Material Testing of Historic Bricks and Mortars in Degraded Masonry Structures.

The subject of this article is material research carried out on the ruins of a medieval castle located in west-central Poland. This facility was built at the beginning of the 15th century by the Order of St. John, and during its long life, it was subjected to many reconstructions. Unfortunately, in 1975, it was destroyed by fire. Since then, it has been left in a state of advanced ruin, exposed to climatic influences without any protection. The subject of the research was to assess the possibility of maintaining such buildings in a severely degraded condition while ensuring their technical efficiency. The article discusses a particular instance of "consolidation" applied to a structure in a state of historical, architectural, and structural ruin. After the diagnosis, it was determined that the structure should be safeguarded using a minimally invasive method. The purpose of these activities was to answer the question of whether the structure could be left to continue operating despite failing to meet the requirements of current standards and regulations while posing an additional danger to itself and the environment,. This goal was achieved by obtaining a considerable amount of data on the condition of the materials embedded in the masonry structure, thanks to which the initial parameters for conducting an assessment of the technical condition of the damaged masonry structure and evaluating the degree of its danger were developed. The results of the research and analysis carried out and described in this article can be used in other similar situations where saving national heritage objects through "artificial modern" strengthening will be unsafe and will lead to a loss of their authenticity. We still have a long way to go to develop a comprehensive method for "in situ" diagnosis of heterogeneous masonry structures, so we should use possible techniques and knowledge to conduct such assessments and propose rescue methods for historically valuable objects in a way that could minimize the damage and that can "easily" disappear from our surroundings. Each study should have a specific purpose, not only research but also a long-term perspective, making it possible to leave material for further research and analysis, including testing new research methods in real conditions of its installation.

Analysis of Resistance to Wind Suction of Flat Roof Coverings Glued with Polyurethane Adhesives.

The article analyses the impact of wind suction on roof coverings glued with polyurethane adhesives to flat roofs, i.e., roofs with an up to 20% slope. The impact of the cyclical wind was simulated in fatigue tests, gradually increasing the test pressure in repeated sequences until the first delamination occurred. The tests were carried out for eight test sets, with concrete and trapezoidal sheets used as a construction substrate, on whose surface thermal insulation layers were glued with polyurethane adhesive; the thermal insulation layers were EPS (expanded polystyrene) and PIR (polymer mainly of polyisocyanurate groups), respectively, followed by flexible sheets, i.e., a laminated PVC membrane (polyvinylchloride) and an EPDM (terpolymer of ethylene, propylene and a diene with a residual unsaturated portion of diene in the side chain)-type rubber-based membrane. The test results were compared with the functional requirements determined with computational simulation methods for the maximum wind load values on the example of wind loads for Poland. The tests confirmed that some polyurethane adhesives could ensure the operation of flexible sheets used as flat roof coverings that are failure-free from the point of view of resistance to wind suction.

Influence of Fire Exposition of Fibre-Cement Boards on Their Microstructure.

The diagnostics of materials, elements and structures after fire exposure are very complicated. Researchers carrying out such diagnostics encounter difficulties at the very beginning, e.g., how to map fire conditions. In this publication, the authors focused on the analysis of the fibre-cement composite used as facade cladding. The fibre-cement boards are construction products used in civil engineering. The fibre-cement boards are characterised by two phases: the matrix phase and the dispersed phase. The analysis of fibre-cement composite was performed using non-destructive methods. The use of non-destructive methods in the future will allow for the analysis of facades after fires without the need to obtain large elements, which will significantly reduce costs while increasing safety. The aim of the work was to determine internal changes in the microstructure of fibre-cement boards after exposure to fire. The degraded samples were compared with reference samples in the evaluation of the microstructure. An analysis was performed using a scanning electron microscope, images of backscattered electrons (BSE) and maps obtained using Energy Dispersive X-ray Spectroscopy (EDX), which allowed conclusions to be drawn. The observed changes were presented in the form of photos showing changes in the composition of the plates, and they were commented on. It should be noted that fire temperatures act destructively, and a number of changes can be observed in the microstructure. The results of the work indicate that, in the future, the use of non-destructive methods will make it possible to assess the degree of degradation of the façade after a fire.

Modelling of Resinous Material Filling Expansion Joints in Reinforced Concrete Structures.

