Rapid and sensitive multiresidue analysis of pesticides in tobacco using low pressure and traditional gas chromatography tandem mass spectrometry.
J Chromatogr A
; 1418: 228-232, 2015 Oct 30.
Article
en En
| MEDLINE
| ID: mdl-26431856
ABSTRACT
Public exposure to pesticide residues through the main/side-stream smoke of tobacco (Nicotiana tabacum L.) is an international concern. This article reports optimization and validation of large-scale multiresidue analysis methods involving low pressure and traditional gas chromatography tandem mass spectrometry in compliance with the guidance residue levels (GRLs) of Cooperative Centre for Scientific Research Relative to Tobacco (CORESTA). Analysis by low pressure GC-MS/MS offered three times rapid turn around time over the traditional GC-MS/MS with limits of quantifications (LOQs) less than 2µg/L for all the 259 test compounds and the recoveries in the range of 70-118% (±20%) at 10 and 20µg/kg levels of fortification.
Palabras clave
Texto completo:
1
Colección:
01-internacional
Banco de datos:
MEDLINE
Asunto principal:
Humo
/
Nicotiana
/
Residuos de Plaguicidas
Tipo de estudio:
Diagnostic_studies
Idioma:
En
Revista:
J Chromatogr A
Año:
2015
Tipo del documento:
Article
País de afiliación:
India