Effects of surface treatments on the translucency, opalescence, and surface texture of dental monolithic zirconia ceramics.

STATEMENT OF PROBLEM: Surface polishing or glazing may increase the appearance of depth of monolithic zirconia restorations. PURPOSE: The purpose of this in vitro study was to investigate the effects of surface treatments on the translucency, opalescence, and surface texture of dental monolithic zirconia ceramics. MATERIAL AND METHODS: Forty-five monolithic zirconia specimens (16.3×16.4×2.0 mm) were divided into groups I to V, according to the number of colorings each received. Each group was then divided into 3 subgroups (n=3) according to the surface treatment: N=no treatment; P=polished; and G=glazed. CIElab color coordinates were obtained relative to D65 on a reflection spectrophotometer. The translucency parameter (TP) and opalescence parameter (OP) were calculated. One specimen per subgroups I and V was selected for evaluation of surface roughness (Ra) and was examined with scanning electron microscopy (SEM). Data were analyzed with 2-way ANOVA and pairwise comparisons (α=.05). Statistical powers were verified to evaluate results (α=.05). RESULTS: The interaction effects of surface treatments combined with the number of colorings were significant for TP, OP, and Ra (P<.001), as follows: Ra=partial eta squared [ηp(2)]=.928; OP ηp(2)=.184; and TP ηp(2)=.144. No significant differences between TP were found among surface treatments in most groups (P>.05), whereas glazing significantly decreased OP and Ra in most groups. SEM images demonstrated that surface treatments affected the surface texture of monolithic zirconia ceramics. CONCLUSIONS: Surface treatments combined with coloring strongly affect the surface texture of dental monolithic zirconia ceramics.

Effect of various intermediate ceramic layers on the interfacial stability of zirconia core and veneering ceramics.

OBJECTIVES: The purposes of this study were to evaluate the effects of intermediate ceramics on the adhesion between the zirconia core and veneer ceramics. MATERIALS AND METHODS: The polished surfaces of fully sintered Y-TZP blocks received three different treatments: (1) connector (C), (2) liner (L) or (3) wash layer (W). All the treated zirconia blocks were veneered with either (a) fluorapatite glass-ceramic (E) or (b) feldspathic porcelain (V) and divided into four groups (CE, CV, LE and WV). For the control group, the testing surfaces of metal blocks were veneered with feldspathic porcelain (VM). A half of the samples in each group (n = 21) were exposed to thermocycling, while the other half of the specimens were stored at room temperature under dry conditions. All specimens were subjected to the shear test and the failed surfaces were microscopically examined. The elemental distribution at the zirconia core/veneer interface was analyzed. RESULTS: The specimens in Groups CE and CV exhibited significantly greater mean bond strength values than those in Groups LE and WV, respectively (p < 0.05). However, the mean bond strengths significantly decreased in the connector groups (CE and CV) after thermal cycling (p < 0.05). The elemental analysis suggested diffusion of ceramic substances into the zirconia surface. CONCLUSIONS: A glass-ceramic based connector is significantly more favorable to core/veneer adhesion than the other intermediate ceramics evaluated in the study. However, thermal cycling affected the bond strength at the core/veneer interface differently according to the intermediate ceramics.

Clinical outcomes of magnesium-incorporated oxidised implants: a randomised double-blind clinical trial.

