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Tf₂O as a CF₃ Source for the Synthesis of Trifluoromethoxylation Reagent ⁿC₄F₉SO₃CF₃.

Chen, Ling-Ying; Pan, Peng-Fei; Lin, Jin-Hong; Jin, Chuan-Ming; Xiao, Ji-Chang.

J Org Chem ; 88(5): 3346-3352, 2023 Mar 03.

Article in English | MEDLINE | ID: mdl-36763542

ABSTRACT

Described herein is the convenient synthesis of an efficient trifluoromethoxylation reagent, nC4F9SO3CF3, by using cheap and widely available reagents and without the need of any tedious column chromatography purification procedure.

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