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1.
Artigo em Inglês | MEDLINE | ID: mdl-25725211

RESUMO

The development of semiconductor materials made a considerable progress of catalytic technologies. In the present study, a simple and eco-friendly chemical direction for the synthesis of zinc oxide nanoparticles (ZnO NPs) using leaf extract of Moringa oleifera has been used. The prepared ZnO NPs were characterized various techniques such as UV-Vis absorption spectroscopy, X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), energy dispersive X-ray analysis (EDX), Fourier transform infrared spectroscopy (FT-IR) and photoluminescence spectroscopy (PL). XRD analysis revealed the wurtzite hexagonal structure of ZnO NPs. FT-IR confirmed the presence of functional groups of both leaf extract and ZnO NPs. The particles size, morphology and topography determined from FE-SEM. The intense and narrow width of zinc and oxygen have high purity and crystalline were identified using EDX. UV-Vis absorption showed the characteristic absorption peak of ZnO NPs. The results of antimicrobial activities revealed that maximum zones of inhibition was observed Gram (+ve) positive bacteria and followed by the Gram (-ve) negative bacteria and fungal at concentration of 200µg/mL of ZnO NPs.


Assuntos
Antibacterianos/química , Antifúngicos/química , Moringa oleifera/química , Extratos Vegetais/química , Óxido de Zinco/química , Antibacterianos/farmacologia , Antifúngicos/farmacologia , Nanopartículas Metálicas , Folhas de Planta/química , Óxido de Zinco/farmacologia
2.
Artigo em Inglês | MEDLINE | ID: mdl-25561298

RESUMO

Biologically synthesized nanoparticles have been widely used in the field of medicine. Especially, silver nanoparticles (Ag NPs) synthesized by the leaf extract lead the biological activity. In the present work, the synthesized Ag NPs by using the leaf extract of Croton sparsiflorus morong Ag NPs were characterized by using UV-Visible (UV-Vis) absorption spectroscopy, X-ray diffraction (XRD), Field Emission Scanning Electron Microscopy (FE-SEM) along with Energy Dispersive X-ray (EDX) Spectroscopy and Fourier Infrared (FT-IR) Spectroscopy, respectively. UV-Vis peak at 457 nm confirmed the Ag NPs due to the absorption. Cubic structural analysis and 16 nm particle size of the Ag NPs were calculated by using XRD analysis. The surface morphology along with the presence of Ag NPs was identified by using FE-SEM and EDX, respectively. The FT-IR study revealed with the functional groups of the Ag NPs. Finally, the present research has been explored to exhibit the significant antimicrobial activities.


Assuntos
Antibacterianos/farmacologia , Antifúngicos/farmacologia , Croton/química , Química Verde/métodos , Nanopartículas Metálicas/química , Extratos Vegetais/farmacologia , Folhas de Planta/química , Prata/farmacologia , Bactérias/efeitos dos fármacos , Fungos/efeitos dos fármacos , Nanopartículas Metálicas/ultraestrutura , Testes de Sensibilidade Microbiana , Tamanho da Partícula , Espectrometria por Raios X , Espectrofotometria Ultravioleta , Espectroscopia de Infravermelho com Transformada de Fourier , Difração de Raios X
3.
Spectrochim Acta A Mol Biomol Spectrosc ; 136 Pt B: 1052-7, 2015 02 05.
Artigo em Inglês | MEDLINE | ID: mdl-25459502

RESUMO

In the present investigation, we chose the very simple and eco-friendly chemical method for synthesis of zinc oxide nanoparticles from leaf extract of Tamarindus indica (L.) (T. indica) and developed the new green route for synthesis of nanoparticles. Formed product has been studied by UV-vis absorption spectroscopy, Photoluminescence (PL) spectroscopy, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), Field emission scanning electron microscopy (FE-SEM) and with corresponding energy dispersive X-ray analysis (EDX). Mainly, the present results depicted that the synthesized nanoproducts are moderately stable, hexagonal phase, roughly spherical with maximum particles in size range within 19-37 nm in diameter. The antibacterial and fungal activities of aqueous extracts of T. indica were ended with corresponding disk diffusion and Minimum Inhibitory Concentration (MIC). The highest mean zones of inhibition were observed in the ZnO NPs (200 µg/mL) against Staphylococcus aureus (13.1±0.28). Finally, it can be concluded that microbial activity of ZnO NPs has more susceptible S. aureus than the other micro organisms. Further, the present investigation suggests that ZnO NPs has the potential applications for various medical and industrial fields.


Assuntos
Antibacterianos/farmacologia , Antifúngicos/farmacologia , Química Verde/métodos , Nanopartículas/química , Fotossíntese , Tamarindus/química , Óxido de Zinco/química , Bactérias/efeitos dos fármacos , Fungos/efeitos dos fármacos , Humanos , Testes de Sensibilidade Microbiana , Nanopartículas/ultraestrutura , Tamanho da Partícula , Extratos Vegetais , Folhas de Planta/química , Espectrometria por Raios X , Espectrofotometria Ultravioleta , Espectroscopia de Infravermelho com Transformada de Fourier , Temperatura , Difração de Raios X
4.
Artigo em Inglês | MEDLINE | ID: mdl-24997264

RESUMO

Green synthesis of silver nanoparticles has been achieved using environmentally acceptable plant extract. It is observed that Abutilon indicum leaf extract can reduce silver ions into silver nanoparticles within 15 min of reaction time. The formation and stability of the reduced silver nanoparticles in the colloidal solution were monitored by UV-Vis spectrophotometer analysis. The mean particle diameter of silver nanoparticles was calculated from the XRD pattern. FT-IR spectra of the leaf extract after the development of nanoparticles are determined to allow identification of possible functional groups responsible for the conversion of metal ions to metal nanoparticles. The AgNPs thus obtained showed highly potent antibacterial activity toward Gram-positive (Staphyloccocus aureus and Bacillus subtilis) and Gram-negative (Salmonella typhi and Escherichia coli) microorganisms.