OBJECTIVES: This study evaluated implant stability and clinical outcomes obtained with magnesium-incorporated oxidised implants (Mg titanate) and compared them to those blasted magnesium-incorporated oxidised implants (blasted Mg titanate). PATIENTS AND METHODS: Mg titanate was manufactured using the microarc oxidation (MAO) process. To obtain blasted Mg titanate, the MAO process was performed after blasting with TiO2 particles. The 15-month, randomised, double -blind clinical trial was conducted on 54 implants in 40 patients (Mg titanate, 27 implants in 18 subjects; blasted Mg titanate, 27 implants in 22 subjects), in whom 4.0 mm × 10 mm implants were placed to restore the unilateral loss of one or two molars in the mandible. The final prosthesis was attached 3 months postoperatively. Implant stability was measured by the implant stability quotient (ISQ) and periotest value (PTV) at the time of implant insertion, and 2, 3, and 15 months postoperatively. Marginal bone loss was evaluated at 2, 6, and 15 months postoperatively. Soft tissue analysis was performed at 15 months postoperatively. RESULTS: Both implant systems showed high stability at all time points (>71). Mean marginal bone loss was 0.71 ± 0.65 mm and 0.75 ± 0.73 after 15 months in Mg titanate and blasted Mg titanate, respectively. There were no significant differences between the two implant surfaces with respect to ISQ(P = 0.988), PTV(P = 0.935), and marginal bone loss(P = 0.807) after 15 months. CONCLUSION: The success rate after 1 year of follow-up was 100% for both magnesium-incorporated oxidised implants. There were no significant differences in the clinical outcomes between the two surfaces at 15 months follow-up.

Bone formation around zirconia implants combined with rhBMP-2 gel in the canine mandible.

OBJECTIVE: The aim of this study was to estimate the effects of zirconia implants and recombinant human bone morphogenetic protein-2 (rhBMP-2) gel on the acceleration of local bone formation and osseointegration in the canine mandible. MATERIALS AND METHODS: Four groups of 48 implants with identical geometry were installed in the mandibles of beagle dogs: alumina-blasted zirconia implants applied with rhBMP-2, alumina-blasted zirconia implants applied with demineralized bone matrix (DBM), alumina-blasted zirconia implants, and resorbable blast media-treated titanium (Ti) implants. For the first two groups, zirconia implants were inserted after the surgical sites were filled with rhBMP-2 or DBM gel. For the other two groups, zirconia or Ti implants were installed with no adjunctive treatment. Fluorescent bone markers were administered to monitor bone remodeling at weeks 2, 4, and 5 postimplantation. After healing periods of 3 weeks and 6 weeks, the animals were sacrificed, and fluorescent microscopy, histology, and histomorphometric analyses were performed. RESULTS: Fluorescent microscopy showed that bone formation around the zirconia implants installed with rhBMP-2 gel was the most prominent at 2 weeks postimplantation, while the Ti implants acquired bone apposition mainly at week 5. No significant differences were found in bone area among the groups (P > 0.05). The zirconia implants showed similar bone-to-implant contact to the Ti implants. There were no significant differences in bone-to-implant contact between the zirconia implants with rhBMP-2 gel and those with DBM (P > 0.05). CONCLUSIONS: The zirconia implants with alumina-blasted surfaces may achieve osseointegration in much the same manner as the well-established Ti implants. The area influenced by rhBMP-2 gel, including the alveolar crest, may cause active remodeling and early bone formation.

The development of quantitative methods using virtual models for the measurement of tooth wear.

Tooth wear is an unavoidable process associated with aging. Currently, virtual three-dimensional dental models are widely used and provide an advantage for studying tooth wear. However, there are no wear assessment parameters using virtual tooth models for the quantitative analysis of wear. Therefore, the aim of this study is to develop and evaluate quantitative wear measurement parameters. Ninety maxillary and mandibular dental casts were prepared and rendered as virtual three-dimensional models. For qualitative wear scoring, Hooper's new tooth wear index (NTWI) was used. For quantitative wear measurement, virtual vectors and occlusal planes were generated with reference points. Angles, height, and distance parameters were measured from reference points, vectors or planes. Intra- and interobserver reproducibility was determined for NTWI scoring and quantitative measurements. Quantitatively measurements for all parameters were subgrouped according to age groups and NTWI score groups. The mean and standard deviation were calculated for each group. One-way analysis of variance (ANOVA) test and the coefficients test were performed on the groups. Overall, intra- and interobserver reproducibility was good for both qualitative and quantitative measurement. In the ANOVA test, angle and height parameters showed significant differences between groups, whereas distance parameters did not. Similar results were observed in the coefficients test. However, plane heights and lingual side measurement parameters of the mandible are not recommended. In conclusion, this study indicates that all angle or height parameters of the maxilla and angle or vector height parameters of the buccal side of the mandible can be used as meaningful parameters in a quantitative wear study.

