Gradient supercritical fluid chromatography coupled to mass spectrometry with a gradient flow of make-up solvent for enantioseparation of cathinones.

Kolderová, Natalie; Jurásek, Bronislav; Kuchar, Martin; Lindner, Wolfgang; Kohout, Michal

Kolderová, Natalie; Jurásek, Bronislav; Kuchar, Martin; Lindner, Wolfgang; Kohout, Michal.

Afiliación

Kolderová N; Department of Organic Chemistry, University of Chemistry and Technology, Technická 5, 16628 Prague, Czech Republic; Forensic Laboratory of Biologically Active Substances, University of Chemistry and Technology, Technická 3, 16628 Prague, Czech Republic; Department of Chemistry of Natural Compounds,
Jurásek B; Forensic Laboratory of Biologically Active Substances, University of Chemistry and Technology, Technická 3, 16628 Prague, Czech Republic; Department of Chemistry of Natural Compounds, University of Chemistry and Technology, Technická 5, 16628 Prague, Czech Republic.
Kuchar M; Forensic Laboratory of Biologically Active Substances, University of Chemistry and Technology, Technická 3, 16628 Prague, Czech Republic; Department of Chemistry of Natural Compounds, University of Chemistry and Technology, Technická 5, 16628 Prague, Czech Republic.
Lindner W; Lindner Consulting GmbH, Ziegelofengasse 37, 3400 Klosterneuburg, Austria; Institute of Analytical Chemistry, University of Vienna, Waehringerstrasse 38, 1090 Vienna, Austria.
Kohout M; Department of Organic Chemistry, University of Chemistry and Technology, Technická 5, 16628 Prague, Czech Republic. Electronic address: michal.kohout@vscht.cz.

J Chromatogr A ; 1625: 461286, 2020 Aug 16.

Article en En | MEDLINE | ID: mdl-32709336

Asunto(s)

Alcaloides/química; Alcaloides/aislamiento & purificación; Cromatografía con Fluido Supercrítico/métodos; Espectrometría de Masas/métodos; Reología; Solventes/química; Alcaloides/síntesis química; Cromatografía Líquida de Alta Presión; Presión; Estereoisomerismo; Temperatura

Palabras clave

Cathinones; Chiral separation; Chiral zwitterion ion exchanger; Make-up solvent gradient; Mass spectrometry; Supercritical fluid chromatography

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Texto completo: 1 Base de datos: MEDLINE Asunto principal: Reología / Solventes / Espectrometría de Masas / Cromatografía con Fluido Supercrítico / Alcaloides Idioma: En Revista: J Chromatogr A Año: 2020 Tipo del documento: Article

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