPR with seven-loop-six-gap resonator: Application to lens membranes derived from eyes of a single donor.

Spin-label W-band (94 GHz) EPR with a five-loop-four-gap resonator (LGR) was successfully applied to study membrane properties (L. Mainali, J.S. Hyde, W.K. Subczynski, Using spin-label W-band EPR to study membrane fluidity in samples of small volume, J. Magn. Reson. 226 (2013) 35-44). In that study, samples were equilibrated with the selected gas mixture outside the resonator in a sample volume ~100 times larger than the sensitive volume of the LGR and transferred to the resonator in a quartz capillary. A seven-loop-six-gap W-band resonator has been developed. This resonator permits measurements on aqueous samples of 150 nL volume positioned in a polytetrafluoroethylene (PTFE) gas permeable sample tube. Samples can be promptly deoxygenated or equilibrated with an air/nitrogen mixture inside the resonator, which is significant in saturation-recovery measurements and in spin-label oximetry. This approach was tested for lens lipid membranes derived from lipids extracted from two porcine lenses (single donor). Profiles of membrane fluidity and the oxygen transport parameter were obtained from saturation-recovery EPR using phospholipid analog spin-labels. Cholesterol analog spin-labels allowed discrimination of the cholesterol bilayer domain and acquisition of oxygen transport parameter profiles across this domain. Results were compared with those obtained previously for membranes derived from a pool of 100 lenses. Results demonstrate that EPR at W-band can be successfully used to study aqueous biological samples of small volume under controlled oxygen concentration.

A Whole W-Band Multi-Polarization Horn Antenna Based on Boifot-Type OMT.

A wideband multi-polarized square-horn antenna based on an orthogonal mode transducer (OMT) is developed for working in the whole W-band in this paper. The designed antenna is capable of radiating multiple polarization modes as horizontal polarization (HP) and vertical polarization (VP) when as single-port excitation and left-handed circular polarization (LHCP) and right-handed circular polarization (RHCP) when as dual-port excitation, owing to the characteristic of the OMT with the transmitting of orthogonally polarized waves. A CNC-layered fabrication approach is proposed, which means that the antenna prototype integrating with a Boifot-type OMT, turning waveguide, twisting waveguide and phase shifter is divided into three layers along the vertical direction to be fabricated based on computerized numerical control (CNC) technology. In the design, the turning waveguide and twisting waveguide are employed to achieve plane consistency of the antenna branch ports. Furthermore, a phase shifter is designed to compensate the orthogonally polarized waves, which can keep the phase of the orthogonally polarized waves consistent in a wideband frequency range from 75 GHz to 110 GHz. A prototype is fabricated and measured to verify the performance of the proposed multi-polarization antenna, and the measured results agree well with the simulation ones. In the whole W-band, the value of return loss is better than 10 dB of all polarization modes, and the value of AR of the LHCP and RHCP is below 3.5 dB. The maximum gain of the antenna reaches up to 18.8 dBi at 110 GHz. In addition, regarding the layered structure, the possible layered assembly error analysis is discussed, which verifies the feasibility of the layered machining for this antenna.

A 77 GHz Power Amplifier with 19.1 dBm Peak Output Power in 130 nm SiGe Process.

This article reports a two-stage differential structure power amplifier based on a 130 nm SiGe process operating at 77 GHz. By introducing a tunable capacitor for amplitude and phase balance at the center tap of the secondary coil of the traditional Marchand balun, the balun achieves amplitude imbalance less than 0.5 dB and phase imbalance less than 1 degree within the operating frequency range of 70-85 GHz, which enables the power amplifier to exhibit comparable output power over a wide operating frequency band. The power amplifier, based on a designed 3-bit digital analog convertor (DAC)-controlled base bias current source, exhibits small signal gain fluctuation of less than 5 dB and saturation output power fluctuation of less than 2 dB near the 80 GHz frequency point when the ambient temperature varies in the range of -40 °C to 125 °C. Benefiting from the aforementioned design, the tested single-path differential power amplifier exhibits a small signal gain exceeding 16 dB, a saturation output power exceeding 18 dBm, and a peak saturation output power of 19.1 dBm in the frequency band of 70-85 GHz.