Variation in the total lengths of abutment/implant assemblies generated with a function of applied tightening torque in external and internal implant-abutment connection.

AIM: Settling (embedment relaxation), which is the main cause for screw loosening, is developed by microroughness between implant and abutment metal surface. The objective of this study was to evaluate and compare the relationship between the level of applied torque and the settling of abutments into implants in external and internal implant-abutment connection. MATERIAL AND METHODS: Five different implant-abutment connections were used (Ext, External butt joint + two-piece abutment; Int-H2, Internal hexagon + two-piece abutment; Int-H1, Internal hexagon + one-piece abutment; Int-O2, Internal octagon + two-piece abutment; Int-O1, Internal octagon + one-piece abutment). All abutments of each group were assembled and tightened with corresponding implants by a digital torque gauge. The total lengths of implant-abutment samples were measured at each torque (5, 10, 30 N cm and repeated 30 N cm with 10-min interval) by an electronic digital micrometer. The settling values were calculated by changes between the total lengths of implant-abutment samples. RESULTS: All groups developed settling with repeated tightening. The Int-H2 group showed markedly higher settling for all instances of tightening torque and the Ext group was the lowest. Statistically significant differences were found in settling values between the groups and statistically significant increases were observed within each group at different tightening torques (P<0.05). After the second tightening of 30 N cm, repeated tightening showed almost constant settling values. CONCLUSIONS: Results from the present study suggested that to minimize the settling effect, abutment screws should be retightened at least twice at 30 N cm torque at a 10-min interval in all laboratory and clinical procedures.

A randomized clinical 1-year trial comparing two types of non-submerged dental implants.

OBJECTIVES: This study compared the implant stability and clinical outcomes obtained with two types of non-submerged dental implants that have different thread designs and surface treatments. MATERIALS AND METHODS: A randomized clinical trial with 1 year of follow-up was performed on 56 participants with 75 implants (control group, 36 implants in 28 subjects; experimental group, 39 implants in 28 subjects). The experimental group received the Osstem SSII Implant system; the control group received the Standard Straumann Dental Implant System. The diameter and length of the fixture were uniform at 4.1 mm and 10 mm and all the implants restored the unilateral loss of one or two molars from the mandible. To compare implant stability, the peak insertion torque, implant stability quotient (ISQ), and periotest value (PTV) were evaluated during surgery, and at 4 and 10 weeks after surgery. To compare marginal bone loss, standard periapical radiographs were obtained during surgery, and at 10 weeks and 1 year after surgery. RESULTS: This study showed statistically significant differences between the two groups in peak insertion torque (P=0.009) and ISQ (P=0.003) but not in PTV (P=0.097) at surgery. In contrast, there was no statistically significant difference in the pattern of change of ISQ during the 10 weeks after surgery (P=0.339). For marginal bone loss, no significant difference was observed between the control and the experimental groups before functional loading (P=0.624), but after 1 year of follow-up, a borderline difference was observed (P=0.048). CONCLUSION: The success rate after 1 year of follow-up was 100% for both implant system despite the presence of a significant difference in implant stability during surgery. There was a borderline difference in marginal bone loss after 1 year of follow-up.

Application of Monolithic Zirconia Ceramics in Dental Practice: A Case History Report.

Monolithic zirconia restorations increasingly have been used in dental practice in recent years and demonstrate superior mechanical performance compared with porcelain-veneered zirconia restorations. Recent advances in manufacturing technology have made possible the fabrication of translucent monolithic zirconia ceramics. This case report describes three clinical examples of monolithic zirconia fixed dental prostheses being used in the anterior and posterior regions and exhibiting acceptable esthetic results.

Effect of the amount of thickness reduction on color and translucency of dental monolithic zirconia ceramics.

