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1.
Am J Dent ; 31(6): 303-308, 2018 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-30658376

RESUMO

PURPOSE: To investigate the effects of whitening toothpastes over the wear and surface roughness of ormocer and methacrylate composites. METHODS: Cylindrical specimens (n=120) were prepared using methacrylate-based composites (Filtek Z350 XT, TPH3 and GrandioSO) and a pure-ormocer composite (Admira Fusion). Brushing abrasion (100,000 strokes) was performed using whitening toothpastes containing different abrasives: alumina (Colgate Ultrawhite), perlite (CloseUp Whitening) and sodium bicarbonate (Kin Progressive Whitening). Wear and roughness alteration were evaluated. Additional analyses of microhardness, degree of conversion and scanning electron microscopy were also performed. RESULTS: Data were separately analyzed with Kruskal-Wallis and ANOVA tests. Statistically significant differences were found for the composites and whitening toothpastes (P<0.05). For all toothpastes, GrandioSO showed lower wear than Z350 XT and Admira Fusion, although non-significant differences in relation to TPH3 were observed. For perlite and bicarbonate-based toothpastes, Z350 XT, Admira Fusion and TPH3 did not present significant differences among them for wear. For alumina-based toothpaste, Z350 XT showed higher wear than TPH3, while Admira Fusion showed intermediate values. Higher wear and roughness alteration were observed after using alumina-containing toothpaste. All composites tested showed increased roughness after brushing. Z350 XT presented the lowest roughness alteration, while Admira Fusion the highest. CLINICAL SIGNIFICANCE: The alumina-containing whitening toothpaste significantly increased the wear and roughness of composites in relation to the other abrasives tested. However, using the ADA standards, the wear promoted by all whitening toothpastes tested would be considered clinically acceptable for all materials. The type of organic matrix in a composite is not the main factor that determines the wear rate, but also its interaction with the inorganic fillers and the filler content. The composite GrandioSO showed the lowest overall wear values, while Z350 XT resulted in the smoothest surfaces.


Assuntos
Metacrilatos , Cerâmicas Modificadas Organicamente , Cremes Dentais , Teste de Materiais , Propriedades de Superfície , Escovação Dentária
2.
J Adhes Dent ; 19(2): 121-127, 2017.
Artigo em Inglês | MEDLINE | ID: mdl-28439576

RESUMO

PURPOSE: To evaluate the influence of previous acid etching on the bond strength of a self-etch universal adhesive system on sound and eroded enamel and dentin. MATERIALS AND METHODS: Flat enamel and dentin surfaces were obtained from bovine incisors (n = 44) and divided into two groups according to the exposure to erosive conditions: sound (without erosion) and eroded (after erosive challenge with 0.3% citric acid, pH 2.6, 5 min, 4x/day, 5 days). Each group was then divided into two subgroups (n = 11) according to the application or not of 37% phosphoric acid before applying a universal self-etch adhesive. Single Bond universal adhesive (3M ESPE) was applied and composite blocks were built up using Amelogen Plus (Ultradent). Sticks (1 × 1 mm) were obtained and the microtensile bond strength (µTBS) was assessed using a universal testing machine at a speed of 1 mm/min. Data were analyzed with two-way ANOVA and Tukey's tests (p < 0.05). RESULTS: For enamel groups, significant differences were observed for erosive challenge (p = 0.034) and acid etching (p = 0.047), but not for the interaction between them (p = 0.182). The means ±â€¯SD (MPa) for the erosive conditions were: sound, 25.02 ±â€¯5.82a; eroded, 28.45 ±â€¯5.92b; and for acid etching: without, 24.89 ±â€¯5.39a; with, 28.58 ±â€¯6.23b (different superscript letters indicate significant differences). For dentin, both the erosive condition (p = 0.936) and acid pretreatment (p = 0.084), as well as their interaction (p = 0.107), did not affect the bond strength. CONCLUSION: The erosive challenge and previous acid etching significantly increased the bond strength of the tested universal adhesive to enamel but not to dentin.


Assuntos
Condicionamento Ácido do Dente , Colagem Dentária , Animais , Bovinos , Resinas Compostas , Cimentos Dentários , Esmalte Dentário , Dentina , Adesivos Dentinários , Teste de Materiais , Cimentos de Resina , Resistência à Tração
3.
J Adhes Dent ; 18(1): 43-50, 2016.
Artigo em Inglês | MEDLINE | ID: mdl-26814318

