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Polyolefins exhibit robust mechanical and chemical properties and can be applied in the medical field, e.g. for the manufacturing of dentures. Despite their wide range of applications, they are rarely used in extrusion-based printing due to their warpage tendency. The aim of this study was to investigate and reduce the warpage of polyolefins compared to commonly used filaments after additive manufacturing (AM) and sterilization using finite element simulation. Three types of filaments were investigated: a medical-grade polypropylene (PP), a glass-fiber reinforced polypropylene (PP-GF), and a biocopolyester (BE) filament, and they were compared to an acrylic resin (AR) for material jetting. Square specimens, standardized samples prone to warpage, and denture bases (n = 10 of each group), as clinically relevant and anatomically shaped reference, were digitized after AM and steam sterilization (134 °C). To determine warpage, the volume underneath the square specimens was calculated, while the deviations of the denture bases from the printing file were measured using root mean square (RMS) values. To reduce the warpage of the PP denture base, a simulation of the printing file based on thermomechanical calculations was performed. Statistical analysis was conducted using the Kruskal-Wallis test, followed by Dunn's test for multiple comparisons. The results showed that PP exhibited the greatest warpage of the square specimens after AM, while PP-GF, BE, and AR showed minimal warpage before sterilization. However, warpage increased for PP-GF, BE and AR during sterilization, whereas PP remained more stable. After AM, denture bases made of PP showed the highest warpage. Through simulation-based optimization, warpage of the PP denture base was successfully reduced by 25%. In contrast to the reference materials, PP demonstrated greater dimensional stability during sterilization, making it a potential alternative for medical applications. Nevertheless, reducing warpage during the cooling process after AM remains necessary, and simulation-based optimization holds promise in addressing this issue.
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Polipropilenos , Vapor , Polienos , Resinas Acrílicas/química , EsterilizaciónRESUMEN
To date, it is unknown whether 3D printed fixed oral implant-supported prostheses can achieve comparable soft tissue integration (STI) to clinically established subtractively manufactured counterparts. STI is mediated among others by gingival fibroblasts (GFs) and is modulated by biomaterial surface characteristics. Therefore, the aim of the present work was to investigate the GF response of a 3D printed methacrylate photopolymer and a hybrid ceramic-filled methacrylate photopolymer for fixed implant-supported prostheses in the sense of supporting an STI. Subtractively manufactured samples made from methacrylate polymer and hybrid ceramic were evaluated for comparison and samples from yttria-stabilized tetragonal zirconia polycrystal (3Y-TZP), comprising well documented biocompatibility, served as control. Surface topography was analyzed by scanning electron microscopy and interferometry, elemental composition by energy-dispersive x-ray spectroscopy, and wettability by contact angle measurement. The response of GFs obtained from five donors was examined in terms of membrane integrity, adhesion, morphogenesis, metabolic activity, and proliferation behavior by a lactate-dehydrogenase assay, fluorescent staining, a resazurin-based assay, and DNA quantification. The results revealed all surfaces were smooth and hydrophilic. GF adhesion, metabolic activity and proliferation were impaired by 3D printed biomaterials compared to subtractively manufactured comparison surfaces and the 3Y-TZP control, whereas membrane integrity was comparable. Within the limits of the present investigation, it was concluded that subtractively manufactured surfaces are superior compared to 3D printed surfaces to support STI. For the development of biologically optimized 3D printable biomaterials, consecutive studies will focus on the improvement of cytocompatibility and the synthesis of STI-relevant extracellular matrix constituents.
