Recovery of a highly reflective Bragg grating in DPDS-doped polymer optical fiber by thermal annealing.

We report fiber Bragg grating manufacturing in poly(methyl methacrylate) (PMMA)-based polymer optical fibers (POFs) with a diphenyl disulfide (DPDS)-doped core by means of a 266 nm pulsed laser and the phase mask technique. Gratings were inscribed with different pulse energies ranging from 2.2 mJ to 2.7 mJ. For the latter, the grating reflectivity reached 91% upon 18-pulse illumination. Though the as-fabricated gratings decayed, they were recovered by post-annealing at 80°C for 1 day, after which they showed an even higher reflectivity of up to 98%. This methodology for the fabrication of highly reflective gratings could be applied for the production of high-quality tilted fiber Bragg gratings (TFBGs) in POFs for biochemical applications.

PCF based modal interferometer for lead ion detection.

A compact, reliable, and fast responsive PCF (photonic crystal fiber) based modal interferometric sensor for lead ion detection is proposed and experimentally demonstrated. The sensor has been fabricated by splicing a small section of PCF with SMF (single mode fiber) followed by collapsing the air holes of PCF at its tip. The interferometer is dip coated with chitosan-PVA (polyvinyl alcohol) and glutathione functionalized gold nanoparticles. Three probes have been fabricated, and the maximum sensitivity has been found to be 0.031 nm/ppb for lead ions whereas the detection range has been considered from 0 ppb to 50 ppb. The probe has been found to have a faster response time of ∼ 10 s. Furthermore, the sensor has been found to be less responsive towards other heavy metal ions, thereby demonstrating its selectivity towards lead ions. Besides, a section of FBG (fiber Bragg grating) has been embedded into the interferometer and the temperature response of FBG peak along with interference spectra has been investigated for better accuracy.

Femtosecond laser point-by-point Bragg grating inscription in BDK-doped step-index PMMA optical fibers.

In this paper, the inscription of 2-mm-long fiber Bragg gratings (FBGs) on benzyl dimethyl ketal (BDK)-doped poly(methyl methacrylate) (PMMA) optical fibers by means of a femtosecond laser and a point-by-point FBG inscription technique is reported. The highest reflectivity of approximately 99% is obtained with a pulse energy of 68.5 nJ, showing a large refractive index modulation amplitude of 7.2 × 10-4. Afterwards, grating stabilities at room and higher temperatures of up to 80°C are investigated.

Femtosecond laser point-by-point Bragg grating inscription in BDK-doped step-index PMMA optical fibers: erratum.

An erratum is presented to correct the laser pulse energy applied on the fiber during grating fabrication in Opt. Lett.47(2), 249 (2022)10.1364/OL.450047.

Random forest assisted vector displacement sensor based on a multicore fiber.

We proposed a two-dimensional vector displacement sensor with the capability of distinguishing the direction and amplitude of the displacement simultaneously, with improved performance assisted by random forest, a powerful machine learning algorithm. The sensor was designed based on a seven-core multi-core fiber inscribed with Bragg gratings, with a displacement direction range of 0-360° and the amplitude range related to the length of the sensor body. The displacement information was obtained under a random circumstance, where the performances with theoretical model and random forest model were studied. With the theoretical model, the sensor performed well over a shorter linear range (from 0 to 9 mm). Whereas the sensor assisted with random forest algorithm exhibits better performance in two aspects, a wider measurement range (from 0 to 45 mm) and a reduced measurement error of displacement. Mean absolute errors of direction and amplitude reconstruction were decreased by 60% and 98%, respectively. The proposed displacement sensor shows the possibility of machine learning methods to be applied in point-based optical systems for multi-parameter sensing.

Pattern recognition in distributed fiber-optic acoustic sensor using an intensity and phase stacked convolutional neural network with data augmentation.

Distributed acoustic sensors (DASs) have the capability of registering faint vibrations with high spatial resolution along the sensing fiber. Advanced algorithms are important for DAS in many applications since they can help extract and classify the unique signatures of different types of vibration events. Deep convolutional neural networks (CNNs), which have powerful spectro-temporal feature learning capability, are well suited for event classification in DAS. Generally, these data-driven methods are highly dependent on the availability of large quantities of training data for learning a mapping from input to output. In this work, to fully utilize the collected information and maximize the power of CNNs, we propose a method to enlarge the useful dataset for CNNs from two aspects. First, we propose an intensity and phase stacked CNN (IP-CNN) to utilize both the intensity and phase information from a DAS with coherent detection. Second, we propose to use data augmentation to further increase the training dataset size. The influence of different data augmentation methods on the performance of the proposed CNN architecture is thoroughly investigated. The experimental results show that the proposed IP-CNN with data augmentation produces a classification accuracy of 88.2% on our DAS dataset with 1km sensing length. This indicates that the usage of both intensity and phase information together with the enlarged training dataset after data augmentation can greatly improve the classification accuracy, which is useful for DAS pattern recognition in real applications.