RESUMO

PURPOSE: To evaluate the color masking effect of infiltration treatment of artificial white spot lesions (AWSL) using a dedicated resin in comparison to different adhesive systems. MATERIALS AND METHODS: Enamel/dentin specimens were obtained from bovine incisors and baseline color was assessed using a reflectance spectrophotometer, according to the CIE L*a*b* system. AWSL were produced using a buffered acid solution and a new color evaluation was performed. The specimens were divided into 8 groups: control: artificial saliva changed daily for 7 days; IC: infiltrating resin Icon; EC: EquiaCoat; FU: Futurabond U; SBU: Single Bond U; SBMP: Scotchbond MP; OB: OptibondFL; BF: Bioforty. After the treatments, the color was evaluated again and the values for the parameters ΔL (change in lightness), Δa (change in chroma), Δb (change in hue), and ΔE (general color difference) were calculated in relation to baseline. Data were analyzed by one-way ANOVA and Tukey's tests. RESULTS: After treatment, ANOVA showed significant differences for all parameters (p = 0.001). Tukey's test showed the greatest lightness reduction (ΔL) for the IC group, followed by EC, FU, and SBU. The SBMP, OB, and BF groups were similar to the control. For Δb values, all groups showed differences in relation to the control, with no differences between them. In relation to ΔE, all groups showed differences in relation to the control (ΔE = 5.24), with no significant differences between them. ΔE values after application of all resinous materials were lower than the threshold of 3.7, indicating effective color masking. CONCLUSIONS: The Icon infiltrant produced a greater lightness reduction of white lesions (ΔL). For general color difference (ΔE), all the resinous materials tested were able to color mask artificial AWSL.


Assuntos
Cárie Dentária/patologia , Cimentos de Resina/química , Animais , Bis-Fenol A-Glicidil Metacrilato/química , Bovinos , Cor , Esmalte Dentário/ultraestrutura , Dentina/ultraestrutura , Teste de Materiais , Metacrilatos/química , Metilmetacrilato/química , Poliuretanos/química , Refratometria , Resinas Sintéticas/química , Saliva Artificial/química , Espectrofotometria
4.
Am J Dent ; 29(5): 289-293, 2016 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-29178743

RESUMO

PURPOSE: To evaluate the bonding behavior of resin composite and different adhesives applied to demineralized or remineralized enamel. METHODS: Bovine tooth crowns were polished to prepare a 5 mm2 enamel bonding area, and divided into five groups (n= 48) according to the surface treatment: CONT (sound enamel control), DEM (demineralized with acid to create white spot lesions), REMS (DEM remineralized with artificial saliva), REMF (DEM remineralized with sodium fluoride) and INF (DEM infiltrated with Icon resin infiltrant). The surface-treated teeth were divided into two subgroups (n= 24) according to adhesive type: ER (etch-and-rinse; Single Bond Universal) and SE (self-etching; Clearfill S3 Bond), and further subdivided into two categories (n= 12) according to aging process: Thermo (thermocycling) and NA (no aging). Composite blocks were made over bonded enamel and sectioned for microtensile bond strength (MTBS) testing. Data were analyzed with three-way ANOVA and post-hoc Tukey's test (α= 0.05). RESULTS: Significant differences were observed for enamel surface treatment (P< 0.0001), adhesive type (P< 0.0001) and aging (P< 0.0001). CONT and INF groups had higher MTBS than the other groups; Single Bond Universal had higher MTBS than Clearfil S3 Bond; thermo-aging resulted in lower MTBS irrespective of adhesive type and surface treatment condition. The predominant failure mode was mixed for all groups. Enamel surface infiltrated with Icon does not interfere with adhesive resin bonding procedures. CLINICAL SIGNIFICANCE: Treatment of enamel surface containing white spot lesions or cavities with cavosurface margins in partially-demineralized enamel can benefit from infiltration with a low viscosity resin infiltrant prior to adhesive bonding of resin composites.


Assuntos
Resinas Compostas/química , Colagem Dentária , Esmalte Dentário/efeitos dos fármacos , Corrosão Dentária/métodos , Materiais Dentários/química , Desmineralização do Dente/patologia , Animais , Bovinos , Esmalte Dentário/ultraestrutura , Análise do Estresse Dentário , Teste de Materiais , Microscopia Eletrônica de Varredura , Propriedades de Superfície , Resistência à Tração , Remineralização Dentária
5.
J Mech Behav Biomed Mater ; 152: 106407, 2024 Apr.
Artigo em Inglês | MEDLINE | ID: mdl-38277911

