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Nickel-catalyzed regioselective hydrogen isotope exchange accelerated by 2-pyridones.
Jiang, Zhi-Jiang; Xu, Si-Han; Su, Yuhang; Hu, Erxun; Han, Jiawei; Bai, Jian-Fei; Tang, Bencan; Chen, Jia; Gao, Zhanghua.
Affiliation
  • Jiang ZJ; NingboTech-Cuiying Joint Laboratory of Stable Isotope Technology, School of Biological and Chemical Engineering, NingboTech University, Ningbo, 315100, P. R. China. zj.jiang@nbt.edu.cn.
  • Xu SH; NingboTech-Cuiying Joint Laboratory of Stable Isotope Technology, School of Biological and Chemical Engineering, NingboTech University, Ningbo, 315100, P. R. China. zj.jiang@nbt.edu.cn.
  • Su Y; School of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, P. R. China.
  • Hu E; NingboTech-Cuiying Joint Laboratory of Stable Isotope Technology, School of Biological and Chemical Engineering, NingboTech University, Ningbo, 315100, P. R. China. zj.jiang@nbt.edu.cn.
  • Han J; School of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, P. R. China.
  • Bai JF; NingboTech-Cuiying Joint Laboratory of Stable Isotope Technology, School of Biological and Chemical Engineering, NingboTech University, Ningbo, 315100, P. R. China. zj.jiang@nbt.edu.cn.
  • Tang B; NingboTech-Cuiying Joint Laboratory of Stable Isotope Technology, School of Biological and Chemical Engineering, NingboTech University, Ningbo, 315100, P. R. China. zj.jiang@nbt.edu.cn.
  • Chen J; School of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, P. R. China.
  • Gao Z; NingboTech-Cuiying Joint Laboratory of Stable Isotope Technology, School of Biological and Chemical Engineering, NingboTech University, Ningbo, 315100, P. R. China. zj.jiang@nbt.edu.cn.
Chem Commun (Camb) ; 60(4): 384-387, 2024 Jan 04.
Article in En | MEDLINE | ID: mdl-38063024
ABSTRACT
A nickel-catalyzed hydrogen isotope exchange has been developed with acetone-d6 as the deuterium source. The reaction showed an improved kinetic feature of H/D exchange under the assistance of 2-pyridones, efficiently affording regioselective labeled aryl and alkyl carboxamides.
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: Chem Commun (Camb) Journal subject: QUIMICA Year: 2024 Type: Article
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: Chem Commun (Camb) Journal subject: QUIMICA Year: 2024 Type: Article