RESUMEN
Poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) nanofibers embedded with borate glasses of 45B5 composition doped with Co2+, Cu2+, and Zn2 +(46.1 B2O326.9-X CaO24.4 Na2O2.6 P2O5, X CoO/CuO/ZnO mol % (X = 0-5)) were produced by electrospinning for wound healing applications. Prior to their addition, the glasses exhibited two broad halos typical of a vitreous borate network, which were mainly composed of ring-type metaborate structural units. The particle distribution in the PHBV nanofibers embedded with 45B5 borate bioactive glasses is present in isolated and agglomerated states, being partially coated by a polymeric layer-except for the cobalt-doped glass, which resulted in a successful encapsulation with 100% embedding efficiency. The incorporation of the glasses reduced the PHBV crystallinity degree and its decomposition temperature, as well as its mechanical properties, including Young's modulus, tensile strength, and elongation at break. The neat PHBV fibers and those containing the cobalt-doped glasses demonstrated great cytocompatibility with human keratinocytes (HaCat), as suggested by the high cell viability after 7 days of exposure. Further studies are needed to fully understand the wound healing potential of these fibers, but our results significantly contribute to the area.
Asunto(s)
Vendajes , Boratos , Cobalto , Cobre , Poliésteres , Zinc , Humanos , Cobre/química , Cobalto/química , Poliésteres/química , Boratos/química , Zinc/química , Vidrio/química , Ensayo de Materiales , Cicatrización de Heridas , Nanofibras/química , Línea Celular , PolihidroxibutiratosRESUMEN
OBJECTIVES: To evaluate the incorporation of repairing capsules containing different monomers and polymerization modulators on the self-healing efficiency of an experimental photopolymerizable resin-based composite. METHODS: Self-healing capsules containing different monomers and polymerization modulators were prepared by emulsion polymerization: TCDHEPT (TEGDMA and DHEPT), BTCDHEPT (Bis-GMA, TEGDMA, and DHEPT), and BTCBPO (Bis-GMA, TEGDMA, and BPO). The capsules were analyzed through Fourier transform infrared spectroscopy and scanning electron microscopy. The capsules were added into experimental photopolymerizable resin composites establishing the following groups: ER (Control without capsules), ER+BPO, ER+BPO+TCDHEPT, and ER+BTCBPO+BTCDHEPT. Filtek Z350 resin composite (3 M ESPE) was used as a commercial reference. The materials were tested for degree of conversion (DC), flexural strength (σf), elastic modulus (Ef), fracture toughness (virgin KIC), self-healing efficiency (healed KIC), and roughness. For statistical analysis, the significance value was established at an a = 0.05 level. RESULTS: When compared to the control material, the incorporation of repairing capsules did not affect DC, σf, and Ef. Fracture toughness was statistically similar between the experimental groups (p ≤ 0.05). Healed KIC was statistically different between the groups ER+TCDHEP and ER+BTCBPO+BTCDHEPT; the self-healing efficiency was higher for ER+TCDHEPT. Surface roughness was statistically similar among all groups. CONCLUSIONS: The use of self-healing capsules promoted repair of the material. Studies with material aging after the self-healing process are necessary to better demonstrate the effectiveness of this system. CLINICAL SIGNIFICANCE: The self-healing system seemed to be a promising technology to be used in self-repaired restorative materials, which may prevent restoration fractures.