RESUMO

OBJECTIVE: To evaluate the effect of a Nisin-based dentin pretreatment solution on microtensile bond strength, antibacterial activity, and matrix metalloproteinase (MMP) activity of the adhesive interface. MATERIALS AND METHODS: 100 human molars were sectioned to expose dentin. The teeth were assigned to five groups (n = 20), according to the dentin pretreatment: 0.5%, 1.0%, or 1.5% Nisin; 0.12% chlorhexidine (positive control), and no solution (negative control), and divided into 2 subgroups: no aging, and thermomechanical aging. Specimens were etched with 37% H3PO4 for 15 s and submitted to the dentin pretreatment. Then, they were bonded with an adhesive (Adper Single Bond 2) and a resin composite for microtensile bond strength (µTBS) evaluation. Antibacterial activity against Streptococcus mutans was qualitatively examined using an agar diffusion test. Anti-MMP activity within hybrid layers was examined using in-situ zymography. Data were analyzed with two-factor ANOVA and post-hoc Tukey's test (α = 0.050). RESULTS: For µTBS, significant differences were identified for the factors "solutions" (p = 0.002), "aging" (p = 0.017), and interaction of the two factors (p = 0.002). In the absence of aging, higher µTBS was observed for the group 0.5% Nisin. In the presence of aging, all groups showed similar µTBS values. All Nisin concentrations were effective in inhibiting the growth of S. mutans. Endogenous MMP activity was more significantly inhibited using 0.5% and 1.0% Nisin (p < 0.050). CONCLUSION: 0.5% and 1.0% Nisin solutions do not adversely affect resin-dentin bond strength and exhibit a potential bactericidal effect against S. mutans. Both concentrations effectively reduce endogenous gelatinolytic activity within the hybrid layer. CLINICAL RELEVANCE: The use of 0.5% and 1.0% Nisin solutions for dentin pretreatment potentially contributes to preserving the adhesive interface, increasing the longevity of composite restorations.


Assuntos
Colagem Dentária , Nisina , Humanos , Nisina/farmacologia , Nisina/análise , Adesivos/análise , Dentina/química , Antibacterianos/farmacologia , Resinas Compostas/química , Resistência à Tração , Adesivos Dentinários/química , Cimentos de Resina/análise , Teste de Materiais
6.
J Contemp Dent Pract ; 14(1): 14-20, 2013 Jan 01.
Artigo em Inglês | MEDLINE | ID: mdl-23579886

RESUMO

AIM: The aim of this study was to compare the microtensile bond strength of three adhesive systems, using different methods of dentin preparation. MATERIALS AND METHODS: A hundred and eight bovine teeth were used. The dentin from buccal face was exposed and prepared with three different methods, divided in 3 groups: Group 1 (DT)- diamond tip on a high-speed handpiece; Group 2 (CVD)-CVD tip on a ultrasonic handpiece; Group 3 (LA)-Er: YAG laser. The teeth were divided into 3 subgroups, according adhesive systems used: Subgroup 1-Adper Single Bond Plus/3M ESPE (SB) total-etch adhesive; Subgroup 2-Adper Scotchbond SE/3M ESPE (AS) selfetching adhesive; Subgroup 3-Clearfil SE Bond/Kuraray (CS) selfetching adhesive. Blocks of composite (Filtek Z250-3M ESPE) 4 mm high were built up and specimens were stored in deionized water for 24 hours at 37°C. Serial mesiodistal and buccolingual cuts were made and stick-like specimens were obtained, with transversal section of 1.0 mm(2). The samples were submitted to microtensile test at 1 mm/min and load of 10 kg in a universal testing machine. Data (MPa) were subjected to ANOVA and Tukey's tests (p < 0.05). RESULTS AND CONCLUSION: Surface treatment with Diamond or CVD tips associated with Clearfil SE Bond adhesive produced significantly lower bond strength values compared to other groups. Surface treatment with Er: YAG laser associated with Single Bond Plus or Clearfil SE Bond adhesives and surface treatment with CVD tip associated with Adper Scotchbond SE adhesive produced significantly lower bond strength values compared to surface treatment with diamond or CVD tips associated with Single Bond Plus or Adper Scotchbond SE adhesives. CLINICAL SIGNIFICANCE: Interactions between laser and the CVD tip technologies and the different adhesive systems can produce a satisfactory bonding strength result, so that these associations may be beneficial and enhance the clinical outcomes.


Assuntos
Colagem Dentária , Preparo da Cavidade Dentária/instrumentação , Adesivos Dentinários/química , Dentina/ultraestrutura , Diamante/química , Lasers de Estado Sólido/uso terapêutico , Animais , Bis-Fenol A-Glicidil Metacrilato/química , Bovinos , Resinas Compostas/química , Equipamentos Odontológicos de Alta Rotação , Análise do Estresse Dentário/instrumentação , Microscopia Eletrônica de Varredura , Distribuição Aleatória , Cimentos de Resina/química , Camada de Esfregaço , Estresse Mecânico , Propriedades de Superfície , Temperatura , Resistência à Tração , Fatores de Tempo , Ultrassom/instrumentação , Água/química
7.
Int J Dent ; 2023: 2182651, 2023.
Artigo em Inglês | MEDLINE | ID: mdl-37435112