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Materiales Biocompatibles , Fibroblastos , Encía , Impresión Tridimensional , Fibroblastos/citología , Fibroblastos/efectos de los fármacos , Fibroblastos/metabolismo , Humanos , Encía/citología , Materiales Biocompatibles/química , Proliferación Celular/efectos de los fármacos , Células Cultivadas , Adhesión Celular/efectos de los fármacos , Humectabilidad , Implantes Dentales , Ensayo de Materiales , Propiedades de Superficie , Metacrilatos/química , Metacrilatos/farmacologíaRESUMEN
OBJECTIVES: This in vitro study aimed to assess the influence of the planning software and design of the surgical template on both trueness and precision of static computer assisted implant surgery (sCAIS) performed using guides fabricated using material extrusion (ME). METHODS: Three-dimensional radiographic and surface scans of a typodont were aligned using two planning software (coDiagnostiX, CDX; ImplantStudio, IST) to virtually position the two adjacent oral implants. Thereafter, surgical guides were fabricated with either an original (O) or modified (M) design with reduced occlusal support and were sterilized. Forty surgical guides were used to install 80 implants equally distributed amongst four groups: CDX-O, CDX-M, IST-O, and IST-M. Thereafter, the scan bodies were adapted to the implants and digitized. Finally, inspection software was used to assess discrepancies between the planned and final positions at the implant shoulder and main axis level. Multilevel mixed-effects generalised linear models were used for statistical analyses (p = 0.05). RESULTS: In terms of trueness, the largest average vertical deviations (0.29 ± 0.07 mm) were be assessed for CDX-M. Overall, vertical errors were dependant on the design (O < M; p ≤ 0.001). Furthermore, in horizontal direction, the largest mean discrepancy was 0.32 ± 0.09 mm (IST-O) and 0.31 ± 0.13 mm (CDX-M). CDX-O was superior compared to IST-O (p = 0.003) regarding horizontal trueness. The average deviations regarding the main implant axis ranged between 1.36 ± 0.41° (CDX-O) and 2.63 ± 0.87° (CDX-M). In terms of precision, mean standard deviation intervals of ≤ 0.12 mm (IST-O and -M) and ≤ 1.09° (CDX-M) were calculated. CONCLUSIONS: Implant installation with clinically acceptable deviations is possible with ME surgical guides. Both evaluated variables affected trueness and precision with negligible differences. CLINICAL SIGNIFICANCE: The planning system and design influenced the accuracy of implant installation using ME-based surgical guides. Nevertheless, discrepancies were ≤ 0.32 mm and ≤ 2.63°, which may be considered within the range of clinical acceptance. ME should be further investigated as an alternative to the more expensive and time-consuming 3D printing technologies.
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Implantes Dentales , Implantación Dental Endoósea , Diseño Asistido por Computadora , Imagenología Tridimensional , Tomografía Computarizada de Haz Cónico , Programas Informáticos , ComputadoresRESUMEN
Dental implants need to combine mechanical strength with promoted osseointegration. Currently used subtractive manufacturing techniques require a multi-step process to obtain a rough surface topography that stimulates osseointegration. Advantageously, additive manufacturing (AM) enables direct implant shaping with unique geometries and surface topographies. In this study, zirconia implants with integrated lamellar surface topography were additively manufactured by nano-particle ink-jetting. The ISO-14801 fracture load of as-sintered implants (516±39 N) resisted fatigue in 5-55 °C water thermo-cycling (631±134 N). Remarkably, simultaneous mechanical fatigue and hydrothermal aging at 90 °C significantly increased the implant strength to 909±280 N due to compressive stress generated at the seamless transition of the 30-40 µm thick, rough and porous surface layer to the dense implant core. This unique surface structure induced an elongated osteoblast morphology with uniform cell orientation and allowed for osteoblast proliferation, long-term attachment and matrix mineralization. In conclusion, the developed AM zirconia implants not only provided high long-term mechanical resistance thanks to the dense core along with compressive stress induced at the transition zone, but also generated a favorable osteoblast response owing to the integrated directional surface pores. STATEMENT OF SIGNIFICANCE: Zirconia ceramics are becoming the material of choice for metal-free dental implants, however significant efforts are required to obtain a rough/porous surface for enhanced osseointegration, along with the risk of surface delamination and/or microstructure variation. In this study, we addressed the challenge by additively manufacturing implants that seamlessly combine dense core with a porous surface layer. For the first time, a unique surface with a directional lamellar pore morphology was additively obtained. This AM implant also provided strength as strong as conventionally manufactured zirconia implants before and after long-term fatigue. Favorable osteoblast response was proved by in-vitro cell investigation. This work demonstrated the opportunity to AM fabricate novel ceramic implants that can simultaneously meet the mechanical and biological functionality requirements.