This paper is a continuation of the research and analysis to estimate hyperelastic material constants when only uniaxial test data are available. The FEM simulation was expanded and the results obtained from three-dimensional and plane strain expansion joint models were compared and discussed. The original tests were carried out for a gap with a width of 10 mm, whereas in the case of axial stretching, the stresses and internal forces caused by the leading deformations were recorded for a smaller gap, and the axial compression was also recorded. The differences in the global response between the three- and two-dimensional models were also considered. Finally, using FEM simulations, the values of stresses and cross-sectional forces in the filling material were determined, which can be the basis for the design of expansion joints geometry. The results of these analyses could form the basis of guidelines for the design of expansion joint gaps filled with material, ensuring the waterproofing of the joint.

Application of the Acoustic Emission Method and Artificial Neural Networks to Assess the Damaging Effect of High Temperature on the Structure of Fibre-Cement Boards.

This article shows the results of research into the damaging effect of high temperature on the structure of fibre-cement boards. Samples of fibre-cement boards were exposed to high temperatures over various lengths of time and then they were investigated under the three-point bending and acoustic emission methods. In this way, the critical temperature and the duration of its influence on the structure of a fibre-cement board were determined. An artificial neural network was used to analyse the results obtained using the acoustic emission method. The investigations showed a marked fall in the number of registered AE events for the tested series of boards exposed to high temperature in comparison with the reference boards. Moreover, in the boards exposed to high temperature, a marked increase in the energy of AE events occurs during the bending test, whereby the registered events, by and large, come down to a single pulse induced by a brittle fracture. It is also demonstrated that the determination of the damaging effect of high temperature on the structure of fibre-cement boards solely on the basis of bending strength (MOR) is inadequate.

Assessment of the Destruction of a Fibre Cement Board Subjected to Fire in a Large-Scale Study.

This article presents the results of a study involving the assessment of the structural destruction of fibre cement boards taken from a large-scale model subjected to fire. These were subjected to a three-point bending test using the acoustic emission method. The analysis of the obtained results took into account the course of bending stresses σm, the modulus of rupture (MOR), the number of acoustic emission events Nzd and the sum of EA events ∑Nzd. The conducted tests showed that the samples subjected to fire exhibited a clear decrease, up to 72%, in the recorded sum of EA events compared to a reference board (not subjected to fire). The analysis of the obtained modulus of rupture (MOR) values showed a similar trend-the reduction of the modulus of rupture for the degraded samples was in the range of 66-96%. In order to illustrate the changes taking place in the structure of the tested plates more precisely, analyses were carried out using the optical method and a digital microscope. This method may be sufficient for the final evaluation of degraded samples.

Testing of Materials and Elements in Civil Engineering.

This issue is proposed and organized as a means to present recent developments in the field of testing of materials in civil engineering. For this reason, the articles highlighted in this issue should relate to different aspects of testing of different materials in civil engineering, from building materials and elements to building structures. The current trend in the development of materials testing in civil engineering is mainly concerned with the detection of flaws and defects in elements and structures using destructive, semi-destructive, and nondestructive testing. The trend, as in medicine, is toward designing test equipment that allows one to obtain a picture of the inside of the tested element and materials. Very interesting results with significance for building practices of testing of materials and elements in civil engineering were obtained.

Analysis of the Possibility of Plastic Deformation Characterisation in X2CrNi18-9 Steel Using Measurements of Electromagnetic Parameters.

An analysis was conducted on the possibility of making an assessment of the degree of plastic deformation ε in X2CrNi18-9 steel by measuring three electromagnetic diagnostic signals: the Barkhausen noise features, the impedance components in in-series LCR circuits, and the residual magnetic field components. The impact of ε on a series of different extracted features of diagnostic signals was investigated. The occurrence of two regions of sensitivity was found for all the features of the analysed signals. The two regions were separated by the following critical deformation value: ε ~ 10% for the components of the residual magnetic field and ε ~ 15% for the normalised components of impedance. As for the Barkhausen noise signal, the values were as follows: ε ~ 20% for the mean value, ε ~ 20% for the peak value of the signal envelope, and ε ~ 5% for the total number of the signal events. Metallographic tests were performed, which revealed essential changes in the microstructure of the tested material for the established critical values. The martensite transformation occurring during the plastic deformation process of X2CrNi18-9 austenitic steel process generated a magnetic phase. This magnetic phase was strong enough to relate the strain state to the values of diagnostic signals. The changes in the material electromagnetic properties due to martensitic transformation (γ → α') began much earlier than indicated by the metallographic testing results.