RESUMO

This study aimed to evaluate Nd:YAG laser, calcium phosphate, and adhesive system effect as different pretreatments in different protocols on dentin permeability (DP) and bond strength (BS). Fifty human dentin discs were used (4 mm in diameter and 1,5 mm in height). Specimens were divided into five groups (n = 10): (A): adhesive system (control); (AL): adhesive system + Nd:YAG laser; (LAL): Nd:YAG laser + adhesive system + Nd:YAG laser; (PAL): calcium phosphate-based dentin desensitizer TeethMate + adhesive system + Nd:YAG laser; and group (PLAL): Nd:YAG laser + calcium phosphate-based dentin desensitizer + adhesive system + Nd:YAG laser. All materials were used according to the manufacturers' instructions. The specimens were submitted to artificial aging (5,000 thermal cycles and 12 × 104 mechanical cycles) then a bond test was performed. DP was measured using the split chamber model. Data were submitted to one-way analysis of variance (ANOVA), paired t-test, RM ANOVA, and Tukey test (p < 0.05). All treatments were effective in DP reduction. For BS, the groups PAL and PLAL had improved BS with a statistically significant difference of the control group (A). Nd:Yag laser irradiation and calcium phosphate-based desensitizing agents significantly reduced DP, and the association between them could improve the BS on resin-human dentin interface.

8.
J Adhes Dent ; 14(1): 69-73, 2012 Feb.
Artigo em Inglês | MEDLINE | ID: mdl-21935516

RESUMO

PURPOSE: To evaluate the cohesive strength between composite and different light-curing characterizing materials (LCCM), which were prepared using the intrinsic technique. MATERIALS AND METHODS: One hundred composite specimens were made by using a prefabricated Teflon device, and a layer of LCCM was applied at the interface. The specimens were divided into 5 groups (n = 20): group 1 (control), no LCCM was used; group 2: application of White Kolor Plus Pigment (Kerr) LCCM; group 3: White Tetric Color Pigment (Ivoclar/Vivadent) LCCM; group 4: Brown Kolor Plus Pigment (Kerr) LCCM; group 5: Black Tetric Color Pigment (Ivoclar/Vivadent) LCCM. All materials were used according to the manufacturers' instructions. Specimens were submitted to a tensile test in a universal testing machine (EMIC DL-200MF) to evaluate the cohesive strength at the composite interface. Data were subjected to one-way ANOVA and Tukey's test (α = 5%). RESULTS: ANOVA showed a p-value = 0.0001, indicating that there were significant differences among the groups. The mean values in MPa (± standard deviation) obtained for the groups were: G1: 28.5 (± 2.74)a; G2: 23.5 (± 2.47)b; G3: 20.3 (± 2.49)b; G4: 10.5 (± 2.40)c; G5: 9.66 (± 3.06)c. The groups with the same letters presented no significant differences. The control group presented statistically significantly higher cohesive strengths when compared to the other groups. The groups in which Brown Kolor Plus Pigment and Black Tetric Color Pigment LCCM were used showed significantly lower cohesive strengths when compared to the groups in which White Kolor Plus Pigment and White Tetric Color Pigment LCMM were used. CONCLUSION: The use of LCCM produced with the intrinsic technique reduced the cohesive strength of composite.


Assuntos
Corantes/química , Resinas Compostas/química , Materiais Dentários/química , Bis-Fenol A-Glicidil Metacrilato/química , Análise do Estresse Dentário/instrumentação , Humanos , Cura Luminosa de Adesivos Dentários , Teste de Materiais , Metacrilatos/química , Polietilenoglicóis/química , Ácidos Polimetacrílicos/química , Poliuretanos/química , Estresse Mecânico , Propriedades de Superfície , Resistência à Tração
9.
Microsc Res Tech ; 85(8): 3014-3024, 2022 Aug.
Artigo em Inglês | MEDLINE | ID: mdl-35593488

RESUMO

The present study evaluated the bond strength (µTBS) of dentin treated with chlorhexidine and propolis subjected to simulated pulpal pressure (SPP) and thermocycle aging. One hundred and twenty healthy human molars were sectioned to obtain 2 mm of dentin thickness and were divided into two groups (n = 60): SPP (15 cm H2 O) and no SPP (Control group). Dentin surfaces were conditioned with 37% phosphoric acid for 15 s and were divided according to the dentin treatment (n = 20): Control; Chlorhexidine gluconate (0.2% for 30 s) and Propolis (aqueous propolis extract for 30 s). Half of the specimens were submitted to 15,000 thermocycle aging (5 ± 2°C and 55 ± 2°C). The samples were sectioned into beams and submitted to µTBS. Data were analyzed by three-way ANOVA (SPP × Dentin treatment × Thermocycle aging) and the Tukey's tests (p < .001). With regard to the SPP, ANOVA revealed that the Control group (32.98 MPa) had significantly higher values of µTBS when compared to the SPP (29.19 MPa). With regard to Thermocycle aging, no aging (34.05 MPa) had significantly higher values of µTBS when compared to the aging (28.12 MPa). With regard to the dentin treatment, Propolis and Chlorhexidine did not statistically influence the results (p > .05). The SPP and thermocycle aging negatively influenced the bond strength between the dentin and resin; the 0.2% chlorhexidine digluconate and aqueous propolis extract solutions did not interfere in the bond strength between the resin and dentin. The use of chlorhexidine and propolis as a dental treatment may not influence the dentin bond strength, but SPP and thermocycle aging may damage the longitudinal dentin bond strength. RESEARCH HIGHLIGHTS: Chlorhexidine and propolis as a dental treatment may not influence the dentin bond strength. Simulated pulpal pressure and thermocycle aging may damage the longitudinal dentin bond strength.


