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Chemodivergent mechanosynthesis of cyclopentenyl and pyrrolinyl spirobarbiturates from unsaturated barbiturates and enamino esters.
Li, Ming-Jun; Lu, Ming-Ming; Xu, Peng; Chen, Si-Qi; Wu, Luan-Ting; Zhang, Ze; Xu, Hui.
Afiliação
  • Li MJ; School of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu 241000, P. R. China. zhangze@ustc.edu.cn.
  • Lu MM; School of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu 241000, P. R. China. zhangze@ustc.edu.cn.
  • Xu P; School of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu 241000, P. R. China. zhangze@ustc.edu.cn.
  • Chen SQ; School of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu 241000, P. R. China. zhangze@ustc.edu.cn.
  • Wu LT; School of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu 241000, P. R. China. zhangze@ustc.edu.cn.
  • Zhang Z; School of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu 241000, P. R. China. zhangze@ustc.edu.cn.
  • Xu H; School of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu 241000, P. R. China. zhangze@ustc.edu.cn.
Chem Commun (Camb) ; 60(29): 3958-3961, 2024 Apr 04.
Article em En | MEDLINE | ID: mdl-38501223
ABSTRACT
A novel and interesting controllable spirocyclization of unsaturated barbiturates with enamino esters for the assembly of cyclopentenyl and pyrrolinyl spirobarbiturates has been developed under ball-milling conditions. The present protocol features high chemoselectivity and efficiency, excellent functional group tolerance and mild reaction conditions.
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article