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EMM-Promoted Pd-Catalyzed Solid State Intramolecular Heck-Type Cyclization/Boronation and Suzuki Couplings: Access to Functionalized Indolines.
Jia, Yuwei; Wang, Hui; Guo, Jintao; Zhang, Feng; Zhang, Lizhi; Li, Xinjin; Zhao, Yan; Bao, Xingliang; Liu, Qing; Li, Xiaowei; Liu, Hui.
Afiliação
  • Jia Y; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
  • Wang H; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
  • Guo J; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
  • Zhang F; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
  • Zhang L; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
  • Li X; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
  • Zhao Y; Clinical Laboratory of Zibo Central Hospital, Zibo 255020, People's Republic of China.
  • Bao X; Zibo New Materials Trading Center Zhangdian District, Zibo Tengyu Chemical Engineering Company, Ltd., Zibo 255020, People's Republic of China.
  • Liu Q; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
  • Li X; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
  • Liu H; School of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, People's Republic of China.
J Org Chem ; 89(10): 6704-6713, 2024 May 17.
Article em En | MEDLINE | ID: mdl-38709904
ABSTRACT
EMM (electromagnetic mill)-promoted Pd-catalyzed solid state intramolecular Heck-type cyclization/boronation and Suzuki couplings are reported. Compared to previous mechanochemistry that constructed one chemical bond through a cross-coupling reaction, this strategy realizes cascade transformation along with multiple chemical bond formation. This conversion does not require organic solvents or additional heating, and it shows a good substrate scope and high functional group tolerance.
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article
Texto completo
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PubMed Links
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article