Low gas pressure sensor based on a polymer optical fiber grating.

A fiber Bragg grating (FBG) inscribed Zeonex-based novel, to the best of our knowledge, side hole polymer optical fiber (SHPOF) is proposed and demonstrated for low gas pressure measurement above and below the atmospheric pressure. Two different grades of Zeonex have been used to fabricate the core and cladding of this fiber, thereby making it dopant free. The side hole introduced in the cladding is parallel to the fiber core. A few ultrashort pulses with nanosecond duration have been used to write the FBG in the core of this fiber. The incorporation of the side hole leads to enhancement of pressure sensitivity as well as low hysteresis and performance repeatability compared to Zeonex-based conventional polymer optical fiber (CPOF). Above the atmospheric pressure, the proposed probe shows a pressure sensitivity of 0.47 pm/kPa, which is 80% more compared to the Zeonex-based CPOF and 0.48 pm/kPa for regime below atmospheric pressure. The sensor has a resolution of 2.12 kPa and exhibited very low hysteresis.

Large refractive index modulation based on a BDK-doped step-index PMMA optical fiber for highly reflective Bragg grating inscription.

We experimentally report high reflectivity on the poly(methyl methacrylate) (PMMA)-based polymer optical fiber Bragg gratings by means of a 266 nm pulsed laser and phase mask technique. In the first recipe, fiber Bragg gratings (FBGs) were manufactured with a single pulse up to 3.7 mJ. After post-annealing, a stable refractive index change up to 4.2×10-4 was obtained. In the second recipe, FBGs were inscribed by 22 pulses with a lower pulse energy of 1.4 mJ, showing a stable refractive index change of 6.2×10-4. Both behaviors may mainly be attributed to the movement of initiating radicals arising from benzyl dimethyl ketal (BDK) under UV irradiation. The high refractive index change in step-index fibers paves the way to tilted FBG manufacturing with large tilt angles potentially for biomedical applications.

Two semicircular-hole fiber in a Sagnac loop for simultaneous discrimination of torsion, strain and temperature.

We report a highly sensitive twist sensor based on a Sagnac interferometer constructed with a new type of optical fiber which contains an elliptical core and two large semicircular-holes, where the slow axis of the core orthogonal to the air-holes has a large sensitivity towards twist-induced birefringent changes. The novel fiber structure results in a highest twist sensitivity of 5.01 nm/° at a chosen dip over the range from 370°-400°. The resonance dips in the interference pattern respond with different rates in the wavelength shifts in the presence of physical parameters permitting to experimentally distinguish directional torsion, axial strain and temperature.

Hydrogel based Fabry-Pérot cavity for a pH sensor.

A simple, reliable, and quick reactive Fabry-Pérot (FP) structure-based fiber optic pH sensor is presented. The pH-sensitive hydrogel and single-mode fiber (SMF) are placed inside a fused silica capillary to form the FP cavity. The gel thickness is characterized by the spin coating method with respect to different spin speeds. The proposed sensor shows a pH sensitivity of 0.30 nm/pH along with a fast response time of 15 s to 20 s for different pH solvents in the acidic range. Also, the temperature sensitivity of the FPI sensor is found to be -0.56 nm/°C.

Sensitive Mach-Zehnder interferometric sensor based on a grapefruit microstructured fiber by lateral offset splicing.

A novel inline Mach-Zehnder interferometric (MZI) sensor based on a homemade grapefruit microstructured fiber (GMF) was proposed and experimentally demonstrated. The sensing unit consists of a short segment of a GMF sandwiched between two single mode fibers using lateral offset splicing. The fabrication of the GMF and the GMF-based MZI sensor was introduced. Mode analysis of the GMF and theoretical simulation of the proposed MZI sensor were investigated and matched well with experimental results. The sensing performance of the MZI sensor for temperature and strain was tested. The strain and temperature sensitivity are 1.97pm/µÉ› and 37pm/°C, respectively. The compact size, low cost and high sensitivity makes the MZI sensor a good candidate for sensing application.

Single nanosecond-pulse production of polymeric fiber Bragg gratings for biomedical applications.