Reduction of Load Capacity of Fiber Cement Board Facade Cladding under the Influence of Fire.

The paper analyzes the issue of the reduction of load capacity in fiber cement board during a fire. Fiber cement boards were put under the influence of fire by using a large-scale facade model. Such a model is a reliable source of knowledge about the behavior of facade cladding and the way fire spreads. One technical solution for external walls-a ventilated facade-is gaining popularity and is used more and more often. However, the problem of the destruction during a fire of a range of different materials used in external facade cladding is insufficiently recognized. For this study, the authors used fiber cement boards as the facade cladding. Fiber cement boards are fiber-reinforced composite materials, mainly used for facade cladding, but also used as roof cladding, drywall, drywall ceiling and floorboards. This paper analyzes the effect of fire temperatures on facade cladding using a large-scale facade model. Samples were taken from external facade cladding materials that were mounted on the model at specific locations above the combustion chamber. Subsequently, three-point bending flexural tests were performed and the effects of temperature and the integrals of temperature and time functions on the samples were evaluated. The three-point bending flexural test was chosen because it is a universal method for assessing fiber cement boards, cited in Standard EN 12467. It also allows easy reference to results in other literature.

The Increase in the Elastic Range and Strengthening Control of Quasi Brittle Cement Composites by Low-Module Dispersed Reinforcement: An Assessment of Reinforcement Effects.

This paper presents the possibility of using low-module polypropylene dispersed reinforcement (E = 4.9 GPa) to influence the load-deflection correlation of cement composites. Problems have been indicated regarding the improvement of elastic range by using that type of fibre as compared with a composite without reinforcement. It was demonstrated that it was possible to increase the ability to carry stress in the Hooke's law proportionality range in mortar and paste types of composites reinforced with low-module fibres, i.e., Vf = 3% (in contrast to concrete composites). The possibility of having good strengthening and deflection control in order to limit the catastrophic destruction process was confirmed. In this paper, we identify the problem of deformation assessment in composites with significant deformation capacity. Determining the effects of reinforcement based on a comparison with a composite without fibres is suggested as a reasonable approach as it enables the comparison of results obtained by various universities with different research conditions.

The Recognition of the Micro-Events in Cement Composites and the Identification of the Destruction Process Using Acoustic Emission and Sound Spectrum.

This paper presents the recognition of micro-events and their concentration in quasi-brittle cement composites and the identification of the destruction process based on acoustic emission and sound spectrum. The tests were conducted on a quasi-brittle composite of a cement paste reinforced with a high volume of dispersed polypropylene fibers. The possibility of identifying the destruction process based on acoustic emission and sound spectrum was confirmed. This paper focused on the identification of micro-events using the 3D spectrum. It was shown that the identification of the concentration of micro-events precedes the occurrence of critical crack fcr, ending the Hooke's law range. The ability to recognize this phenomenon with the use of the 3D spectrum makes it possible to predict the structure destruction process and subsequently to assess the structure destruction (micro and macro-cracks) and the reinforcement destruction (pull-off, breaking). It was confirmed that the three-dimensional spectrum provided additional information, enabling a better recognition of micro and macro-changes in the structure of the samples based on the analysis of sound intensity, amplitudes, and frequencies.

Tests of Fiber Cement Materials Containing Recycled Cellulose Fibers.

This paper presents the results of investigations into the effect of the use of recycled waste paper cellulose fibers on the properties of fiber cement boards subjected to contamination by moisture. Four series of fiber cement boards were tested. A reference fiber cement board manufactured without the use of recycled cellulose fibers constituted as one of the series. The other three series consisted of boards differing in their recycled cellulose fiber content-ranging from 10% to 50% of the total cellulose fiber content. Specimens of the fiber cement boards were subjected to contamination by moisture by storing them in water for 1-96 h. Subsequently, their basic physical and mechanical parameters, i.e., mass moisture content, absorbability, and modulus of rupture (MOR), were tested. Then, the specimens were investigated by means of acoustic emission during three-point bending. Artificial neural networks were employed to analyze the acoustic emission test results. The tests clearly showed the amount of recycled waste paper cellulose fibers and the length of storage in water to have an adverse effect on the boards, contributing to their degradation. This was reflected in the decrease of the acoustic emission (AE) events count recognized by the artificial neural networks, accompanying the rupture of fibers during the three-point bending of the specimens. In order to gain a more detailed insight into the changes taking place in the structure of the tested fiber cement boards, optical examinations were carried out by means of a scanning electron microscope. Interesting findings crucial for building practice were noted.

