Your browser doesn't support javascript.
loading
Mostrar: 20 | 50 | 100
Resultados 1 - 1 de 1
Filtrar
Más filtros

Bases de datos
Tipo del documento
País de afiliación
Intervalo de año de publicación
1.
J Sep Sci ; 41(2): 590-601, 2018 Jan.
Artículo en Inglés | MEDLINE | ID: mdl-29095569

RESUMEN

Molecularly imprinted polymers were prepared using the molecular structure analogs of sanshool as template molecule, 2-vinylpyridine and ß-cyclodextrin as double functional monomers, ethylene dimethacrylate as cross linker, and azobisisobutyronitrile as initiator. The structural characteristics of the polymers were determined by Fourier-transform infrared spectroscopy and scanning electron microscopy. Dynamic adsorption and isothermal adsorption were also investigated. The molecularly imprinted polymers were used to prepare a molecularly imprinted solid-phase extraction column in order to separate acid amide components from pepper oil resin derived from Chinese prickly ash (Zanthoxylum bungeanum). After eluting, the percentage of acid amide components was enhanced to 92.40 ± 1.41% compared with 23.34 ± 1.21% in the initial pepper oil resin, indicating good properties of purification of molecularly imprinted polymers and potential industrial application.


Asunto(s)
Amidas/análisis , Impresión Molecular , Polímeros/análisis , Zanthoxylum/química , Ácidos/química , Adsorción , Amidas/síntesis química , Cromatografía Líquida de Alta Presión , Reactivos de Enlaces Cruzados , Cromatografía de Gases y Espectrometría de Masas , Microscopía Electrónica de Rastreo , Estructura Molecular , Aceites de Plantas/química , Extracción en Fase Sólida , Espectroscopía Infrarroja por Transformada de Fourier , beta-Ciclodextrinas/análisis
SELECCIÓN DE REFERENCIAS
DETALLE DE LA BÚSQUEDA