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Implantes Dentales , Ensayo de Materiales , Osteoblastos , Impresión Tridimensional , Propiedades de Superficie , Titanio/química , Circonio/química , Circonio/farmacologíaRESUMEN
OBJECTIVE: To evaluate the impact of reducing the radiographic field of view (FOV) on the trueness and precision of the alignment between cone beam computed tomography (CBCT) and intraoral scanning data for implant planning. MATERIALS AND METHODS: Fifteen participants presenting with one of three clinical scenarios: single tooth loss (ST, n = 5), multiple missing teeth (MT, n = 5) and presence of radiographic artifacts (AR, n = 5) were included. CBCT volumes covering the full arch (FA) were reduced to the quadrant (Q) or the adjacent tooth/teeth (A). Two operators, an expert (exp) in virtual implant planning and an inexperienced clinician, performed multiple superimpositions, with FA-exp serving as a reference. The deviations were calculated at the implant apex and shoulder levels. Thereafter, linear mixed models were adapted to investigate the influence of FOV on discrepancies. RESULTS: Evaluation of trueness compared to FA-exp resulted in the largest mean (AR-A: 0.10 ± 0.33 mm) and single maximum discrepancy (AR-Q: 1.44 mm) in the presence of artifacts. Furthermore, for the ST group, the largest mean error (-0.06 ± 0.2 mm, shoulder) was calculated with the FA-FOV, while for MT, with the intermediate volume (-0.07 ± 0.24 mm, Q). In terms of precision, the mean SD intervals were ≤0.25 mm (A-exp). Precision was influenced by FOV volume (FA < Q < A) but not by operator expertise. CONCLUSIONS: For single posterior missing teeth, an extended FOV does not improve registration accuracy. However, in the presence of artifacts or multiple missing posterior teeth, caution is recommended when reducing FOV.
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Implantes Dentales , Diente , Tomografía Computarizada de Haz Cónico/métodos , Humanos , Imagenología Tridimensional , Proyectos Piloto , Estudios RetrospectivosRESUMEN
OBJECTIVE: To evaluate the manufacturing accuracy of zirconia four-unit fixed dental prostheses (FDPs) fabricated by three different additive manufacturing technologies compared with subtractive manufacturing. METHODS: A total of 79 zirconia FDPs were produced by three different manufacturing technologies, representing additive (one stereolithography [aSLA] and one material jetting [aMJ] device, two digital light processing [aDLP1/aDLP2] devices) and subtractive manufacturing (two devices [s1/s2]), the latter serving as references. After printing, additively manufactured FDPs were debound and finally sintered. Subsequently, samples were circumferentially digitized and acquired surface areas were split in three Regions Of Interest (ROIs: inner/outer shell, margin). Design and acquired data were compared for accuracy using an inspection software. Statistical evaluation was performed using the root mean square error (RMSE) and nonparametric Kruskal-Wallis method with post hoc Wilcoxon-Mann-Whitney U tests. Bonferroni correction was applied in case of multiple testing. RESULTS: Regardless the ROI, significant differences were observed between manufacturing technologies (P < 0.001). Subtractive manufacturing was the most accurate with no significant difference regarding the material/device (s1/s2, P > 0.054). Likewise, no statistical difference regarding accurary was found when comparing s2 with aMJ and aSLA in most ROIs (P > 0.085). In general, mean surface deviation was< 50 µm for s1/s2 and aMJ and< 100 µm for aSLA and aDLP2. aDLP1 showed surface deviations> 100 µm and was the least accurate compared to the other additive/subtractive technologies. SIGNIFICANCE: Additive manufacturing represents a promising set of technologies for the manufacturing of zirconia FDPs, but not yet as accurate as subtractive manufacturing. Methodological impact on accuracy within and in between different additive technologies needs to be further investigated.
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Diseño de Prótesis Dental , Estereolitografía , Diseño Asistido por Computadora , CirconioRESUMEN
BACKGROUND: There are little scientific data on fully automated Peer Assessment Rating (PAR); this study compares a number of PAR scoring methods to assess their reliability. OBJECTIVES: This investigation evaluated PAR scores of plaster, 3D printed, and virtual digital models scored by specialist orthodontists, dental auxiliaries, undergraduate dental students,and using a fully automated method. MATERIALS AND METHODS: Twelve calibrated assessors determined the PAR score of a typodont and this score was used as the gold standard. Measurements derived from a plaster model, a 3D printed model, and a digital model, were compared. A total of 120 practitioners (specialist orthodontists, dental auxiliaries, and undergraduate dental students, n = 40 each) scored the models (n = 10) per group. The digital models were scored twice, using OnyxCeph (OnyxCeph) and OrthoAnalyzer (3Shape). The fully automated PAR scoring was performed with Model+ (Carestream Dental). RESULTS: Neither type of model (P = 0.077), practitioner category (P = 0.332), nor interaction between the two (P = 0.728) showed a statistically significant effect on PAR scoring. The mean PAR score and standard deviation were comparable for all models and groups except the automated group, where the standard deviation was the smallest (SD = 0). Overall, the greatest variation was observed for weighted overjet and contact point displacements. CONCLUSIONS: PAR scoring using plaster, 3D printed, and digital study models by orthodontists, dental auxiliaries, dental students, and a fully automated method produced very similar results and can hence be considered equivalent. Automated measurements improve repeatability compared with all groups of practitioners, but this did not reach the significance level.