Identification of the Destruction Model of Ventilated Facade under the Influence of Fire.

Ventilated facades are becoming an increasingly popular solution for external part of walls in the buildings. They may differ in many elements, among others things: claddings (fiber cement boards, HPL plates, large-slab ceramic tiles, ACM panels, stone cladding), types of substructures, console supports, etc. The main part that characterizes ventilated facades is the use of an air cavity between the cladding and thermal insulation. Unfortunately, in some aspects they are not yet well-standardized and tested. Above all, the requirements for the falling-off of elements from ventilated facades during a fire are not precisely defined by, among other things, the lack of clearly specified requirements and testing. This is undoubtedly a major problem, as it significantly affects the safety of evacuation during a fire emergency. For the purposes of this article, experimental tests were carried out on a large-scale facade model, with two types of external-facade cladding. The materials used as external cladding were fiber cement boards and large-slab ceramic tiles. The model of large-scale test was 3.95 m × 3.95 m, the burning gas released from the burner was used as the source of fire. The test lasted one hour. The facade model was equipped with thermocouples. The cladding materials showed different behavior during the test. Large-slab ceramic tiles seemed to be a safer form of external cladding for ventilated facades. Unfortunately, they were destroyed much faster, for about 6 min. Large-slab ceramic tiles were destroyed within the first dozen or so minutes, then their destruction did not proceed or was minimal. In the case of fiber cement boards, the destruction started from the eleventh minute and increased until the end of the test. The authors referred the results of large-scale test to testing on samples carried out by other authors. The results presented the convergence of large-scale test with samples. External claddings was equipped with additional mechanical protection. The use of additional mechanical protection to maintain external cladding elements increases their safety but does not completely eliminate the problem of the falling-off of parts of the facade. As research on fiber cement boards and large-slab ceramic tiles presented, these claddings were a major hazard due to fall-off from facade.

Mechanical and Non-Destructive Testing of Plasterboards Subjected to a Hydration Process.

The aim of this study was to investigate the effect of plasterboards' humidity absorption on their performance. Specimens' hydration procedure consisted of consecutive immersing in water and subsequent drying at room temperature. Such a procedure was performed to increase the content of moisture within the material volume. The microstructural observations of five different plasterboard types were performed through optical and scanning electron microscopy. The deterioration of their properties was evaluated by using a three-point bending test and a subsequent ultrasonic (ultrasound testing (UT)) longitudinal wave velocity measurement. Depending on the material porosity, a loss of UT wave velocity from 6% to 35% and a considerable decrease in material strength from 70% to 80% were observed. Four types of approximated formulae were proposed to describe the dependence of UT wave velocity on board moisture content. It was found that the proposed UT method could be successfully used for the on-site monitoring of plasterboards' hydration processes.

Evaluation of Ferromagnetic Steel Hardness Based on an Analysis of the Barkhausen Noise Number of Events.

Measurements are carried out of the Barkhausen noise (BN) and hardness on specimens where changes in hardness were obtained due to strain hardening (S235 and DC01 steels) and due to thermochemical treatment (AMS 6414 steel). A method is presented of processing the recorded BN signal to extract diagnostic information. The BN number of events is selected as the signal characteristic property to develop relevant correlations. A new methodology is presented for the development of correlations between the Barkhausen noise number of events and hardness. A possibility is indicated of developing correlations with a high R2 determination coefficient. The method limitations are specified.

Assessment of the Mechanical Properties of ESD Pseudoplastic Resins for Joints in Working Elements of Concrete Structures.