PURPOSE: This study investigated the effect of amount of thickness reduction on color and translucency of dental monolithic zirconia ceramics. MATERIALS AND METHODS: One-hundred sixty-five monolithic zirconia specimens (16.3 mm × 16.3 mm × 2.0 mm) were divided into 5 groups (Group I to V) according to the number of A2-coloring liquid applications. Each group was then divided into 11 subgroups by reducing the thickness up to 1.0 mm in 0.1-mm increments (Subgroup 0 to 10, n=3). Colors and spectral distributions were measured according to CIELAB on a reflection spectrophotometer. All measurements were performed on five different areas of each specimen. Color difference (ΔE(*) ab) and translucency parameter (TP) were calculated. Data were analyzed using one-way ANOVA and multiple comparison Scheffé test (α=.05). RESULTS: There were significant differences in CIE L(*) between Subgroup 0 and other subgroups in all groups. CIE a(*) increased (0.523.7) were obtained between Subgroup 0 and other subgroups. TP values generally increased as the thickness reduction increased in all groups (R(2)>0.89, P<.001). CONCLUSION: Increasing thickness reduction reduces lightness and increases a reddish, bluish appearance, and translucency of monolithic zirconia ceramics.

A root submergence technique for pontic site development in fixed dental prostheses in the maxillary anterior esthetic zone.

PURPOSE: This case report discusses the effect of a root submergence technique on preserving the periodontal tissue at the pontic site of fixed dental prostheses in the maxillary anterior aesthetic zone. METHODS: Teeth with less than ideal structural support for fixed retainer abutments were decoronated at the crestal bone level. After soft tissue closure, the final fixed dental prostheses were placed with the pontics over the submerged root area. Radiographic and clinical observations at the pontic sites were documented. RESULTS: The submerged roots at the pontic sites preserved the surrounding periodontium without any periapical pathology. The gingival contour at the pontic site was maintained in harmony with those of the adjacent teeth, as well as the overall form of the arch. CONCLUSIONS: The results of this clinical report indicate that a root submergence technique can be successfully applied in pontic site development with fixed dental prostheses, especially in the maxillary anterior esthetic zone.

Measuring abutment convergence angles using stereovision dental image processing system.

PURPOSE: The purpose of this study was to develop a dental image processing system using a three-dimensional (3D) camera and stereovision technology. The reliability of the system for measuring axial wall convergence angles was evaluated. MATERIALS AND METHODS: The new system predicted 3D coordinate points from 2D images and calculated distances and angles between points. Two examiners measured axial wall convergence angles for seven artificial abutments using a traditional tracing-based method (TBM) and the stereovision-based method (SVBM). Five wax abutment models of simplified abutment forms were made and axial wall convergence angles of wax models were measured by both methods. The data were statistically analyzed at the level of significance, 0.05. RESULTS: Intraclass correlation coefficients showed excellent intra-examiner and inter-examiner reliabilities for both methods. Bland-Altman plots and paired t-tests showed significant differences between measurements and true values using TBM; differences were not significant with SVBM. CONCLUSION: This study found that the SVBM reflected true angle values more accurately than a TMB and illustrated an example of 3D computer science applied to clinical dentistry.

The reliability of an easy measuring method for abutment convergence angle with a computer-aided design (CAD) system.

PURPOSE: The purpose of this study was to evaluate the intra-rater reliability and inter-rater reliability of three different methods using a drawing protractor, a digital protractor after tracing, and a CAD system. MATERIALS AND METHODS: Twenty-four artificial abutments that had been prepared by dental students were used in this study. Three dental students measured the convergence angles by each method three times. Bland-Altman plots were applied to examine the overall reliability by comparing the traditional tracing method with a new method using the CAD system. Intraclass Correlation Coefficients (ICC) evaluated intra-rater reliability and inter-rater reliability. RESULTS: All three methods exhibited high intra-rater and inter-rater reliability (ICC>0.80, P<.05). Measurements with the CAD system showed the highest intra-rater reliability. In addition, it showed improved inter-rater reliability compared with the traditional tracing methods. CONCLUSION: Based on the results of this study, the CAD system may be an easy and reliable tool for measuring the abutment convergence angle.

Effect of surface treatment and liner material on the adhesion between veneering ceramic and zirconia.

