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Ultrason Sonochem ; 20(1): 202-8, 2013 Jan.
Artículo en Inglés | MEDLINE | ID: mdl-22964031

RESUMEN

The effectiveness of ultrasonic-assisted extraction (UAE) of pomegranate seed oil (PSO) was evaluated using a variety of solvents. Petroleum ether was the most effective for oil extraction, followed by n-hexane, ethyl acetate, diethyl ether, acetone, and isopropanol. Several variables, such as ultrasonic power, extraction temperature, extraction time, and the ratio of solvent volume and seed weight (S/S ratio) were studied for optimization using response surface methodology (RSM). The highest oil yield, 25.11% (w/w), was obtained using petroleum ether under optimal conditions for ultrasonic power, extraction temperature, extraction time, and S/S ratio at 140 W, 40 °C, 36 min, and 10 ml/g, respectively. The PSO yield extracted by UAE was significantly higher than by using Soxhlet extraction (SE; 20.50%) and supercriti cal fluid extraction (SFE; 15.72%). The fatty acid compositions were significantly different among the PSO extracted by Soxhlet extraction, SFE, and UAE, with punicic acid (>65%) being the most dominant using UAE.


Asunto(s)
Fraccionamiento Químico/métodos , Lythraceae/química , Aceites de Plantas/aislamiento & purificación , Semillas/química , Ultrasonido , Ácidos Grasos/análisis , Aceites de Plantas/química , Solventes/química , Temperatura , Factores de Tiempo
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