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Sci Rep ; 10(1): 17815, 2020 10 20.
Artículo en Inglés | MEDLINE | ID: mdl-33082402

RESUMEN

The present study explores the methodology for the synthesis of bio-oil from waste trichosanthes cucumerina seeds by the solvent extraction method. It investigates the yield percentage, concentration of free fatty acids and acid contents in the extracted bio-oil. Effects of size of the crushed seeds, moisture content, extraction time, solvent to seed ratio and extraction temperatures were examined. The non-polar hexane solvent resulted in a higher percentage of oil yield (28.4 ± 0.4%) for the crushed seed size of 0.21 mm, 6% moisture content, 270 min extraction time, 68 °C temperature and 6:1(ml/g) of solvent to seed ratio. The synthesized bio-oil was characterized using Fourier Transform Infra-Red spectrum and Gas Chromatography-Mass Spectroscopy analysis. The properties of the bio-oil and biodiesel were assessed according to the American Society for Testing and Materials and the Association of Official Analytical Chemists standards. The obtained methyl-ester by trans-esterification process results in the fuel properties closer to the conventional fuel. Thus, Trichosanthes cucumerina bio-diesel can be used as a potential substitute.


Asunto(s)
Aceites de Plantas/síntesis química , Polifenoles/síntesis química , Energía Renovable , Trichosanthes/fisiología , Biocombustibles , Catálisis , Esterificación , Cromatografía de Gases y Espectrometría de Masas , Gasolina , Semillas , Espectroscopía Infrarroja por Transformada de Fourier
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