Fully sintered zirconia blocks, each with one polished surface, were treated with one of the followings: 1) no treatment, 2) airborne-particle abrasion with 50µm alumina, and 3) airborne-particle abrasion with 125µm alumina. Before veneering with glass ceramic, either liner Α or liner B were applied on the treated surfaces. All veneered blocks were subjected to shear force in a universal testing machine. For the groups with liner A, irrespective of the particle size, air abrasion on Y-TZP surfaces provided greater bond strength than polishing. Application of liner B on an abraded zirconia surface yielded no significant influence on the adhesion. In addition, specimens with liner A showed higher bond strength than those with liner B, if applied on roughened surfaces. Fractured surfaces were observed as mixed patterns in all groups. For the liner A, surface treatment was helpful in bonding with veneering ceramic, while it was ineffective for the liner B.

Marginal fit of anterior 3-unit fixed partial zirconia restorations using different CAD/CAM systems.

PURPOSE: Few studies have investigated the marginal accuracy of 3-unit zirconia fixed partial dentures (FPDs) fabricated by computer-aided design/computer-aided manufacturing (CAD/CAM) system. The purpose of this study was to compare the marginal fit of zirconia FPDs made using two CAD/CAM systems with that of metal-ceramic FPDs. MATERIALS AND METHODS: Artificial resin maxillary central and lateral incisors were prepared for 3-unit FPDs and fixed in yellow stone. This model was duplicated to epoxy resin die. On the resin die, 15 three-unit FPDs were fabricated per group (45 in total): Group A, zirconia 3-unit FPDs made with the Everest system; Group B, zirconia 3-unit FPDs made with the Lava system; and Group C, metal-ceramic 3-unit FPDs. They were cemented to resin dies with resin cement. After removal of pontic, each retainer was separated and observed under a microscope (Presize 440C). Marginal gaps of experimental groups were analyzed using one-way ANOVA and Duncan test. RESULTS: Mean marginal gaps of 3-unit FPDs were 60.46 µm for the Everest group, 78.71 µm for the Lava group, and 81.32 µm for the metal-ceramic group. The Everest group demonstrated significantly smaller marginal gap than the Lava and the metal-ceramic groups (P<.05). The marginal gap did not significantly differ between the Lava and the metal-ceramic groups (P>.05). CONCLUSION: The marginal gaps of anterior 3-unit zirconia FPD differed according to CAD/CAM systems, but still fell within clinically acceptable ranges compared with conventional metal-ceramic restoration.

Comparative fracture strength analysis of Lava and Digident CAD/CAM zirconia ceramic crowns.

PURPOSE: All-ceramic crowns are subject to fracture during function. To minimize this common clinical complication, zirconium oxide has been used as the framework for all-ceramic crowns. The aim of this study was to compare the fracture strengths of two computer-aided design/computer-aided manufacturing (CAD/CAM) zirconia crown systems: Lava and Digident. MATERIALS AND METHODS: Twenty Lava CAD/CAM zirconia crowns and twenty Digident CAD/CAM zirconia crowns were fabricated. A metal die was also duplicated from the original prepared tooth for fracture testing. A universal testing machine was used to determine the fracture strength of the crowns. RESULTS: THE MEAN FRACTURE STRENGTHS WERE AS FOLLOWS: 54.9 ± 15.6 N for the Lava CAD/CAM zirconia crowns and 87.0 ± 16.0 N for the Digident CAD/CAM zirconia crowns. The difference between the mean fracture strengths of the Lava and Digident crowns was statistically significant (P<.001). Lava CAD/CAM zirconia crowns showed a complete fracture of both the veneering porcelain and the core whereas the Digident CAD/CAM zirconia crowns showed fracture only of the veneering porcelain. CONCLUSION: The fracture strengths of CAD/CAM zirconia crowns differ depending on the compatibility of the core material and the veneering porcelain.

The influence of various core designs on stress distribution in the veneered zirconia crown: a finite element analysis study.