A Substrate Integrated Waveguide-Based W-Band Antenna for Microwave Power Transmission.

A W-band slot array antenna based on a substrate integrated waveguide (SIW) for microwave power transmission (MPT) is proposed in this paper. By size optimization, the transition from the rectifier element to the antenna is limited to a small size. It realizes a compact arrangement of the radiating slots, which not only improves the aperture efficiency of the antenna but also makes it easy to integrate into a large-scale array. For antenna testing, a coplanar waveguide-SIW-rectangular waveguide transition structure is added at the end of the antenna, and an antenna with this transition structure is processed by PCB printing technology and measured. The measured reflection coefficient is less than -10 dB at 90-96 GHz, the aperture efficiency is greater than 60% at 93.5-94.5 GHz, the maximum gain is 13.2 dB at 93.5 GHz, and the aperture efficiency is 79%. The test results of the antenna show that the antenna has a good performance and can be applied to the MPT system as a rectenna.

A Novel Wideband Transition from LTCC Laminated Waveguide to Air-Filled Rectangular Waveguide for W-band Applications.

In this paper, a novel wideband transition from a laminated waveguide (LWG) to an air-filled rectangular waveguide (RWG) is proposed for millimeter-wave integration solutions based on multilayer low-temperature co-fired ceramic (LTCC) technology. The integrated transition cavity is divided into several resonators by introducing five grounded via holes. Due to the magnetic wall existing in the symmetry plane, the equivalent circuit of the proposed transition can be simplified as a three-pole filter model to explain the working mechanism with wideband performance. A W-band integrated LWG-to-RWG transition is designed as an example using LTCC technology. Two back-to-back prototypes with different lengths are fabricated and measured. A measured 25.7% bandwidth from 76 GHz to 101 GHz can be achieved for return loss better than 14 dB. The average insertion loss of a single transition is about 0.5 dB. The compact structure and wideband performance give it potential in high-density millimeter-wave and terahertz packaging.

Uniform Field Resonators for EPR Spectroscopy: A Review.

Cavity resonators are often used for electron paramagnetic resonance (EPR). Rectangular TE102 and cylindrical TE011 are common modes at X-band even though the field varies cosinusoidally along the Z-axis. The authors found a way to create a uniform field (UF) in these modes. A length of waveguide at cut-off was introduced for the sample region, and tailored end sections were developed that supported the microwave resonant mode. This work is reviewed here. The radio frequency (RF) magnetic field in loop-gap resonators (LGR) at X-band is uniform along the Z-axis of the sample, which is a benefit of LGR technology. The LGR is a preferred structure for EPR of small samples. At Q-band and W-band, the LGR often exhibits nonuniformity along the Z-axis. Methods to trim out this nonuniformity, which are closely related to the methods used for UF cavity resonators, are reviewed. In addition, two transmission lines that are new to EPR, dielectric tube waveguide and circular ridge waveguide, were recently used in UF cavity designs that are reviewed. A further benefit of UF resonators is that cuvettes for aqueous samples can be optimum in cross section along the full sample axis, which improves quantification in EPR spectroscopy of biological samples.

An Improved Large Signal Model for 0.1 µm AlGaN/GaN High Electron Mobility Transistors (HEMTs) Process and Its Applications in Practical Monolithic Microwave Integrated Circuit (MMIC) Design in W band.

An improved empirical large signal model for 0.1 µm AlGaN/GaN high electron mobility transistor (HEMT) process is proposed in this paper. The short channel effect including the drain induced barrier lowering (DIBL) effect and channel length modulation has been considered for the accurate description of DC characteristics. In-house AlGaN/GaN HEMTs with a gate-length of 0.1 µm and different dimensions have been employed to validate the accuracy of the large signal model. Good agreement has been achieved between the simulated and measured S parameters, I-V characteristics and large signal performance at 28 GHz. Furthermore, a monolithic microwave integrated circuit (MMIC) power amplifier from 92 GHz to 96 GHz has been designed for validation of the proposed model. Results show that the improved large signal model can be used up to W band.