Assuntos
Colagem Dentária , Própole , Clorexidina/química , Clorexidina/farmacologia , Resinas Compostas/química , Dentina , Adesivos Dentinários/química , Humanos , Teste de Materiais , Cimentos de Resina/química , Resistência à Tração
10.
Int J Dent ; 2022: 4821021, 2022.
Artigo em Inglês | MEDLINE | ID: mdl-36249726

RESUMO

Objective: This study aims to analyze the fluorescence-aided identification technique efficacy on adhesive remnant removal from the enamel surface after orthodontic bracket debonding. Materials and Methods: Forty-five extracted human upper central incisors were divided into 3 groups (n = 15) according to the kind of adhesive for bracket bonding and the use or absence of near UV light for remnant removal: BF/UV- fluorescent adhesive/UV light, BF/0-fluorescent adhesive/no UV light, and TB/0-nonfluorescent adhesive/no UV light. For all teeth, 100% of the adhesive used remained on the enamel surface after debonding. Fifteen dentists performed adhesive removal on the enamel surface using a carbide bur. The specimens were analyzed by a stereomicroscope, and the adhesive remnant percentage from each specimen was calculated. The time used by each dentist to perform the removal was recorded. The data were analyzed by one-way ANOVA and Tukey's test. Results: Significant differences were observed among groups for adhesive remnant (p=0.0008) and for time (p=0.0001). The means of adhesive remnant were BF/UV (5.84), BF/0 (34.37), and TB/0 (37.02). The mean times necessary to remove adhesive were BF/UV (1 min 40 s), BF/0 (3 min 03 s), and TB/0 (2 min 46 s). For the BF/UV group, significantly lower values of adhesive remnants and time for debonding were found (p < 0.05). Conclusion: The fluorescence-aided identification technique significantly reduced the amount of adhesive remnant, and the time necessary to perform this clinical procedure.

11.
Int J Dent ; 2022: 5771341, 2022.
Artigo em Inglês | MEDLINE | ID: mdl-35265134

RESUMO

Objective: To evaluate the physicochemical (sorption (SOR), solubility (SOL), and degree of conversion (DC)) and mechanical (flexural strength (FS), modulus of elasticity (ME), and compressive strength (CS)) properties of adhesives with different water contents (D2O). Materials and Methods: An adhesive was formulated: 55 wt% BisGMA, 45 wt% HEMA, 0.5 wt% camphorquinone, 0.5 wt% EDMAB, and 1.0 wt% DPIHP. D2O was added into the adhesives (0 wt%, 10 wt%, and 16 wt%). DC was monitored through the FTIR. FS, ME, CS, SOR, and SOL were tested. The adhesive samples were aged in deionized water, ethanol, and acetone. Data were submitted to ANOVA and Tukey's tests (5%). Results: For DC, the 0 wt% group showed a significant reduction (68.09 ± 0.14A) compared with the 10 wt% (87.07 ± 0.81B) and 16 wt% groups (89.87 ± 0.24B); 10 wt% showed the highest FS (MPa) mean values (141.6 ± 6.71B) compared with the 0 wt% (109.4 ± 20.5A) and 16 wt% (107.8 ± 15.8A). For the CS (MPa) and ME (GPa), the 16 wt% showed the lowest mean values (98.8 ± 18.0B and 2.2 ± 0.3B, respectively) compared with the 10 wt% and 0 wt%. For the SOR, 16 wt% of water showed the highest mean values and the ethanol showed the lowest mean values of SOL regardless of water content. Conclusion: The amount of water content and the types of aging solvents significantly affect the adhesive properties.

12.
Eur J Dent ; 2022 Dec 13.
Artigo em Inglês | MEDLINE | ID: mdl-36513340

RESUMO

OBJECTIVES: This article evaluated the effect of substrates rigidities on the post-fatigue fracture resistance of adhesively cemented simplified restorations in lithium disilicate glass ceramic. METHODS: Precrystalized computer-aided design/computer-aided manufacturing ceramic blocks were processed into disc-shaped specimens (n = 10, Ø = 10 mm), mimicking a simplified restoration at two thicknesses (0.5 and 1.0 mm). Thereafter, the discs were cemented onto different base substrates (dentin analogue [control], dentin analogue with a central core build-up of resin composite [RC], or glass ionomer cement [GIC]). The specimens were subjected to mechanical cycling in a chewing simulator (100 N, 1 × 106 cycles, 4 Hz) and then subjected to thermocycling aging (10,000 cycles, 5/37/55°C, 30 seconds). After the fatigue protocol, the specimens were loaded until failure (N) in a universal testing machine. Finite element analysis calculated the first principal stress at the center of the adhesive interface. RESULTS: The results showed that "restoration thickness," "type of substrate," and their interaction were statistically significant (one-way analysis of variance; p < 0.001). Regardless the restoration thickness a higher fracture load was observed for specimens cemented to dentin analogue. Among the base materials, RC build-up presented the highest fracture load and lower stress magnitude for both restoration thicknesses in comparison with GIC build-up. The 0.5-mm restoration showed higher stress peak and lower fracture load when submitted to the compressive test. CONCLUSION: More flexible base material reduces the fracture load and increases the stress magnitude of adhesively cemented lithium disilicate restorations regardless the ceramic thickness. Therefore, more rigid substrates are suggested to be used to prevent restoration mechanical failures.

