Crystal structure of 13-(2-meth-oxy-phenyl)-3,4-di-hydro-2H-indazolo[1,2-b]phthalazine-1,6,11(13H)-trione.
Acta Crystallogr E Crystallogr Commun
; 71(Pt 8): o604-5, 2015 Aug 01.
Article
en En
| MEDLINE
| ID: mdl-26396820
In the title compound, C22H18N2O4, the three fused rings of the pyrazolo-phthalazine moiety are coplanar (r.m.s. deviation = 0.027â
Å). The cyclo-hexene ring fused to the pyrazolidine ring, so forming the indazolophthalazine unit, has a half-chair conformation. The benzene ring is almost normal to the mean plane of the pyrazolo-phthalazine moiety, with a dihedral angle of 87.21â
(6)° between their planes. In the crystal, mol-ecules are linked by pairs of C-Hâ¯O hydrogen bonds forming inversion dimers. The dimers are linked via C-Hâ¯π inter-actions, forming slabs parallel to (100). Between the slabs there are weak π-π inter-actions [shortest inter-centroid distance = 3.6664â
(9)â
Å], leading to the formation of a three-dimensional structure.
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Acta Crystallogr E Crystallogr Commun
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2015
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Article