The use of composite pulses for improving DEER signal at 94GHz.

The sensitivity of pulsed electron paramagnetic resonance (EPR) measurements on broad-line paramagnetic centers is often limited by the available excitation bandwidth. One way to increase excitation bandwidth is through the use of chirp or composite pulses. However, performance can be limited by cavity or detection bandwidth, which in commercial systems is typically 100-200MHz. Here we demonstrate in a 94GHz spectrometer, with >800MHz system bandwidth, an increase in signal and modulation depth in a 4-pulse DEER experiment through use of composite rather than rectangular π pulses. We show that this leads to an increase in sensitivity by a factor of 3, in line with theoretical predictions, although gains are more limited in nitroxide-nitroxide DEER measurements.

Broadband W-band Rapid Frequency Sweep Considerations for Fourier Transform EPR.

A multi-arm W-band (94 GHz) electron paramagnetic resonance spectrometer that incorporates a loop-gap resonator with high bandwidth is described. A goal of the instrumental development is detection of free induction decay following rapid sweep of the microwave frequency across the spectrum of a nitroxide radical at physiological temperature, which is expected to lead to a capability for Fourier transform electron paramagnetic resonance. Progress toward this goal is a theme of the paper. Because of the low Q-value of the loop-gap resonator, it was found necessary to develop a new type of automatic frequency control, which is described in an appendix. Path-length equalization, which is accomplished at the intermediate frequency of 59 GHz, is analyzed. A directional coupler is favored for separation of incident and reflected power between the bridge and the loop-gap resonator. Microwave leakage of this coupler is analyzed. An oversize waveguide with hyperbolic-cosine tapers couples the bridge to the loop-gap resonator, which results in reduced microwave power and signal loss. Benchmark sensitivity data are provided. The most extensive application of the instrument to date has been the measurement of T1 values using pulse saturation recovery. An overview of that work is provided.

High-frequency pulsed ENDOR spectroscopy of the NV(-) centre in the commercial HPHT diamond.

This work reports direct 94GHz ENDOR spectroscopy of the (14)N nuclei in the NV(-) centre in single-crystal diamond. Roadmaps of ENDOR frequencies were measured and hyperfine/quadrupole interaction parameters were obtained, with AX,Y=-2.7MHz, AZ=-2.2MHz and P=-4.8MHz. The sign and value of each parameter was calculated using spin Hamiltonian matrix diagonalization, first and second order perturbation theory and confirmed experimentally. Magnetic field magnitude was measured by (13)C ENDOR signal with 0.02% precision or 0.5mT. The orientation of quadrupole, hyperfine and fine structure tensors are the same within error of experiment, g-factor is isotropic.

Zero field splitting fluctuations induced phase relaxation of Gd3+ in frozen solutions at cryogenic temperatures.

Distance measurements using double electron-electron resonance (DEER) and Gd(3+) chelates for spin labels (GdSL) have been shown to be an attractive alternative to nitroxide spin labels at W-band (95GHz). The maximal distance that can be accessed by DEER measurements and the sensitivity of such measurements strongly depends on the phase relaxation of Gd(3+) chelates in frozen, glassy solutions. In this work, we explore the phase relaxation of Gd(3+)-DOTA as a representative of GdSL in temperature and concentration ranges typically used for W-band DEER measurements. We observed that in addition to the usual mechanisms of phase relaxation known for nitroxide based spin labels, GdSL are subjected to an additional phase relaxation mechanism that features an increase in the relaxation rate from the center to the periphery of the EPR spectrum. Since the EPR spectrum of GdSL is the sum of subspectra of the individual EPR transitions, we attribute this field dependence to transition dependent phase relaxation. Using simulations of the EPR spectra and its decomposition into the individual transition subspectra, we isolated the phase relaxation of each transition and found that its rate increases with |ms|. We suggest that this mechanism is due to transient zero field splitting (tZFS), where its magnitude and correlation time are scaled down and distributed as compared with similar situations in liquids. This tZFS induced phase relaxation mechanism becomes dominant (or at least significant) when all other well-known phase relaxation mechanisms, such as spectral diffusion caused by nuclear spin diffusion, instantaneous and electron spin spectral diffusion, are significantly suppressed by matrix deuteration and low concentration, and when the temperature is sufficiently low to disable spin lattice interaction as a source of phase relaxation.