13.
Int J Dent ; 2022: 5837864, 2022.
Artigo em Inglês | MEDLINE | ID: mdl-35815117

RESUMO

Radiotherapy induces a higher level of Candida spp. colonization, resulting in oral candidiasis. This study aimed to evaluate the phototransformation potential of the glycolic extract of Curcuma longa (C. longa); the antifungal activity of C. longa, curcumin, and antifungal photodynamic therapy (aPDT) with blue light-emitting diodes "LED" on Candida albicans and Candida tropicalis in vitro; and the toxicity of C. longa and curcumin in Galleria mellonella model. In order to confirm the light absorption capacity of the C. longa extract, its phototransformation potential was evaluated. The antifungal effect of C. longa, curcumin, and aPDT was evaluated over Candida spp. Finally, the toxicity of C. longa and curcumin was evaluated on the Galleria mellonella model. The data were analyzed using the GraphPad Prism 5.0 software considering α = 5%. It was found that C. longa, curcumin, and aPDT using blue LED have an antifungal effect over C. albicans and C. tropicalis. The extract of C. longa 100 mg/mL and curcumin 200 µg/mL do not show toxicity on Galleria mellonella model.

14.
J Adhes Dent ; 13(5): 433-8, 2011 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-20978642

RESUMO

PURPOSE: The aim of this study was to evaluate the influence of dentin abrasion on the microshear bond strength of two self-etching adhesive systems, using either an ultrasound diamond bur or a high-speed diamond bur. MATERIALS AND METHODS: Twenty noncarious human third molars were sectioned mesiodistally into halves. The enamel was ground to expose a flat dentin surface on both sections. The dentinal surfaces were randomly assigned to two groups, depending on the method of smear layer preparation: ultrasound diamond bur (UB) or conventional diamond bur (CB). The prepared dentin surfaces received one of two self-etching systems: Clearfil SE Bond (CF) and One-Up Bond F (OB). A composite cylinder with a 0.95-mm diameter was bonded to each specimen and the microshear bond test was performed. The results were expressed in MPa and were subjected to two-way analysis of variance (ANOVA) and Tukey's test (α = 0.05). RESULTS: There was no significant difference in dentin bond strength when comparing the conventional and ultrasonic abrasion methods. When the adhesive systems were compared, Clearfil SE Bond achieved higher bond strength means than did One-Up Bond F. CONCLUSION: The dentin surface preparation method did not influence the microshear bond strength and the Clearfil SE Bond adhesive system, independent of bur type used, Clearfil SE Bond showed higher bond strengths than did the One-Up Bond F adhesive system.


Assuntos
Condicionamento Ácido do Dente/métodos , Colagem Dentária , Adesivos Dentinários/química , Dentina/ultraestrutura , Diamante/química , Preparo do Dente/instrumentação , Resinas Compostas/química , Equipamentos Odontológicos de Alta Rotação , Materiais Dentários/química , Análise do Estresse Dentário/instrumentação , Humanos , Teste de Materiais , Metacrilatos/química , Microscopia Eletrônica de Varredura , Cimentos de Resina/química , Resistência ao Cisalhamento , Camada de Esfregaço , Estresse Mecânico , Ultrassom/instrumentação
15.
Oper Dent ; 36(2): 162-8, 2011.
Artigo em Inglês | MEDLINE | ID: mdl-21777098

RESUMO

The aim of this study was to assess the influence of manganese gluconate, a chemical activator of bleaching agents, at a concentration of 0.01% on the efficiency of a 10% carbamide peroxide-based bleaching agent. Forty bovine incisors were immersed in a 25% instant coffee solution for seven days and randomly divided into two groups. Group 1 was the control group and consisted of 10% carbamide peroxide-based bleaching gel only. Group 2 consisted of 10% carbamide peroxide-based bleaching gel and 0.01% manganese gluconate. Three readings of color were taken using the Vita Easyshade spectrophotometer: the initial reading, a reading at seven days, and a reading at 14 days. Total color variation was calculated by ΔE*Lab. Data were submitted to the statistical t-test (5%), which showed that after seven days group 2 had a significant increase in the degree of tooth bleaching compared with group 1. The mean values (±SD) were 16.33 (±3.95) for group 1 and 19.29 (±4.97) for group 2. However, the results for group 1 and group 2 were similar after 14 days. Adding 0.01% manganese gluconate to 10% carbamide peroxide bleaching gel increased the degree of tooth bleaching after a seven-day treatment and did not influence the resulting shade after 14 days.