In this study, we present first-time fabrication of FBGs in all ZEONEX-based SMPOFs with a single 25 ns pulse of 248 nm UV irradiation over a 12-month period, which opens up new frontiers in optics and photonics for the effective fabrication of polymer optical fiber Bragg gratings (POFBGs), permitting mass producibility of them. POFBGs were characterized by subjecting them to various physical parameters including temperature and tensile strain. Strain responses of FBGs with similar grating strengths fabricated with 248 nm and 325 nm He-Cd laser irradiations were explored over a year to demonstrate their long-term stability and applicability. Owing to the unique features of the proposed sensing device fabricated by embedding POFBGs in silicone rubber, a good performance in the detection of human heart rate with an amplitude of 4 pm, which is 4 times higher compared to that of silica single mode fiber (SMF) was demonstrated. The response of the sensing device during a human respiration process was also explored where exhalation and inhalation were monitored and distinguished while the breath was held. These revelations signify the importance of ZEONEX-based POFBGs, which allow consistent and effective grating fabrication and are highly promising in the foreseeable future for biomedical applications.

Resurgent regenerated fiber Bragg gratings and thermal annealing techniques for ultra-high temperature sensing beyond 1400°C.

We report for the first time the resurgence of regenerated fiber Bragg gratings (RFBGs) useful for ultra-high temperature measurements exceeding 1400 °C. A detailed study of the dynamics associated with grating regeneration in six-hole microstructured optical fibers (SHMOFs) and single mode fibers (SMFs) was conducted. Rapid heating and rapid cooling techniques appeared to have a significant impact on the thermal sustainability of the RFBGs in both types of optical fibers reaching temperature regimes exceeding 1400 °C. The presence of air holes sheds new light in understanding the thermal response of RFBGs and the stresses associated with them, which governs the variation in the Bragg wavelength.

Impact of high UV fluences on the mechanical and sensing properties of polymer optical fibers for high strain measurements.

PMMA-based fibers are widely studied for strain measurements and show repeatable results for Fiber Bragg Gratings (FBGs) inscribed using 325 nm laser and 248 nm laser. However, there is no available material mechanical behavior characterization of the UV source impact on the fiber properties. In this manuscript, fibers are irradiated with high fluence of 325 nm and 248 nm lasers and the fibers properties are investigated using dynamic mechanical analysis and tensile strain for potential use of these fibers past the yield point. It is demonstrated that the UV sources shifted the ultimate tensile strength and changed the strain hardening behavior. Tensile strain measurements show excellent repeatability for gratings inscribed with these two sources with similar sensitivity of 1.305 nm/mɛ for FBG inscribe with 325 nm laser, and 1.345 nm/mɛ for grating written with 248 nm laser in the range 0 to 1.5 % elongation. Furthermore, tests far beyond the yield point (up to 2.8 % elongation) show that grating inscribed with lower UV wavelength exhibit hysteresis. Finally, we demonstrate that 248 nm laser fluence shall be chosen carefully whereas even high 325 nm laser fluence do not critically impact the sensor properties.

All-optical fiber filter based on an FBG inscribed in a silica/silicone composite fiber.

An all-optical tunable filter based on a fiber Bragg grating (FBG) inscribed in a self-heated silica/silicone composite fiber is demonstrated. A thin silicone film is coated inside the suspended core fiber), which acts as the silicone cladding. A periodic refractive index modulation is inscribed in the silicone cladding by UV irradiation. Silicone is an organic material whose optical properties are different than silica, which leads to interesting applications. The high thermo-optic properties are studied and applied here. A 1550 nm pump laser is utilized to heat the silicone grating where a wavelength shift is observed for the gratings when subjected to different pump powers. Experimental results indicate a wavelength tuning coefficient of -0.128nm/mW with a response time of 0.5 s to obtain a wavelength shift of 1 nm under periodic pump light. The new design of this miniature all-optical filter is cost-effective and can potentially be adhered in optical fiber sensing and communication systems.

Simultaneous measurement of temperature and strain based on a hollow core Bragg fiber.

A novel, to the best of our knowledge, reflective sensor fabricated by simply sandwiching a homemade hollow core Bragg fiber (HCBF) between two single-mode fibers is proposed and demonstrated for the simultaneous measurement of the temperature and the strain. Different from traditional Fabry-Perot interferometer (FPI) sensors that can achieve only one-parameter sensing with inevitable cross-correspondence to other parameters, the proposed sensor based on the HCBF, which functions as an FPI-inducing FPI spectrum pattern and a weak waveguide confining light-inducing periodic envelope in reflection spectrum, ensures double-parameter sensing. For the HCBF-based reflective sensor, different sensing mechanisms lead to the various sensitivity values of temperature and strain (2.98 pm/°C, 19.4 pm/°C, 2.02 pm/µÎµ, -0.36pm/µÎµ), resulting in a different shift of the confining spectrum envelope and the FPI spectrum fringe. Experimental results indicate that our proposed sensor can measure temperature and strain simultaneously by utilizing a 2×2 matrix. Taking advantage of the compact size, easy fabrication, and low cost, this sensor has an applicable value in harsh environment for simultaneous strain and temperature sensing.