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Modelos Dentales , Ortodoncistas , Humanos , Imagenología Tridimensional , Reproducibilidad de los Resultados , Estudiantes de OdontologíaRESUMEN
Extrusion-based printing enables simplified and economic manufacturing of surgical guides for oral implant placement. Therefore, the cytotoxicity of a biocopolyester (BE) and a polypropylene (PP), intended for the fused filament fabrication of surgical guides was evaluated. For comparison, a medically certified resin based on methacrylic esters (ME) was printed by stereolithography (n = 18 each group). Human gingival keratinocytes (HGK) were exposed to eluates of the tested materials and an impedance measurement and a tetrazolium assay (MTT) were performed. Modulations in gene expression were analyzed by quantitative PCR. One-way ANOVA with post-hoc Tukey tests were applied. None of the materials exceeded the threshold for cytotoxicity (< 70% viability in MTT) according to ISO 10993-5:2009. The impedance-based cell indices for PP and BE, reflecting cell proliferation, showed little deviations from the control, while ME caused a reduction of up to 45% after 72 h. PCR analysis after 72 h revealed only marginal modulations caused by BE while PP induced a down-regulation of genes encoding for inflammation and apoptosis (p < 0.05). In contrast, the 72 h ME eluate caused an up-regulation of these genes (p < 0.01). All evaluated materials can be considered biocompatible in vitro for short-term application. However, long-term contact to ME might induce (pro-)apoptotic/(pro-)inflammatory responses in HGK.
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Polímeros , Estereolitografía , Encía , Humanos , Queratinocitos , Polipropilenos/toxicidadRESUMEN
The purpose of the study was to compare conventional to digital workflows of occlusal splint production regarding time efficiency, overall fit, and wear. Fifteen Michigan splints were fabricated with a conventional and digital method. The duration for the dentist's and the dental technician's workload was recorded. Subsequently, the overall fit was examined with a four-level score (1-4). Paired t-tests were used to compare the time results for the conventional and digital workflows and the sign test to compare the overall fit. The mean time (16 min 58 s) for computerized optical impressions was longer than for conventional impressions (6 min 59 s; p = 0.0001). However, the dental technician needed significantly less mean time for the digital splint production (47 min 52 s) than for the conventional (163 min 32 s; p = 0.001). The overall fit of the digitally-fabricated splints was significantly better compared to the conventionally-fabricated splints (p = 0.002). There was no impact of the different materials used in the conventional and digital workflow on the wear (p = 0.26). The results suggest that the digital workflow for the production of occlusal splints is more time efficient and leads to a better fit than the conventional workflow.
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PURPOSE: The accuracy of intraoral and model scanners has been widely investigated with heterogeneous results, but the impact of the applied diversity of measurement methods on the outcomes remains unknown. This study aimed to evaluate the influence of methodological factors on the measurement result when comparing full-arch scans. METHODS: The evaluation referred to a 5M model to analyze whether accuracy measurements are affected by (1) the reference geometry, (2) mesh density of the standard tessellation language (STL) datasets, (3) operator, (4) inspection software, and (5) alignment procedure. STL datasets of full-arch reference models were measured with 29 different combinations of these factors. For each combination, 10 repeated measurements of the intermolar width were performed. Trueness was statistically analyzed with one-way ANOVA and T-tests, repeatability with Levene tests, and reproducibility with interclass correlation coefficients. RESULTS: Measurement method variations affected the intermolar width by up to 186 µm. The alignment algorithm had a significant effect on the measurement outcome (p = 0.001). Likewise, reference geometry influenced trueness and repeatability significantly (p = 0.001), whereas mesh density affected the repeatability only in some cases. The operator had no impact on the measurement result. The inspection software affected the repeatability but not the trueness. CONCLUSION: The factors reference geometry and alignment algorithm highly affected the measurement outcome, while the operator, inspection software, and mesh density showed no impact on the trueness of the outcome. Cylindrical reference geometries showed fewer differences than bar-shaped ones and best-fit alignments fewer variations than alignments based on boundary parameters.
