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Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3'-Dibromo-1,1'-bi-2-naphthol as a Chiral Solvating Agent.
Du, Guoxin; Li, Yisu; Ma, Shunan; Wang, Rui; Li, Bo; Guo, Fujiang; Zhu, Weiliang; Li, Yiming.
Afiliación
  • Du G; School of Pharmacy, Shanghai University of Traditional Chinese Medicine , 1200 Cailun Road, Shanghai, 201203, People's Republic of China.
  • Li Y; CAS Key Laboratory of Receptor Research, Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zuchongzhi Road, Shanghai, 201203, People's Republic of China.
  • Ma S; CAS Key Laboratory of Receptor Research, Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zuchongzhi Road, Shanghai, 201203, People's Republic of China.
  • Wang R; Nano Science and Technology Institute, University of Science and Technology of China , 166 Renai Road, Suzhou, 215123, People's Republic of China.
  • Li B; School of Pharmacy, Shanghai University of Traditional Chinese Medicine , 1200 Cailun Road, Shanghai, 201203, People's Republic of China.
  • Guo F; School of Pharmacy, Shanghai University of Traditional Chinese Medicine , 1200 Cailun Road, Shanghai, 201203, People's Republic of China.
  • Zhu W; CAS Key Laboratory of Receptor Research, Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zuchongzhi Road, Shanghai, 201203, People's Republic of China.
  • Li Y; School of Pharmacy, Shanghai University of Traditional Chinese Medicine , 1200 Cailun Road, Shanghai, 201203, People's Republic of China.
J Nat Prod ; 78(12): 2968-74, 2015 Dec 24.
Article en En | MEDLINE | ID: mdl-26641704
ABSTRACT
The enantiomeric purity and absolute configuration of flavanones were first determined using (S)-3,3'-dibromo-1,1'-bi-2-naphthol as a chiral solvating agent by means of (1)H NMR spectroscopy. The enantiomeric purity results closely matched those based on chiral HPLC analysis.
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Texto completo: 1 Banco de datos: MEDLINE Asunto principal: Flavanonas / Naftoles Idioma: En Año: 2015 Tipo del documento: Article
Texto completo
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Texto completo: 1 Banco de datos: MEDLINE Asunto principal: Flavanonas / Naftoles Idioma: En Año: 2015 Tipo del documento: Article