Asunto(s)
Resinas Compuestas , Ácidos Polimetacrílicos , Bisfenol A Glicidil Metacrilato/química , Ensayo de Materiales , Resinas Compuestas/química , Ácidos Polimetacrílicos/química , Polietilenglicoles/química , Materiales Dentales/química , Cápsulas/química , Metacrilatos/químicaRESUMEN
The aim of this study was to develop a highly porous calcium-containing chitosan scaffold suitable for dentin regeneration. A calcium hydroxide (Ca[OH]2 ) suspension was used to modulate the degree of porosity and chemical composition of chitosan scaffolds. The chitosan solution concentration and freezing protocol were adjusted to optimize the porous architecture using the phase-separation technique. Scanning electron microscopy/energy-dispersive spectroscopy demonstrated the fabrication of a highly porous calcium-linked chitosan scaffold (CH-Ca), with a well-organized and interconnected porous network. Scaffolds were cross-linked on glutaraldehyde (GA) vapor. Following a 28-day incubation in water, cross-linked CH scaffold had no changes on humid mass, and CH-Ca featured a controlled degradability profile since the significant humid mass loss was observed only after 21 (26.0%) and 28 days (42.2%). Fourier-transform infrared spectroscopy indicated the establishment of Schiff base on cross-linked scaffolds, along with calcium complexation for CH-Ca. Cross-linked CH-Ca scaffold featured a sustained Ca2+ release up to 21 days in a humid environment. This porous and stable architecture allowed for human dental pulp cells (HDPCs) to spread throughout the scaffold, with cells exhibiting a widely stretched cytoplasm; whereas, the cells seeded onto CH scaffold were organized in clusters. HDPCs seeded onto CH-Ca featured significantly higher ALP activity, and gene expressions for ALP, Col1, DMP-1, and DSPP in comparison to CH, leading to a significant 3.5 times increase in calcium-rich matrix deposition. In sum, our findings suggest that CH-Ca scaffolds are attractive candidates for creating a highly porous and bioactive substrate for dentin tissue engineering.
Asunto(s)
Hidróxido de Calcio/química , Calcio/química , Quitosano/química , Dentina/química , Ingeniería de Tejidos/métodos , Andamios del Tejido/química , Adolescente , Materiales Biocompatibles , Células Cultivadas , Reactivos de Enlaces Cruzados , Pulpa Dental/citología , Expresión Génica , Glutaral , Humanos , Humedad , Porosidad , Espectroscopía Infrarroja por Transformada de FourierRESUMEN
This study evaluated the effect of different hydrofluoric acid (HF) concentrations on the bond strength between a lithium disilicate-based glass ceramic and a resin cement. Eighty ceramic-blocks (12×7×2 mm) of IPS e.Max CAD (Ivoclar Vivadent) were produced and randomly assigned to 8 groups, considering 2 study factors: HF concentration in 4 levels, i.e., 1% (HF1), 3% (HF3), 5% (HF5), and 10% (HF10), and storage in 2 levels, i.e., baseline (tests were performed 24 h after cementation), and aged (storage for 150 days + 12,000 thermal-cycles at 5°C and 55°C). Acid etching (20 s) was performed, followed by washing, drying, and silanization. Four resin cement cylinders (Ï= 0.96 mm) were built-up from starch matrices on each ceramic sample (n= 40). Additional ceramic samples were etched and analyzed for contact angle, micro-morphology, and roughness. In baseline condition (without aging), the HF3, HF5, and HF10 groups showed similar bond strength values (13.9 - 15.9 MPa), and HF1 (11.2 MPa) presented lower values than HF5, being that statistically different (p= 0.012). After aging, all the mean bond strengths statistically decreased, being that HF3, HF5, and HF10 (7.8 - 11 MPa) were similar and higher than HF1 (1.8 MPa) (p= 0.0001). For contact angle, HF3, HF5, and HF10 presented similar values (7.8 - 10.4°), lower than HF1 and CTRL groups. HF5 and HF10 presented rougher surfaces than other conditions. For better bond strength results, the tested ceramic may be etched by HF acid in concentrations of 3%, 5%, and 10%.
