Quality analysis of Da,Xiao-Chengqi Decoction produced in Taiwan / 中成药
Chinese Traditional Patent Medicine
; (12)1992.
Article
в Zh
| WPRIM
| ID: wpr-579482
Ответственная библиотека:
WPRO
ABSTRACT
AIM:
To establish a HPLC method for determing naringin,rhein,emodin,chrysophanol,honokiol and magnolol in Da,Xiao-Chengqi Decoction bought from Taiwan.METHODS:
The seperation was performed on Licrospher C_(18) column(150 mm?4.6 mm,5 ?m) with acetonitrile-0.5% HAc(gradient elution) as mobile phase and the detection wavelength was set at 270 nm.RESULTS:
In the eight samples measured the content of naringin was from 0.54 to 44.20 mg/g;rhein from 0.51 and 2.10 mg/g;honokiol from 0.44 to 6.65 mg/g;emodin from 0.02 to 0.23 mg/g;magnolol from 1.09 to 2.29 mg/g,chrysophanol from 0.09 to 2.70 mg/g.However,honokiol and magnolol were not detected in some samples.CONCLUSION:
This established method is fully validated with respect to linearity,precision,reproducibility and accuracy and successfully applied to quantifying the six constituents in eight commercial samples.The overall results demonstrate that this proposed method is simple,reliable,and suitable for the quality control of Da,Xiao-Chengqi Decoction.
Полный текст:
1
База данных:
WPRIM
Язык:
Zh
Журнал:
Chinese Traditional Patent Medicine
Год:
1992
Тип:
Article