Assuntos
Gluconatos/uso terapêutico , Peróxidos/uso terapêutico , Clareadores Dentários/uso terapêutico , Clareamento Dental/métodos , Ureia/análogos & derivados , Animais , Peróxido de Carbamida , Bovinos , Café , Cor , Esmalte Dentário/efeitos dos fármacos , Sinergismo Farmacológico , Teste de Materiais , Distribuição Aleatória , Espectrofotometria , Fatores de Tempo , Descoloração de Dente/tratamento farmacológico , Ureia/uso terapêutico
16.
Acta Odontol Scand ; 69(3): 176-81, 2011 May.
Artigo em Inglês | MEDLINE | ID: mdl-21250920

RESUMO

OBJECTIVE: To evaluate the effectiveness of the color change of hybrid light-emitting diode (LED) and low-intensity infrared diode laser devices for activating dental bleaching and to verify the occurrence of a color regression with time. MATERIAL AND METHODS: A total of 180 specimens obtained from human premolars were immersed in a coffee solution for 15 days for darkening and then divided into eight experimental groups (n = 20 in each) as follows: G1, bleaching without light; G2, bleaching with halogen light; G3, bleaching with a blue LED (1000 mW/470 nm) and a laser device (120 mW/795 nm) simultaneously; G4, bleaching with an LED emitting blue light (1000 mW/470 nm); G5, bleaching with a blue LED (800 mW/470 nm) and a laser device (500 mW/830 nm) simultaneously; G6, bleaching with a blue LED device (800 mW); G7, bleaching with a green LED (600 mW/530 nm) and a laser device (120 mW/795 nm) simultaneously; and G8, bleaching with a green LED (600 mW). Three measurements were performed (at baseline and 14 days and 12 months after bleaching) using a Vita Easyshade spectrophotometer. The data were submitted to two-way ANOVA and a Tukey test. RESULTS: All groups showed significantly higher ΔE values than Group G1, with the exception of Group G8. Variations in the ΔE values at 14 days were significant when compared with those obtained at baseline and after 12 months. CONCLUSIONS: Light activation of the bleaching gel provided faster and more intense bleaching than use of the bleaching gel without light activation. Combinations of low-intensity diode lasers are ineffective as a bleaching gel activator. Color regression was observed after 12 months of storage.


Assuntos
Lâmpadas de Polimerização Dentária , Lasers Semicondutores , Clareamento Dental/instrumentação , Clareamento Dental/métodos , Análise de Variância , Dente Pré-Molar , Cor , Halogênios , Humanos , Peróxido de Hidrogênio , Semicondutores , Estatísticas não Paramétricas , Clareadores Dentários
17.
J Contemp Dent Pract ; 12(2): 109-13, 2011 Mar 01.
Artigo em Inglês | MEDLINE | ID: mdl-22186753

RESUMO

OBJECTIVES: This study aimed to measure pH changes during 14 days intracoronal bleaching with hydrogen peroxide/sodium perborate and carbamide peroxide/sodium perborate. MATERIALS AND METHODS: Twenty patients presenting endodontically treated central maxillary incisors with color alterations were divided in two groups (n = 10): Group CP + SP: 37% carbamide peroxide + sodium perborate paste; Group HP + SP: 30% hydrogen peroxide + sodium perborate paste. The pH values were measured using a digital microprocessor at different times: Baseline, 2, 7 and 14 days. Data were analyzed with two-way ANOVA followed by Tukey's test (α = 0.05). RESULTS: ANOVA showed p < 0.00 which indicated significant difference between the groups. The mean values (± sd) and the results of the Tukey´s test were: HP + SP/14 days-7.98 (±0.58)a; HP + SP/7 days-8.59 (±0.18)b; HP + SP/2 days- 8.83 (±0.32)bc; HP + SP/Baseline-8.83 (±0.01)bc; CP + SP/ Baseline-8.89 (±0.01)bc; CP + SP/14 days-9.11 (±0.58)cd; CP + SP/7 days-9.54 (±0.16)de; CP + SP/2 days-9.66 (±0.08) de. The group HP + SP resulted in significantly lower pH values compared with group CP + SP. CONCLUSION: It can be concluded that both associations showed alkaline pH values; however, there was significant reduction in the pH values of the 30% hydrogen peroxide associated with sodium perborate after 14 days. CLINICAL SIGNIFICANCE: The association of hydrogen peroxide and carbamide peroxide with sodium perborate paste presented alkaline characteristics during the 14-day evaluated period. Thus, regarding pH changes, both associations can be considered safe as intracoronal bleaching agents.