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Técnica de Impresión Dental , Modelos Dentales , Diseño Asistido por Computadora , Imagenología Tridimensional , Reproducibilidad de los ResultadosRESUMEN
The ongoing COVID-19 pandemic has revealed alarming shortages of personal protective equipment for frontline healthcare professionals and the general public. Therefore, a 3D-printable mask frame was developed, and its air seal performance was evaluated and compared. Personalized masks (PM) based on individual face scans (n = 8) and a statistically shaped mask (SSM) based on a standardized facial soft tissue shape computed from 190 face scans were designed. Subsequently, the masks were additively manufactured, and in a second step, the PM and SSM were compared to surgical masks (SM) and FFP2 masks (FFP2) in terms of air seal performance. 3D-printed face models allowed for air leakage evaluation by measuring the pressure inside the mask in sealed and unsealed conditions during a breathing simulation. The PM demonstrated the lowest leak flow (p < 0.01) of inspired or expired unfiltered air of approximately 10.4 ± 16.4%, whereas the SM showed the highest (p < 0.01) leakage with 84.9 ± 7.7%. The FFP2 and SSM had similar values of 34.9 ± 18.5% leakage (p > 0.68). The developed framework allows for the time- and resource-efficient, on-demand, and in-house production of masks. For the best seal performance, an individually personalized mask design might be recommended.
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COVID-19 , Máscaras , Equipo de Protección Personal , Biometría , Diseño de Equipo , Personal de Salud , Humanos , Impresión Tridimensional , Salud PúblicaRESUMEN
OBJECTIVE: To investigate the tensile and flexural strength of poured, subtractive, and additive manufactured denture base methacrylates bonded to soft and hard relining materials after hydrothermal cycling and microwave irradiation. METHODS: This study included a conventional (CB), subtractive (SB), and additive (AB) base material as well as a soft (SCR) and hard (HCR) chairside and one hard laboratory-side (HLR) relining material. Reference bodies of the base materials and bonded specimens to the relining materials were produced with a rectangular cross-section. The specimens were either pre-treated by water storage (50 h, 37 °C), hydrothermal cycling (5000 cycles, 5 °C and 55 °C, 30 s each), or microwave irradiation (6 cycles, 640 W, 3 min, wet). A tensile and four-point bending test were performed for a total of 504 specimens. Data were analysed using multivariate analysis of variance (MANOVA) with post-hoc Tukey tests (α = 0.05). RESULTS: In comparison with the other reference groups SB showed marginally higher tensile and flexural strength (p < 0.047). Bond strength to SCR was affected neither by the base material nor by the pre-treatment (p > 0.085). HCR demonstrated twice the bond strength to AB compared with SB and CB (p ≤ 0.001). HLR showed the highest bond strength to CB (p ≤ 0.001). There was no difference between the specimens after hydrothermally cycling and microwave irradiation (p > 0.318). SIGNIFICANCE: The bond strength of hard relining materials to subtractive and additive manufactured denture bases differ compared with conventional pouring.
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Recubrimiento Dental Adhesivo , Alineadores Dentales , Resinas Acrílicas , Bases para Dentadura , Ensayo de Materiales , Propiedades de Superficie , Resistencia a la TracciónRESUMEN
Computer-aided design and computer-aided manufacturing (CAD-CAM) enable subtractive or additive fabrication of temporary fixed dental prostheses (FDPs). The present in-vitro study aimed to compare the fracture resistance of both milled and additive manufactured three-unit FDPs and bar-shaped, ISO-conform specimens. Polymethylmethacrylate was used for subtractive manufacturing and a light-curing resin for additive manufacturing. Three (bars) and four (FDPs) different printing orientations were evaluated. All bars (n = 32) were subjected to a three-point bending test after 24 h of water storage. Half of the 80 FDPs were dynamically loaded (250,000 cycles, 98 N) with simultaneous hydrothermal cycling. Non-aged (n = 40) and surviving FDPs (n = 11) were subjected to static loading until fracture. Regarding the bar-shaped specimens, the milled group showed the highest flexural strength (114 ± 10 MPa, p = 0.001), followed by the vertically printed group (97 ± 10 MPa, p < 0.007). Subtractive manufactured FDPs revealed the highest fracture strength (1060 ± 89 N) with all specimens surviving dynamic loading. During artificial aging, 29 of 32 printed specimens failed. The present findings indicate that both printing orientation and aging affect the strength of additive manufactured specimens. The used resin and settings cannot be recommended for additive manufacturing of long-term temporary three-unit FDPs.
