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1.
Zhongguo Zhong Yao Za Zhi ; 34(20): 2577-80, 2009 Oct.
Artículo en Zh | MEDLINE | ID: mdl-20069895

RESUMEN

OBJECTIVE: To establish a gas chromatography method for simultaneous determination of organochlorine and pyrethroid pesticide residues in Viscum coloratum by cloud-point extraction (CPE). METHOD: Pesticides were extracted with the non-ionic surfactant Triton X-100. The apparatus was gas chromatography with electron capture detector and the separation was performed on an Hp-5 column. The pesticide residues were calculated by external standard method. RESULT: Good linear relation was obtained over the range of 5-500 microg L(-1) for organochlorine and 10-1,000 microg L(-1) for pyrethroid. The limits of detection was 1.5-7.5 microg kg(-1). The average recoveries of organochlorine and pyrethroid were 74.15% -111.6% with corresponding RSD of 4.0% -9.1%. CONCLUSION: The sample and rapid method was applied to pesticide residues determination.


Asunto(s)
Cromatografía de Gases/métodos , Residuos de Plaguicidas/análisis , Extractos Vegetales/análisis , Viscum/química , Límite de Detección , Octoxinol/química
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