Assuntos
Clareadores Dentários/química , Clareamento Dental/métodos , Dente não Vital , Adolescente , Adulto , Análise de Variância , Boratos/química , Peróxido de Carbamida , Combinação de Medicamentos , Humanos , Peróxido de Hidrogênio/química , Concentração de Íons de Hidrogênio , Pessoa de Meia-Idade , Peróxidos/química , Estatísticas não Paramétricas , Ureia/análogos & derivados , Ureia/química , Adulto Jovem
18.
J Contemp Dent Pract ; 12(5): 339-42, 2011 Sep 01.
Artigo em Inglês | MEDLINE | ID: mdl-22269193

RESUMO

AIM: This study evaluated the prevalence of the chewing side preference (CSP) in the deciduous, mixed and permanent dentitions. MATERIALS AND METHODS: Three-hundred subjects were divided in three groups (n = 100): Group 1 - children with deciduous dentition; group 2-children with mixed dentition; group 3 - subjects with permanent dentition. The CSP was determined using a direct method (visual observation) developed by McDonnell et al. (2004). Descriptive statistic was used to observe the prevalence of CSP. The Pearson's Chi-square was used to investigate signicant associations between gender, presence of CSP and preferred side (right/left). RESULTS AND CONCLUSION: Eighty-seven percent of group 1 had a CSP. Eighty-two percent of group 2 had a CSP. Seventy-six percent of group 3 had a CSP. There was no statistically significant association between presence of CSP and gender in all groups. There was no statistically significant association between preferred side (right/left) and gender in all groups. CLINICAL SIGNIFICANCE: There is a higher prevalence of subjects in deciduous, mixed and permanent dentition that presented chewing side preference. The early diagnosis of the presence of chewing side preference can prevent the unilateral chewing pattern with prophylactic therapy applied to the first teeth (deciduous).


Assuntos
Dentição Mista , Dentição Permanente , Lateralidade Funcional/fisiologia , Mastigação/fisiologia , Dente Decíduo , Adolescente , Adulto , Goma de Mascar , Criança , Pré-Escolar , Feminino , Humanos , Masculino , Pessoa de Meia-Idade , Fatores Sexuais , Adulto Jovem
19.
Int J Dent ; 2021: 6677159, 2021.
Artigo em Inglês | MEDLINE | ID: mdl-33815502

RESUMO

This study evaluated the effect of different surface treatments on the tensile bond strength between lithium disilicate glass-ceramics, resin cement, and dentin. Fifty truncated cone-shape glass-ceramics were divided into five groups (n = 10): G1, control: 10% hydrofluoric acid (HF); G2, Nd:YAG laser + silane; G3, Sil + Nd:YAG laser; G4, graphite + Nd:YAG laser + Sil; and G5, graphite + Sil + Nd:YAG laser. Fifty human third-molars were cut to cylindrical shape and polished to standardize the bonding surfaces. The glass-ceramic specimens were bonded to dentin with a dual-cured resin cement and stored in distilled water for 24 h at 37ºC. Tensile testing was performed on a universal testing machine (10 Kgf load cell at 1 mm/min) until failure. The bond strength values (mean ± SD) in MPa were G1 (9.4 ± 2.3), G2 (9.7 ± 2.0), G3 (6.7 ± 1.9), G4 (4.6 ± 1.1), and G5 (1.2 ± 0.3). Nd:YAG laser and HF improve the bond strength between lithium disilicate glass-ceramics, resin cement, and dentin. The application of a graphite layer prior to Nd:YAG laser irradiation negatively affects this bonding and presented inferior results.

20.
Int J Dent ; 2021: 2935507, 2021.
Artigo em Inglês | MEDLINE | ID: mdl-34956366

RESUMO

This study compared the bond strength of a composite repair made with a bulk fill composite and a conventional one using different surface treatments. Specimens were prepared as truncated cones (bases: 4 mm × 2 mm, height: 4 mm) using a bulk fill (OBFa: Filtek One) or a conventional resin (FTKa: Filtek Z250) (n = 66). They were artificially aged (10,000 cycles, 5°C-55°C, 30 sec) and subdivided according to surface treatments: NT-no treatment (control), Abr-abrasion with a diamond tip, and sand-sandblasting with aluminum oxide (50 µm). Treatments were performed over the smaller diameter surface, followed by adhesive (Scothbond Universal) application. A new specimen with similar dimensions was constructed over it using either the OBF or the FTK, totaling 12 groups (n = 11). Bond strength was assessed by tensile test. The data were submitted to two-way ANOVA separately for OBFa and FTKa, followed by Tukey's test (p < 0.05). For the aged OBFa groups, there was significant differences for composite type and surface treatment, with higher values of bond strength when repaired with the same material (OBFa/OBF > OBFa/FTK), and sandblasting and bur abrasion presented higher values compared to the control group (NT). For the aged FTKa groups, there were no differences for the composite or surface treatment. Therefore, the bulk fill resin composite tested present better repair performance when the same composite was used, while the conventional resin composite was less influenced by the material and the surface treatment performed.

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