Assuntos
Antibacterianos/farmacologia , Química Verde/métodos , Malvaceae/química , Nanopartículas Metálicas/química , Extratos Vegetais/química , Prata/química , Antibacterianos/síntese química , Bacillus subtilis/efeitos dos fármacos , Bacillus subtilis/isolamento & purificação , Técnicas de Química Sintética , Escherichia coli/efeitos dos fármacos , Escherichia coli/isolamento & purificação , Humanos , Testes de Sensibilidade Microbiana , Microscopia Eletrônica de Varredura , Microscopia Eletrônica de Transmissão , Folhas de Planta/química , Salmonella typhi/efeitos dos fármacos , Salmonella typhi/isolamento & purificação , Espectroscopia de Infravermelho com Transformada de Fourier , Staphylococcus aureus/efeitos dos fármacos , Staphylococcus aureus/isolamento & purificação , Difração de Raios X
5.
Environ Sci Pollut Res Int ; 21(19): 11439-46, 2014 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-24906826

RESUMO

A novel green approach for the synthesis and stabilization of silver nanoparticles (AgNPs) using water extract of Leucas martinicensis leaf has been developed. As obtained, the nanoparticles are characterized by UV-visible (UV-Vis), transmission electron microscope (TEM), and X-ray diffraction (XRD). The crystalline nature of the AgNPs is confirmed by the prominent peaks in the XRD pattern. FTIR spectra suggest that the possible biomolecules are responsible for the efficient stabilization of the sample. The effects of leaf quantity on the biosynthesis of AgNPs are investigated by UV-Vis spectrophotometer. The synthesized AgNPs are observed to have a good catalytic activity on the reduction of methylene blue by L. martinicensis leaf. This is confirmed by the decrease in absorbance maximum values of methylene blue with respect to time through UV-Vis spectrophotometer. Moreover, the antibacterial activity of synthesized AgNPs against Staphylococcus aureus, Bacillus subtilis, Salmonella typhi, and Escherichia coli are screened.


Assuntos
Antibacterianos/biossíntese , Lamiaceae , Nanopartículas Metálicas , Extratos Vegetais/química , Prata/metabolismo , Antibacterianos/química , Antibacterianos/farmacologia , Bactérias/efeitos dos fármacos , Bactérias/crescimento & desenvolvimento , Catálise , Nanopartículas Metálicas/química , Nanopartículas Metálicas/ultraestrutura , Azul de Metileno/química , Microscopia Eletrônica de Transmissão , Folhas de Planta/química , Prata/química , Prata/farmacologia , Espectroscopia de Infravermelho com Transformada de Fourier , Difração de Raios X
6.
Spectrochim Acta A Mol Biomol Spectrosc ; 130: 116-21, 2014 Sep 15.
Artigo em Inglês | MEDLINE | ID: mdl-24769382

RESUMO

Silver nanoparticles have a significant role in the pharmaceutical science. Especially, silver nanoparticles synthesized by the plant extracts lead a significant role in biological activities such as antimicrobial, antioxidant and anticancer. Keeping this in mind, the present work investigation has been taken up with the synthesized silver nanoparticles using the plant extract of Melia dubia and it characterizes by using UV-visible, XRD and SEM-EDS. The effect of the silver nanoparticles on human breast cancer (KB) cell line has been tested. Silver nanoparticles showed remarkable cytotoxicity activity against KB cell line with evidence of high therapeutic index value are the results are discussed.


Assuntos
Antineoplásicos/química , Neoplasias da Mama/patologia , Melia/química , Nanopartículas Metálicas/química , Folhas de Planta/química , Prata/química , Animais , Linhagem Celular Tumoral/efeitos dos fármacos , Sobrevivência Celular , Chlorocebus aethiops , Feminino , Química Verde , Humanos , Células MCF-7 , Microscopia Eletrônica de Varredura , Extratos Vegetais/química , Espectrofotometria Ultravioleta , Espectroscopia de Infravermelho com Transformada de Fourier , Sais de Tetrazólio/química , Tiazóis/química , Células Vero , Difração de Raios X
7.
Artigo em Inglês | MEDLINE | ID: mdl-24231743

RESUMO

Biomediated silver nanoparticles were synthesized with the aid of an eco-friendly biomaterial, namely, aqueous Tribulus terrestris extract. Silver nanoparticles were synthesized using a rapid, single step, and completely green biosynthetic method employing aqueous T. terrestris leaf extracts as both the reducing and capping agent. Silver ions were rapidly reduced by aqueous T. terrestris leaf extracts, leading to the formation of highly crystalline silver nanoparticles. An attempt has been made and formation of the silver nanoparticles was verified by surface plasmon spectra using an UV-vis (Ultra violet), spectrophotometer. Morphology and crystalline structure of the prepared silver nanoparticles were characterized by TEM (Transmission Electron Microscope) and XRD (X-ray Diffraction), techniques, respectively. FT-IR (Fourier Transform Infrared), analysis suggests that the obtained silver nanoparticles might be stabilized through the interactions of carboxylic groups, carbonyl groups and the flavonoids present in the T. terrestris extract.


Assuntos
Nanopartículas Metálicas/química , Extratos Vegetais/química , Folhas de Planta/química , Prata/química , Tribulus/química , Catálise , Luminescência , Nanopartículas Metálicas/ultraestrutura , Azul de Metileno/química , Nitrato de Prata/farmacologia , Espectrofotometria Ultravioleta , Espectroscopia de Infravermelho com Transformada de Fourier , Difração de Raios X
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