RESUMEN
The present study focused on preparing and characterizing magnetite-polyvinyl alcohol (PVA) hybrid nanoparticles using Acanthophora spicifera marine algae extract as a reducing agent. Various analytical techniques, including UV-Visible spectrometry, Fourier-transform infrared (FTIR) analysis, energy-dispersive X-ray (EDX), scanning electron microscopy (SEM), and X-ray diffraction (XRD) analysis, were used to characterize the nanoparticles. The results showed the successful synthesis of nanoparticles with a characteristic color change and absorption peak at 400 nm in UV-Visible spectrometry. FTIR analysis indicated an interaction between the carboxyl group and magnetite-polyvinyl alcohol hybrid ions. SEM analysis revealed spherical nanoparticles with sizes ranging from 20 to 100 nm. EDX analysis confirmed the presence of strong magnetite peaks in Acanthophora spicifera, validating successful preparation. XRD analysis indicated the crystalline nature of the nanoparticles. Furthermore, the antimicrobial potential of As-PVA-MNPs was evaluated, demonstrating a significant zone of inhibition against tested bacterial and fungal samples at a concentration of 100 µg. These findings suggest the promising antimicrobial activity of the synthesized nanoparticles for potential applications in combating pathogenic microorganisms.
RESUMEN
In this study, a novel ecofriendly chitosan- silver nanoparticles hybrid was developed. Biological method using leaf extract of T. portulacifolium was used as reducing agent for its synthesis and the antibacterial efficiency of these hybrid nanoparticles were evaluated against the bacteria E. coli and S. marcescens organisms. The intense peak observed around 419â¯nm in the UV-Vis indicates the formation of silver nanoparticles. The XRD analysis showed that the hybrid chitosan-silver nanoparticles have a polycrystalline and face-centered cubic configuration. FTIR spectrum hybrid chitosan-silver nanoparticles indicated speaks vibration of NH and OH. The EDS analysis confirmed the presence of Ag, O, C and N elements in the prepared sample. The spherical shape was obtained from TEM analysis and it indicated that with average particles around 3.24â¯nm to 44.80â¯nm. The prepared hybrid chitosan-silver nanoparticles showed significant antibacterial activities against E. coli and S. marcescens. In addition, the surface membrane damages and surface morphology of test pathogens were visualized using FESEM analysis.