1.
Nanotechnology
; 24(5): 055702, 2013 Feb 08.
Artículo
en Inglés
| MEDLINE
| ID: mdl-23307038
RESUMEN
We have investigated the morphology and structure of dolomite MgCa(CO(3))(2)(104) surfaces by bimodal dynamic force microscopy with flexural and torsional resonance modes in ultra-high vacuum at room temperature. We found that the surface slowly decomposes by degassing CO(2) in a vacuum and becomes covered by amorphous clusters, presumably MgO and CaO. By choosing an optimal sample preparation procedure (i.e. cleaving in a vacuum and mild annealing for stabilizing clusters for a short time), atomically clean surfaces were obtained. The complex tip-sample interaction, arising from carbonate groups and Mg and Ca atoms of the surface, induces a large variety of atomic-scale imaging features.