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STATEMENT OF PROBLEM: Reliable studies comparing the accuracy of complete-arch casts from 3D printers are scarce. PURPOSE: The purpose of this in vitro study was to investigate the accuracy of casts printed by using various extrusion- and photopolymerization-based printers. MATERIAL AND METHODS: A master file was sent to 5 printer manufacturers and distributors to print 37 identical casts. This file consisted of a standardized data set of a maxillary cast in standard tessellation language (STL) format comprising 5 reference points for the measurement of 3 distances that served as reference for all measurements: intermolar width (IMW), intercanine width (ICW), and dental arch length (AL). The digital measurement of the master file obtained by using a surveying software program (Convince Premium 2012) was used as the control. Two extrusion-based (M2 and Ultimaker 2+) and 3 photopolymerization-based printers (Form 2, Asiga MAX UV, and myrev140) were compared. The casts were measured by using a multisensory coordinate measuring machine (O-Inspect 422). The values were then compared with those of the master file. The Mann-Whitney U test and Levene tests were used to determine significant differences in the trueness and precision (accuracy) of the measured distances. RESULTS: The deviations from the master file at all 3 distances for the included printers ranged between 12 µm and 240 µm (trueness), with an interquartile range (IQR) between 17 µm and 388 µm (precision). Asiga MAX UV displayed the highest accuracy, considering all the distances, and Ultimaker 2+ demonstrated comparable accuracy for shorter distances (IMW and ICW). Although myrev140 operated with high precision, it displayed high deviations from the master file. Similarly, although Form 2 exhibited high IQR, it did not deviate significantly from the master file in the longest range (AL). M2 performed consistently. CONCLUSIONS: Both extrusion-based and photopolymerization-based printers were accurate. In general, inexpensive printers were no less accurate than more expensive ones.
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Modelos Dentales , Impresión Tridimensional , Diseño Asistido por Computadora , Técnica de Impresión Dental , Imagenología Tridimensional , Maxilar , Programas InformáticosRESUMEN
STATEMENT OF PROBLEM: Intraoral scanners (IOSs) are based on light-optical imaging methods. However, little is known about whether the ambient light in dental practices influences the accuracy and scanning time of the IOS. PURPOSE: The purpose of this in vitro study was to investigate the influence of different illuminations on the accuracy of 4-unit and complete-arch scans of 6 IOSs. In addition, the required scanning time was evaluated. MATERIAL AND METHODS: A reference structure was attached to the first premolars (P) and second molars (M) in both quadrants (L/R) of a maxillary model. The resulting measured distances were M1-P1, M2-P2, P1-P2, and M1-M2. The investigation included 6 IOSs: TRIOS 3 (TRI), Cerec Omnicam (OC), iTero Element (ITE), CS 3600 (CS), Planmeca Emerald (EME), and GC Aadva (AAD). With each IOS, 17 scans at different illuminances (100, 500, 1000, and 5000 lux) were performed (N = 408). The precision and trueness for all distances were determined, and the scanning time was recorded. For statistical analyses, the Levene tests (precision) and 1-way analysis of variance with the post hoc Tukey honestly significant difference and Games-Howell tests (trueness) were calculated. RESULTS: Illuminance significantly influenced the trueness of 4-unit scans for OC, EME, and AAD. TRI, OC, ITE, and CS demonstrated comparable results. AAD (>96 ±22 µm; 1000 lux) and EME (>248 ±88 µm; 500 lux) revealed greater deviations. For complete-arch scans, illuminance did not influence TRI and AAD, but significant variations were detected for ITE, CS, EME, and AAD. The least deviations were achieved with TRI and OC. The scanning time was extended for all IOSs except ITE at more than 500 lux. The shortest scanning times with OC and EME were recorded at 100 lux; with TRI, CS, and AAD at 500 lux; and with ITE at both 100 and 5000 lux. At all illuminances, the fastest scans were obtained with TRI. CONCLUSIONS: Ambient light was found to influence the accuracy and scanning time of IOSs. This influence varies depending on the device. For 4-unit scans, the effect was not clinically relevant, but for complete-arch scans, accuracy and scanning time can be improved with appropriate lighting.