Ultracompact optical fiber acoustic sensors based on a fiber-top spirally-suspended optomechanical microresonator.

Acoustic wave sensors with a high sensitivity and small size are highly desired for a wide variety of important and emerging applications such as photoacoustic gas sensing and bio-imaging. Here we present an ultracompact optical fiber acoustic sensor based on an optomechanical resonator that is directly in situ printed on the end face of a standard single-mode optical fiber by using an optical 3D µ-printing technology. The fiber-top optomechanical microresonator is composed of a microscale suspended polymer micro-disk that forms a Fabry-Perot interferometric cavity, together with the optical fiber end face, and acts as the acoustic wave-sensitive micromechanical resonator simultaneously. The microbeams for suspending the micro-disk are devised with a spiral structure to overcome the small-size imposed low deflection amplitude so as to improve its sensitivity to acoustic waves. The sensor with a high sensitivity of 118.3 mV/Pa and low noise equivalent acoustic signal level of 0.328µPa/Hz1/2 at audio frequency is experimentally demonstrated. Moreover, with a resonance amplification mechanism, the sensitivity can be enhanced by 40.1 times when the frequency of the acoustic wave matches with the natural resonance frequency of the optomechanical resonator. Such an ultrasmall fiber-tip acoustic sensor has not only a miniaturization-induced broad bandwidth, but also a structure-enhanced ultrahigh sensitivity and thus is very promising in various acoustic wave-based sensing, imaging, and testing applications.

Silicone Rubber Based Highly Sensitive Fiber-Optic Fabry-Perot Interferometric Gas Pressure Sensor.

A simple, compact, and highly sensitive gas pressure sensor based on a Fabry-Perot interferometer (FPI) with a silicone rubber (SR) diaphragm is demonstrated. The SR diaphragm is fabricated on the tip of a silica tube using capillary action followed by spin coating. This process ensures uniformity of its inner surface along with reproducibility. A segment of single mode fiber (SMF) inserted into this tube forms the FPI which produces an interference pattern with good contrast. The sensor exhibits a high gas pressure sensitivity of -0.68 nm/kPa along with a low temperature cross-sensitivity of ≈ 1.1 kPa/°C.

Two-dimensional vector accelerometer based on Bragg gratings inscribed in a multi-core fiber.

We propose and demonstrate a novel orientation-sensitive two-dimensional accelerometer based on fiber Bragg gratings inscribed in a multi-core fiber. Through monitoring of the wavelength shifts of three of the seven cores, including the central core and two outer cores which are not aligned in a straight line, information on vibration orientation as well as acceleration can be obtained simultaneously. Performance of the proposed accelerometer in terms of frequency, acceleration and vibration orientation are experimentally investigated. The designed two-dimensional accelerometer is capable of obtaining all these three parameters simultaneously. A sensitivity which is strongly dependent on the orientation is achieved, with a best orientation accuracy of 0.127° over a range of 0-180°. Moreover, the resonance frequency and the sensitivity can be optimized through adjusting the length and weight of the free-fiber. The ease of fabrication as well as the versatility of the proposed sensor makes it potentially useful in dynamic monitoring for industrial applications.

Single-ring suspended fiber for Bragg grating based hydrostatic pressure sensing.

We present a novel optical fiber composed of a suspended core, a supporting ring and an outer ring. To establish a large holey region, a germanium-doped core is suspended by a silica ring and the entire structure is enclosed by another silica ring. By monitoring the Bragg wavelength shift of an FBG written in such a fiber with an air filling fraction of 65%, a hydrostatic pressure sensitivity of -43.6 pm/MPa was achieved experimentally. The high-pressure sensitivity is in good agreement with the numerically calculated value of ~40 pm/MPa. Due to the significant impact of the fiber core suspended in the large holey region inside the fiber, the pressure sensitivity improved by approximately eleven times compared to a Bragg grating inscribed in a standard single-mode fiber. To the best of our knowledge, it is the highest pressure sensitivity obtained for a FBG-based sensor experimentally, when compared to other FBG-based pressure sensors reported up to date. The large air hole region and the suspended core in the center of the fiber not only make the proposed fiber sensor a good candidate for pressure measurements, especially in the oil industry where space is at a premium, but also allow the detection of substances, by exploiting interaction of light with liquids or gases.