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A device for the application of uniaxial strain to single crystal samples for use in synchrotron radiation experiments.
Gannon, L; Bosak, A; Burkovsky, R G; Nisbet, G; Petrovic, A P; Hoesch, M.
Afiliación
  • Gannon L; Clarendon Laboratory, University of Oxford Physics Department, Parks Road, Oxford OX1 3PU, United Kingdom.
  • Bosak A; European Synchrotron Radiation Facility, BP 220, F-38043 Grenoble Cedex, France.
  • Burkovsky RG; European Synchrotron Radiation Facility, BP 220, F-38043 Grenoble Cedex, France.
  • Nisbet G; Diamond Light Source, Harwell Science and Innovation Campus, Didcot OX11 ODE, United Kingdom.
  • Petrovic AP; DPMC-MaNEP, Université de Genève, Quai Ernest-Ansermet 24, 1211 Genève 4, Switzerland.
  • Hoesch M; Diamond Light Source, Harwell Science and Innovation Campus, Didcot OX11 ODE, United Kingdom.
Rev Sci Instrum ; 86(10): 103904, 2015 Oct.
Article en En | MEDLINE | ID: mdl-26520968
We present the design, construction, and testing of a straining device compatible with many different synchrotron radiation techniques, in a wide range of experimental environments (including low temperature, high field and ultra-high vacuum). The device has been tested by X-ray diffraction on single crystal samples of quasi-one-dimensional Cs2Mo6Se6 and K2Mo6Se6, in which microscopic strains up to a Δc/c = 0.12% ± 0.01% change in the c lattice parameters have been achieved. We have also used the device in an inelastic X-ray scattering experiment, to probe the strain-dependent speed of sound ν along the c axis. A reduction Δν/ν of up to -3.8% was obtained at a strain of Δc/c = 0.25% in K2Mo6Se6.

Texto completo: 1 Colección: 01-internacional Banco de datos: MEDLINE Idioma: En Revista: Rev Sci Instrum Año: 2015 Tipo del documento: Article País de afiliación: Reino Unido

Texto completo: 1 Colección: 01-internacional Banco de datos: MEDLINE Idioma: En Revista: Rev Sci Instrum Año: 2015 Tipo del documento: Article País de afiliación: Reino Unido