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Técnica de Impresión Dental , Modelos Dentales , Diseño Asistido por Computadora , Arco Dental , Imagenología TridimensionalRESUMEN
OBJECTIVES: To investigate the wear resistance of polymers for injection molding, subtractive and additive manufacturing of occlusal devices in comparison with enamel antagonist wear and material properties (i.e., hardness, flexural strength, and flexural modulus). METHODS: Injection molding was compared with milling and the additive technologies stereolithography, low force stereolithography, and digital light processing. For each material, eight specimens were produced for wear measurements. Extracted human premolars served as indenters. All samples were subjected to two series of a 2-body wear test consisting of 200,000 circular loading cycles with an applied load of 1) 20 N and 2) 50 N in a thermocycling environment (5/55 °C, 30 s, 3860 cycles, H2O). Wear resistance was characterized by means of maximum depth and volume of the resulting traces. In addition, enamel wear of the indenters and Vickers hardness, flexural strength, and flexural modulus of the polymers were determined. Wear was statistically analyzed with linear general models for repeated measures and material properties with one-way ANOVA with post-hoc Tukey-HSD tests. RESULTS: Wear of the antagonists was not influenced by the material (P ≥ 0.343). Likewise, no differences in wear resistance were found between materials after cyclic loading with 20 N or 50 N (P ≥ 0.074). Material properties investigated revealed decreased values for the resins for the additive manufacturing with the exception of flexural strength of one material. SIGNIFICANCE: Within the limitations of this in-vitro study, arylates for conventional, subtractive, and additive manufacturing of occlusal devices differ in material properties but not in wear resistance and antagonist wear.
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Resistencia Flexional , Polímeros , Dureza , Humanos , Ensayo de Materiales , Estereolitografía , Propiedades de SuperficieRESUMEN
Occlusal devices to reduce symptoms of bruxism and temperomandibular disorders can nowadays be manufactured in a digital workflow but studies comparing the accuracy of those occlusal devices are still limited. Therefore, the aim of this investigation was to investigate the accuracy of injection molding compared with four computer-aided design (CAD) and computer-aided manufacturing (CAM) techniques for the manufacturing of occlusal devices. In addition, the number of contact points and retention were evaluated to assess clinical relevance. A conventional workflow consisting of alginate impression, wax-up, and injection molding (IM) and digital workflows including intraoral scanning, digital design, and subtractive manufacturing (SM) or additive manufacturing by using stereolithography (SLA), digital light processing (DLP), and material jetting (Polyjet) were investigated. Sixteen splints were fabricated with each method. The intaglio surfaces of the splints were laser scanned and superimposed with the reference data sets to analyze the surface deviations. In addition, the number of contact points after repositioning the splints on the reference model was evaluated with occlusal foil. Finally, the retention was measured in a tensile test. One-way ANOVA with post hoc Tukey tests were used for statistical analyses (α = .05). IM and SM splints demonstrated the highest manufacturing accuracy without significant differences to each other (P > .985). Additive manufactured splints revealed greater deviations with equal results for SLA and Polyjet (P > .949) and significantly higher deviations for DLP compared to all other groups (P < .002). Comparable retention force was measured for IM, SM, and SLA (P > .923), whereas Polyjet splints showed the greatest variability. IM and SM splints presented the most contact points (P = .505). Additive manufactured splints demonstrated fewer contacts without significant difference to each other (P > .116). It can be concluded, that there is no difference in manufacturing accuracy, retention, and number of contacts between IM and SM splints. AM splints demonstrated higher, however, clinically acceptable deviations.
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Bruxismo , Ferulas Oclusales , Diseño Asistido por Computadora , Diseño de Prótesis Dental , Humanos , Férulas (Fijadores) , Flujo de TrabajoRESUMEN
A polyolefin with certified biocompatibility according to USP class VI was used by our group as feedstock for filament-based 3D printing to meet the highest medical standards in order to print personal protective equipment for our university hospital during the ongoing pandemic. Besides the chemical resistance and durability, as well as the ability to withstand steam sterilization, this polypropylene (PP) copolymer is characterized by its high purity, as achieved by highly efficient and selective catalytic polymerization. As the PP copolymer is suited to be printed with all common printers in fused filament fabrication (FFF), it offers an eco-friendly cost-benefit ratio, even for large-scale production. In addition, a digital workflow was established focusing on common desktop FFF printers in the medical sector. It comprises the simulation-based optimization of personalized print objects, considering the inherent material properties such as warping tendency, through to validation of the process chain by 3D scanning, sterilization, and biocompatibility analysis of the printed part. This combination of digital data processing and 3D printing with a sustainable and medically certified material showed great promise in establishing decentralized additive manufacturing in everyday hospital life to meet peaks in demand, supply bottlenecks, and enhanced personalized patient treatment.