Concrete structure joints are filled in mainly in the course of sealing works ensuring protection against the influence of water. This paper presents the methodology of testing the mechanical properties of ESD pseudoplastic resins (E-elastic deformation, S-strengthening control, D-deflection control) recommended for concrete structure joint fillers. The existing standards and papers concerning quasi-brittle cement composites do not provide an adequate point of reference for the tested resins. The lack of a standardised testing method hampers the development of materials universally used in expansion joint fillers in reinforced concrete structures as well as the assessment of their properties and durability. An assessment of the obtained results by reference to the reference sample has been suggested in the article. A test stand and a method of assessing the mechanical properties results (including adhesion to concrete surface) of pseudoplastic resins in the axial tensile test have been presented.

Detection of Flaws in Concrete Using Ultrasonic Tomography and Convolutional Neural Networks.

Non-destructive testing of concrete for defects detection, using acoustic techniques, is currently performed mainly by human inspection of recorded images. The images consist of the inside of the examined elements obtained from testing devices such as the ultrasonic tomograph. However, such an automatic inspection is time-consuming, expensive, and prone to errors. To address some of these problems, this paper aims to evaluate a convolutional neural network (CNN) toward an automated detection of flaws in concrete elements using ultrasonic tomography. There are two main stages in the proposed methodology. In the first stage, an image of the inside of the examined structure is obtained and recorded by performing ultrasonic tomography-based testing. In the second stage, a convolutional neural network model is used for automatic detection of defects and flaws in the recorded image. In this work, a large and pre-trained CNN is used. It was fine-tuned on a small set of images collected during laboratory tests. Lastly, the prepared model was applied for detecting flaws. The obtained model has proven to be able to accurately detect defects in examined concrete elements. The presented approach for automatic detection of flaws is being developed with the potential to not only detect defects of one type but also to classify various types of defects in concrete elements.

Non-Destructive Testing of Materials in Civil Engineering.

This issue was proposed and organized as a means to present recent developments in the field of non-destructive testing of materials in civil engineering. For this reason, the articles highlighted in this editorial relate to different aspects of non-destructive testing of different materials in civil engineering, from building materials to building structures. The current trend in the development of non-destructive testing of materials in civil engineering is mainly concerned with the detection of flaws and defects in concrete elements and structures, and acoustic methods predominate in this field. As in medicine, the trend is towards designing test equipment that allows one to obtain a picture of the inside of the tested element and materials. Interesting results with significance for building practices were obtained.

Multi-Scale Structural Assessment of Cellulose Fibres Cement Boards Subjected to High Temperature Treatment.

The methodology of multi-scale structural assessment of the different cellulose fibre cement boards subjected to high temperature treatment was proposed. Two specimens were investigated: Board A (air-dry reference specimen) and Board B (exposed to a temperature of 230 °C for 3 h). At macroscale all considered samples were subjected to the three-point bending test. Next, two methodologically different microscopic techniques were used to identify evolution (caused by temperature treatment) of geometrical and mechanical morphology of boards. For that purpose, SEM imaging with EDS analysis and nanoindentation tests were utilized. High temperature was found to have a degrading effect on the fibres contained in the boards. Most of the fibres in the board were burnt-out, or melted into the matrix, leaving cavities and grooves which were visible in all of the tested boards. Nanoindentation tests revealed significant changes of mechanical properties caused by high temperature treatment: "global" decrease of the stiffness (characterized by nanoindentation modulus) and "local" decrease of hardness. The results observed at microscale are in a very good agreement with macroscale behaviour of considered composite. It was shown that it is not sufficient to determine the degree of degradation of fibre-cement boards solely on the basis of bending strength; advanced, microscale laboratory techniques can reveal intrinsic structural changes.

Effect of Freeze-Thaw Cycling on the Failure of Fibre-Cement Boards, Assessed Using Acoustic Emission Method and Artificial Neural Network.

This paper presents the results of investigations into the effect of freeze-thaw cycling on the failure of fibre-cement boards and on the changes taking place in their structure. Fibre-cement board specimens were subjected to one and ten freeze-thaw cycles and then investigated under three-point bending by means of the acoustic emission method. An artificial neural network was employed to analyse the results yielded by the acoustic emission method. The investigations conclusively proved that freeze-thaw cycling had an effect on the failure of fibre-cement boards, as indicated mainly by the fall in the number of acoustic emission (AE) events recognized as accompanying the breaking of fibres during the three-point bending of the specimens. SEM examinations were carried out to gain better insight into the changes taking place in the structure of the tested boards. Interesting results with significance for building practice were obtained.