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1.
Bioorg Med Chem Lett ; 25(16): 3264-9, 2015 Aug 15.
Artículo en Inglés | MEDLINE | ID: mdl-26112443

RESUMEN

Despite recent approvals of anti-obesity drugs there is still a high therapeutic need for alternative options with higher efficacy in humans. As part of our MCH-R1 antagonist program for the treatment of obesity, a series of biphenylacetamide HTS hits was evaluated. Several issues of the initial lead structures had to be resolved, such as potency, selectivity over related GPCRs and P-gp efflux limiting brain exposure in this series. We could demonstrate that all parameters can be significantly improved by structural modifications resulting in BI 414 as a potent and orally available MCH-R1 antagonist tool compound with acceptable in vivo efficacy in an animal model of obesity.


Asunto(s)
Alquinos/síntesis química , Alquinos/farmacología , Fármacos Antiobesidad/síntesis química , Fármacos Antiobesidad/farmacología , Piridinas/síntesis química , Piridinas/farmacología , Receptores de Somatostatina/antagonistas & inhibidores , Miembro 1 de la Subfamilia B de Casetes de Unión a ATP/metabolismo , Animales , Peso Corporal/efectos de los fármacos , Citocromo P-450 CYP2D6/metabolismo , Inhibidores Enzimáticos del Citocromo P-450/síntesis química , Inhibidores Enzimáticos del Citocromo P-450/farmacología , Diseño de Fármacos , Ingestión de Alimentos/efectos de los fármacos , Ensayos Analíticos de Alto Rendimiento , Obesidad/tratamiento farmacológico , Ratas , Receptores Acoplados a Proteínas G/efectos de los fármacos , Receptores Acoplados a Proteínas G/metabolismo , Relación Estructura-Actividad
2.
Bioorg Med Chem Lett ; 25(16): 3275-80, 2015 Aug 15.
Artículo en Inglés | MEDLINE | ID: mdl-26105194

RESUMEN

Although overweight and obesity are highly prevalent conditions, options to treat them are still very limited. As part of our search for safe and effective MCH-R1 antagonists for the treatment of obesity, two series of pyridones and pyridazinones were evaluated. Optimization was aimed at improving DMPK properties by increasing metabolic stability and improving the safety profile by reducing inhibition of the hERG channel and reducing the potential to induce phospholipidosis. Steric shielding of a labile keto moiety with an ortho-methyl group and fine-tuning of the polarity in several parts of the molecule resulted in BI 186908 (11 g), a potent and selective MCH-R1 antagonist with favorable DMPK and CMC properties. Chronic administration of BI 186908 resulted in significant body weight reduction comparable to sibutramine in a 4 week diet-induced obesity model in rats. Based on its favorable safety profile, BI 186908 was advanced to pre-clinical development.


Asunto(s)
Fármacos Antiobesidad/síntesis química , Fármacos Antiobesidad/farmacología , Piridazinas/síntesis química , Piridazinas/farmacología , Piridinas/síntesis química , Piridinas/farmacología , Receptores de Somatostatina/antagonistas & inhibidores , Animales , Depresores del Apetito/farmacología , Peso Corporal/efectos de los fármacos , Ciclobutanos/farmacología , Descubrimiento de Drogas , Canales de Potasio Éter-A-Go-Go/antagonistas & inhibidores , Hepatocitos/metabolismo , Ensayos Analíticos de Alto Rendimiento , Humanos , Técnicas In Vitro , Lipidosis/tratamiento farmacológico , Microsomas Hepáticos/metabolismo , Fosfolípidos/metabolismo , Bloqueadores de los Canales de Potasio/síntesis química , Bloqueadores de los Canales de Potasio/farmacología , Pirazinas/síntesis química , Pirazinas/farmacología , Ratas , Relación Estructura-Actividad
3.
Bioorg Med Chem Lett ; 25(16): 3270-4, 2015 Aug 15.
Artículo en Inglés | MEDLINE | ID: mdl-26077492

RESUMEN

Despite recent success there remains a high therapeutic need for the development of drugs targeting diseases associated with the metabolic syndrome. As part of our search for safe and effective MCH-R1 antagonists for the treatment of obesity, a series of 3,6-disubstituted pyridazines was evaluated. During optimization several issues of the initial lead structures had to be resolved, such as selectivity over related GPCRs, inhibition of the hERG channel as well as the potential to induce phospholipidosis. Utilizing property-based design, we could demonstrate that all parameters can significantly be improved by consequently increasing the polarity of the compounds. By this strategy, we succeeded in identifying potent and orally available MCH-R1 antagonists with good selectivity over M1 and 5-HT2A and an improved safety profile with respect to hERG inhibition and phospholipidosis.


Asunto(s)
Fármacos Antiobesidad/síntesis química , Canales de Potasio Éter-A-Go-Go/antagonistas & inhibidores , Lipidosis/tratamiento farmacológico , Fosfolípidos/metabolismo , Bloqueadores de los Canales de Potasio/síntesis química , Bloqueadores de los Canales de Potasio/farmacología , Piridazinas/síntesis química , Piridazinas/farmacología , Receptores de Somatostatina/antagonistas & inhibidores , Animales , Fármacos Antiobesidad/farmacología , Bloqueadores de los Canales de Potasio/farmacocinética , Piridazinas/farmacocinética , Ratas , Ratas Wistar , Receptor de Serotonina 5-HT2A/efectos de los fármacos , Antagonistas de la Serotonina/síntesis química , Antagonistas de la Serotonina/farmacología , Relación Estructura-Actividad
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