PURPOSE: The purpose of this study was to evaluate various core designs on stress distribution within zirconia crowns. MATERIALS AND METHODS: Three-dimensional finite element models, representing mandibular molars, comprising a prepared tooth, cement layer, zirconia core, and veneer porcelain were designed by computer software. The shoulder (1 mm in width) variations in core were incremental increases of 1 mm, 2 mm and 3 mm in proximal and lingual height, and buccal height respectively. To simulate masticatory force, loads of 280 N were applied from three directions (vertical, at a 45° angle, and horizontal). To simulate maximum bite force, a load of 700 N was applied vertically to the crowns. Maximum principal stress (MPS) was determined for each model, loading condition, and position. RESULTS: In the maximum bite force simulation test, the MPSs on all crowns observed around the shoulder region and loading points. The compressive stresses were located in the shoulder region of the veneer-zirconia interface and at the occlusal region. In the test simulating masticatory force, the MPS was concentrated around the loading points, and the compressive stresses were located at the 3 mm height lingual shoulder region, when the load was applied horizontally. MPS increased in the shoulder region as the shoulder height increased. CONCLUSION: This study suggested that reinforced shoulder play an essential role in the success of the zirconia restoration, and veneer fracture due to occlusal loading can be prevented by proper core design, such as shoulder.

Initial in vitro bacterial adhesion on dental restorative materials.

OBJECTIVES: The purpose of this study was to evaluate initial bacterial adhesion on several restorative materials with similar roughness. MATERIALS AND METHODS: Sixty cylindrical slabs were prepared from four restorative materials: zirconia (Zr), alumina-toughened zirconia (Al-Zr), type III gold alloy (Au), and cp-titanium (Ti). All the materials were polished until a mirror-like shine was achieved. The average surface roughness and topography were determined by atomic force microscopy. Contact angles were measured to calculate surface free energy by the sessile drop technique. After the formation of a salivary pellicle, S. sanguinis, S. gordonii, and S. oralis were inoculated onto the specimens and incubated for 4 h. Quantification of the adherent bacteria was performed by crystal violet staining technique and resazurin reduction assay. One-way ANOVA and Tukey's post hoc test were adopted for statistical analysis. The level of significance was 0.05. RESULTS: The Ra values determined with atomic force microscopy for all specimens were lower than 5 nm. Surface free energy increased in the order of Al-Zr, Zr, Ti, and Au. Differences were significant between the investigated materials in both crystal violet absorbance and fluorescence intensities. Gold alloy showed the highest values for all bacterial strains (p<0.05). CONCLUSIONS: Zirconia, alumina-toughened zirconia, and titanium may be more suitable than gold alloy as an abutment material with respect to the initial bacterial adhesion and subsequent advance of peri-implantitis.

In vitro evaluation of fracture strength of zirconia restoration veneered with various ceramic materials.

PURPOSE: Fracture of the veneering material of zirconia restorations frequently occurs in clinical situations. The purpose of this in vitro study was to compare the fracture strengths of zirconia crowns veneered with various ceramic materials by various techniques. MATERIALS AND METHODS: A 1.2 mm, 360° chamfer preparation and occlusal reduction of 2 mm were performed on a first mandibular molar, and 45 model dies were fabricated in a titanium alloy by CAD/CAM system. Forty-five zirconia copings were fabricated and divided into three groups. In the first group (LT) zirconia copings were veneered with feldspathic porcelain by the layering technique. In the second group (HT) the glass ceramic was heat-pressed on the zirconia coping, and for the third group (ST) a CAD/CAM-fabricated high-strength anatomically shaped veneering cap was sintered onto the zirconia coping. All crowns were cemented onto their titanium dies with Rely X™ Unicem (3M ESPE) and loaded with a universal testing machine (Instron 5583) until failure. The mean fracture values were compared by an one-way ANOVA and a multiple comparison post-hoc test (α=0.05). Scanning electron microscope was used to investigate the fractured interface. RESULTS: Mean fracture load and standard deviation was 4263.8±1110.8 N for Group LT, 5070.8±1016.4 for Group HT and 6242.0±1759.5 N for Group ST. The values of Group ST were significantly higher than those of the other groups. CONCLUSION: Zirconia crowns veneered with CAD/CAM generated glass ceramics by the sintering technique are superior to those veneered with feldspathic porcelain by the layering technique or veneered with glass ceramics by the heat-pressing technique in terms of fracture strength.