Insights into copper coordination in the EcoRI-DNA complex by ESR spectroscopy.

The EcoRI restriction endonuclease requires one divalent metal ion in each of two symmetrical and identical catalytic sites to catalyse double-strand DNA cleavage. Recently, we showed that Cu2+ binds outside the catalytic sites to a pair of new sites at H114 in each sub-unit, and inhibits Mg2+ -catalysed DNA cleavage. In order to provide more detailed structural information on this new metal ion binding site, we performed W-band (~94 GHz) and X-band (~9.5 GHz) electron spin resonance spectroscopic measurements on the EcoRI-DNA-(Cu2+ )2 complex. Cu2+ binding results in two distinct components with different gzz and Azz values. X-band electron spin echo envelope modulation results indicate that both components arise from a Cu2+ coordinated to histidine. This observation is further confirmed by the hyperfine sub-level correlation results. W-band electron nuclear double resonance spectra provide evidence for equatorial coordination of water molecules to the Cu2+ ions.

Identification of Fe3+-Li+ complexes in ZnO by means of high-frequency EPR/ENDOR spectroscopy.

Theoretical prediction of a high Curie temperature in ZnO doped with Mn, Fe, and other transition metals has stimulated the investigation of these materials by many research groups. Although charge-compensated Fe(3+) centers in ZnO:Fe have been observed by means of EPR and have been known for decades, conclusions on the chemical nature of these defects are still contradictory. Originally, these centers were treated as Fe(3+)-Li(+) complexes with both ions occupying adjacent cationic sites. Recently, however, the centers were interpreted as a substitutional Fe(3+) ion with a vacancy at an adjacent zinc or oxygen site (Fe-VZn or Fe-VO). In order to determine the chemical nature of the impurity associated with Fe(3+), electron-nuclear double resonance (ENDOR) spectroscopy was used. ENDOR measurements reveal NMR transitions corresponding to nuclei with g-factor gN=2.171 and spin I=3/2. This unambiguously shows presence of Li as a charge compensator and also resolves contradictions with the theoretical prediction of the Fe-VO formation energy. The electric field gradients at the (7)Li nuclei (within the Fe(3+)-Li(+) complexes) were estimated to be significantly lower than the gradient at undistorted Zn sites.

Increasing sensitivity of pulse EPR experiments using echo train detection schemes.

Modern pulse EPR experiments are routinely used to study the structural features of paramagnetic centers. They are usually performed at low temperatures, where relaxation times are long and polarization is high, to achieve a sufficient Signal/Noise Ratio (SNR). However, when working with samples whose amount and/or concentration are limited, sensitivity becomes an issue and therefore measurements may require a significant accumulation time, up to 12h or more. As the detection scheme of practically all pulse EPR sequences is based on the integration of a spin echo--either primary, stimulated or refocused--a considerable increase in SNR can be obtained by replacing the single echo detection scheme by a train of echoes. All these echoes, generated by Carr-Purcell type sequences, are integrated and summed together to improve the SNR. This scheme is commonly used in NMR and here we demonstrate its applicability to a number of frequently used pulse EPR experiments: Echo-Detected EPR, Davies and Mims ENDOR (Electron-Nuclear Double Resonance), DEER (Electron-Electron Double Resonance|) and EDNMR (Electron-Electron Double Resonance (ELDOR)-Detected NMR), which were combined with a Carr-Purcell-Meiboom-Gill (CPMG) type detection scheme at W-band. By collecting the transient signal and integrating a number of refocused echoes, this detection scheme yielded a 1.6-5 folds SNR improvement, depending on the paramagnetic center and the pulse sequence applied. This improvement is achieved while keeping the experimental time constant and it does not introduce signal distortion.