[Determination of papaverine in Qiangli Pipalu by HPLC].
Zhongguo Zhong Yao Za Zhi
; 31(16): 1330-2, 2006 Aug.
Article
en Zh
| MEDLINE
| ID: mdl-17061552
ABSTRACT
OBJECTIVE:
To establish a method for the determination of the papaverine content in Qiangli Pibalu by HPLC.METHOD:
A C18 column with a solvent system of acetonitrile-0.02 mol x L(-1) sodium dihydrogen phosphate (0.2% triethylamine, phosphoric acid, at pH 3) (2575) and UV detection 240 nm were used. The flow rate was 1.0 mL x min(-1). The column temperature was maintained at 40 degrees C.RESULT:
There was a good linear relationship between the absorption value and the concentration in the range of 0.020 2-0.100 5 microg for papaverine. The average recovery rates were 99.1% (RSD 2.3%).CONCLUSION:
The method is simple, accurate and can be used to determine the contents in Qiangli Pibalu.
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Bases de datos:
MEDLINE
Medicinas Tradicionales:
Medicinas_tradicionales_de_asia
/
Medicina_china
Métodos Terapéuticos y Terapias MTCI:
Terapias_biologicas
Asunto principal:
Papaverina
/
Plantas Medicinales
/
Medicamentos Herbarios Chinos
Idioma:
Zh
Revista:
Zhongguo Zhong Yao Za Zhi
Año:
2006
Tipo del documento:
Article
País de afiliación:
China