The effect of preparation order on the crystal structure of yttria-stabilized tetragonal zirconia polycrystal and the shear bond strength of dental resin cements.

OBJECTIVES: The purpose of this study was to evaluate the effect of preparation order on the crystal structure of yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) and the shear bond strength of dental resin cements. METHODS: One-hundred fifty pre-sintered Y-TZP cylinders (Ø 9mm×13.5mm) were prepared and divided into three groups (control group, SBS group and SAS group). Specimens in control group were not treated. Specimens in SBS group were sandblasted and then densely sintered, and specimens in SAS group were sintered in advance, and then sandblasted. The specimens were analyzed by X-ray diffractometry, confocal laser scanning microscopy and Energy dispersive X-ray spectroscopy before and after sandblasting. All specimens were embedded in polytetrafluoroethylene (PTFE) molds using PMMA and each group was divided into five subgroups. The mixed resin cements (Clearfil SA luting cement, Zirconite, Superbond C&B, Rely-X Unicem, and Multilink) were placed onto the Y-TZP surfaces using PTFE molds with Ø 3mm×3mm, followed by storage in distilled water at 37°C for 24h, and thermocycling (5000 cycles at 5°C and 55°C with a 30s dwelling time). All specimens were tested for the shear bond strengths with a universal testing machine, and fractured surfaces were evaluated by SEM. Statistical analysis was performed using one-way ANOVA and Scheffé comparison with α=.05. RESULTS: Sandblasting of the zirconia significantly increased shear bond strength of resin cements, but the preparation order had no significant influence on the shear bond strength in both test groups. In SEM observation, the natures of the surface faceting of the zirconia grains were totally different between SBS and SAS groups. SBS group exhibited less monoclinic structures than SAS group. SIGNIFICANCE: Sandblasting of pre-sintered Y-TZP and then sintering may induce favorable proportion of tetragonal structures. This might have positive effect on the clinical performance of zirconia restorations.

Effect of sandblasting and various metal primers on the shear bond strength of resin cement to Y-TZP ceramic.

OBJECTIVES: This study was designed to evaluate the effect of sandblasting and metal primers on the shear bond strength of three commercial resin cements to Yttria-Tetragonl Zirconia Polycrystal (Y-TZP) ceramics. METHODS: One hundred and twenty Y-TZP ceramic cylinders (Ø7 mm x 12 mm) were embedded in polytetrafluoroethylene (PTFE) molds using PMMA. The specimens were divided randomly into 12 groups (n=10), according to the surface treatments (control; sandblast-only; metal primer-only; sandblast+metal primer) and metal primer-resin cements (Alloy primer - Panavia F 2.0, V-primer - Superbond C&B, Metaltite - M bond) rendered. The mixed resin cements were placed onto the treated zirconia surfaces in cylindrical shape (Ø3 mm x 3 mm) using PTFE molds. All specimens were thermocycled (5 and 55 degrees C, 5000 cycles) and subjected to shear bond strength test by a universal testing machine with a crosshead speed of 0.5 mm/min. All data were statistically analyzed using two-way ANOVA and multiple comparison Scheffé test (alpha=0.05), and SEM images of the fractured areas were used to evaluate the fracture mode. RESULTS: In Panavia F 2.0, the bond strength of the specimens treated with sandblasting and metal primer (Alloy primer) was significantly higher than those of the other subgroups. In Superbond C&B and M bond, sandblasting significantly increased the shear bond strength, but the effect of metal primers (V-primer and Metaltite) was not significant and there was disordinal interaction. SIGNIFICANCE: Metal primers are not always effective for bonding between Y-TZP ceramics and resin cements. Even though a metal primer is not enough to be used alone, combined application with sandblasting seems to be an appropriate pretreatment for improving the bond strength of resin cement to Y-TZP ceramics, especially in Panavia F 2.0.