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Polienos/química , Polímeros/química , Humanos , Equipo de Protección Personal , Polipropilenos/química , Impresión TridimensionalRESUMEN
OBJECTIVE: To investigate the fracture resistance and phase composition of tooth supported four-unit fixed dental prostheses (FDPs) made from three different zirconia grades after loading and aging. METHODS: Seventy-two FDPs were fabricated from 3Y-TZP, 4Y-PSZ and 5Y-PSZ. This resulted in 24 FDPs per grade, subdivided into three groups (n = 8): a control group (C), a hydrothermally aged (H2O, 85 °C, 90 days) group (A) and a group subjected to loading (2.5M cycles, 98N) with simultaneous thermal cycling (H2O, 5-55 °C) subsequent to treatment A (AL). Subsequently, FDPs were statically loaded to fracture. Phase composition was quantified by X-ray diffraction (XRD) and µ-Raman spectroscopy. Focused ion beam (FIB) - Scanning electron microscopy (SEM) was used for visualization in-depth. RESULTS: Compared to 3Y-C FDPs (1233 ± 165N), reduced fracture load was found for 5Y-C FDPs (889 ± 80 N; p < .001). This did not apply for 4Y-C samples (1065 ± 111N). Treatments (A, AL) did not negatively affect the fracture load for the three grades of zirconia (p > .645). Both A and AL increased monoclinic phase content for 3Y and 4Y FDPs, whereas FIB-SEM suggests no transformability of 5Y-PSZ. 5Y-AL FDPs showed cracks and fractures at the abutment walls and restoration margins after dynamic loading. Reduced fracture load of 5Y samples as compared to 3Y and 4Y was associated with deficient transformability in the fracture zone. SIGNIFICANCE: Aging and loading did not negatively affect the fracture resistance of monolithic four-unit FDPs made from three grades of zirconia. Due to cracks after dynamic loading, 5Y-PSZ cannot be recommended for the clinical application of four-unit FDPs.
Asunto(s)
Porcelana Dental , Prótesis Dental , Materiales Dentales , Fracaso de la Restauración Dental , Análisis del Estrés Dental , Ensayo de Materiales , Reproducibilidad de los Resultados , CirconioRESUMEN
Zirconia implants are appreciated in some clinical indications in light of their aesthetic appearance and good biocompatibility. The aim of this work was to evaluate the performance of a newly developed two-piece zirconia/polyether ketone ketone (PEKK) implant-abutment combination after long-term cyclic loading in a hydrothermal environment, using a new protocol adapted from two available ISO standards. Sixteen implants (n = 8/group) were embedded according to ISO 14801 and divided into two groups: implants in the Observational Group (OG) were cyclically loaded for 60 days (98 N, 10 million loading cycles, 2 Hz) in 85 °C water in a chewing simulator, while non-loaded/non-aged implants (as-received) constituted the Control Group (CG). After 4.7 million loading cycles, one OG implant fractured in the chewing simulator. The surviving implants were compared to CG implants by X-ray diffraction (XRD) to investigate potential ageing as suggested by ISO 13356, but also µ-Raman spectroscopy, Focused-Ion-Beam - Scanning-Electron-Microscopy (FIB-SEM), and load-to-fracture. Ageing was shown to have limited influence on the evaluated zirconia implant, with increased monoclinic content after loading/ageing being to a shallow transformed zone of ~2 µm at the implant surface. However, OG implants showed a significantly decreased fracture load of 751 ± 231 N (CG: 995 ± 161 N; p = .046). These values enable clinical application, but the fact that one failure was recorded during cyclic fatigue along with the significant decrease in strength after cyclic loading/ageing suggest that there may be room for further optimization of especially the PEKK abutment. Furthermore, good agreement was observed between the fracture modes of the implant that failed during the cyclic fatigue experiment and the in vivo failure of one implant during pre-clinical trials, validating the interest of the in vitro protocol used in this work to check the reliability of zirconia implant.