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1.
J Biol Chem ; 294(7): 2329-2339, 2019 02 15.
Artículo en Inglés | MEDLINE | ID: mdl-30602568

RESUMEN

Phospholipids are an integral part of the cellular membrane structure and can be produced by a de novo biosynthetic pathway and, alternatively, by the Kennedy pathway. Studies in several yeast species have shown that the phospholipid phosphatidylserine (PS) is synthesized from CDP-diacylglycerol and serine, a route that is different from its synthesis in mammalian cells, involving a base-exchange reaction from preexisting phospholipids. Fungal-specific PS synthesis has been shown to play an important role in fungal virulence and has been proposed as an attractive drug target. However, PS synthase, which catalyzes this reaction, has not been studied in the human fungal pathogen Cryptococcus neoformans Here, we identified and characterized the PS synthase homolog (Cn Cho1) in this fungus. Heterologous expression of Cn CHO1 in a Saccharomyces cerevisiae cho1Δ mutant rescued the mutant's growth defect in the absence of ethanolamine supplementation. Moreover, an Sc cho1Δ mutant expressing Cn CHO1 had PS synthase activity, confirming that the Cn CHO1 encodes PS synthase. We also found that PS synthase in C. neoformans is localized to the endoplasmic reticulum and that it is essential for mitochondrial function and cell viability. Of note, its deficiency could not be complemented by ethanolamine or choline supplementation for the synthesis of phosphatidylethanolamine (PE) or phosphatidylcholine (PC) via the Kennedy pathway. These findings improve our understanding of phospholipid synthesis in a pathogenic fungus and indicate that PS synthase may be a useful target for antifungal drugs.


Asunto(s)
Cryptococcus neoformans/metabolismo , Retículo Endoplásmico/metabolismo , Viabilidad Microbiana , Fosfatidilserinas/biosíntesis , Animales , CDPdiacilglicerol-Serina O-Fosfatidiltransferasa/genética , CDPdiacilglicerol-Serina O-Fosfatidiltransferasa/metabolismo , Cryptococcus neoformans/genética , Citidina Difosfato Diglicéridos/genética , Citidina Difosfato Diglicéridos/metabolismo , Retículo Endoplásmico/genética , Proteínas Fúngicas/genética , Proteínas Fúngicas/metabolismo , Humanos , Fosfatidilserinas/genética , Saccharomyces cerevisiae/genética , Saccharomyces cerevisiae/metabolismo
2.
Parasitol Int ; 62(3): 253-61, 2013 Jun.
Artículo en Inglés | MEDLINE | ID: mdl-23416156

RESUMEN

The aim of this study was to isolate and evaluate the withanolides in inducing apoptotic like death in Leishmania donovani in vitro. Withanolides were fractionated and isolated from the leaves of Withania somnifera and LC-MS/MS analysis of two fractions namely, F5 and F6 of ethanolic extracts, obtained through column chromatography with silica gel, was performed. The antileishmanial effect of withanolides on L. donovani promastigotes was assessed in vitro using PI dye exclusion test. The effect of withanolides on promastigote morphology was determined by scanning electron microscopy. To understand their mode of action against L. donovani, DNA fragmentation, quantification of parasites at sub G0/G1 phase, determination of phosphatidylserine externalization, measurement of reactive oxygen species (ROS) and mitochondrial membrane potential (Ψm) were done. Results showed that LC-MS/MS analysis confirmed the presence of withanolides in isolated fractions. Treatment with withanolides resulted in morphological alterations from spindle to round shape and loss of flagella/cell integrity in promastigotes. Moreover, it induced DNA nicks, cell cycle arrest at sub G0/G1 phase and externalization of phosphatidylserine in dose and time dependent manner via increase in ROS and decrease in Ψm. Results of this study indicate that withanolides induce apoptotic like death through the production of ROS from mitochondria and disruption of Ψm in promastigotes of L donovani.


Asunto(s)
Antiprotozoarios/farmacología , Apoptosis/efectos de los fármacos , Leishmania donovani/efectos de los fármacos , Withania/química , Witanólidos/farmacología , Antiprotozoarios/aislamiento & purificación , Puntos de Control del Ciclo Celular/efectos de los fármacos , Cromatografía Líquida de Alta Presión , Fragmentación del ADN/efectos de los fármacos , Relación Dosis-Respuesta a Droga , Concentración 50 Inhibidora , Leishmania donovani/citología , Leishmania donovani/genética , Potencial de la Membrana Mitocondrial/efectos de los fármacos , Microscopía Electrónica de Rastreo , Mitocondrias/efectos de los fármacos , Mitocondrias/genética , Mitocondrias/metabolismo , Fosfatidilserinas/genética , Fosfatidilserinas/metabolismo , Extractos Vegetales/aislamiento & purificación , Extractos Vegetales/farmacología , Especies Reactivas de Oxígeno/análisis , Especies Reactivas de Oxígeno/metabolismo , Espectrometría de Masas en Tándem , Witanólidos/aislamiento & purificación
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