Asunto(s)
Grabado Ácido Dental/métodos , Cerámica/química , Recubrimiento Dental Adhesivo/métodos , Porcelana Dental/química , Ácido Fluorhídrico/química , Cementos de Resina/química , Ensayo de Materiales , Microscopía de Fuerza Atómica , Resistencia al Corte , Estrés Mecánico , Propiedades de SuperficieRESUMEN
Abstract This study evaluated the effect of different hydrofluoric acid (HF) concentrations on the bond strength between a lithium disilicate-based glass ceramic and a resin cement. Eighty ceramic-blocks (12×7×2 mm) of IPS e.Max CAD (Ivoclar Vivadent) were produced and randomly assigned to 8 groups, considering 2 study factors: HF concentration in 4 levels, i.e., 1% (HF1), 3% (HF3), 5% (HF5), and 10% (HF10), and storage in 2 levels, i.e., baseline (tests were performed 24 h after cementation), and aged (storage for 150 days + 12,000 thermal-cycles at 5°C and 55°C). Acid etching (20 s) was performed, followed by washing, drying, and silanization. Four resin cement cylinders (ϕ= 0.96 mm) were built-up from starch matrices on each ceramic sample (n= 40). Additional ceramic samples were etched and analyzed for contact angle, micro-morphology, and roughness. In baseline condition (without aging), the HF3, HF5, and HF10 groups showed similar bond strength values (13.9 - 15.9 MPa), and HF1 (11.2 MPa) presented lower values than HF5, being that statistically different (p= 0.012). After aging, all the mean bond strengths statistically decreased, being that HF3, HF5, and HF10 (7.8 - 11 MPa) were similar and higher than HF1 (1.8 MPa) (p= 0.0001). For contact angle, HF3, HF5, and HF10 presented similar values (7.8 - 10.4°), lower than HF1 and CTRL groups. HF5 and HF10 presented rougher surfaces than other conditions. For better bond strength results, the tested ceramic may be etched by HF acid in concentrations of 3%, 5%, and 10%.
Resumo Este estudo avaliou o efeito de diferentes concentrações de ácido fluorídrico (HF) na resistência de união entre uma cerâmica vítrea à base de dissilicato de lítio e um cimento resinoso. Oitenta blocos cerâmicos (12×7×2 mm) de IPS e.Max CAD (Ivoclar Vivadent) foram produzidos e distribuídos aleatoriamente em 8 grupos, considerando 2 fatores de estudo: concentração de HF em 4 níveis, isto é, 1% (HF1), 3% (HF3), 5% (HF5), e 10% (HF10), e armazenamento em 2 níveis, isto é, condição inicial (testes foram realizados 24 h após a cimentação), e envelhecidos (150 dias de armazenamento + 12.000 ciclos térmicos a 5°C e 55°C). Condicionamento ácido (20 s) foi realizado, seguido por lavagem, secagem e silanização. Quatro cilindros de cimento resinoso (ϕ= 0.96 mm) foram construídos a partir de matrizes de amido em cada amostra cerâmica (n= 40). Amostras cerâmicas adicionais foram condicionadas e analisadas quanto ao ângulo de contato, micro-morfologia e rugosidade. Na condição inicial (sem envelhecimento), os grupos HF3, HF5, e HF10 mostraram valores de resistência de união similares (13.9 - 15.9 MPa), e HF1 apresentou valores menores que HF5, sendo estatisticamente diferente (p= 0.012). Após o envelhecimento, todas as médias de resistência de união diminuíram estatisticamente, sendo que HF3, HF5 e HF10 foram similares e maiores que HF1 (p= 0.0001). Para o ângulo de contato, HF3, HF5 e HF10 apresentaram valores similares (7.8 - 10.4°), menores que os grupos HF1 e CTRL. HF5 e HF10 apresentaram superfícies mais rugosas que as outras condições. Para melhores resultados de resistência de união, a cerâmica testada pode ser condicionada com ácido fluorídrico nas concentrações de 3%, 5% e 10%.
Asunto(s)
Grabado Ácido Dental/métodos , Cerámica/química , Recubrimiento Dental Adhesivo/métodos , Cementos de Resina/química , Porcelana Dental/química , Ácido Fluorhídrico/química , Estrés Mecánico , Propiedades de Superficie , Ensayo de Materiales , Microscopía de Fuerza Atómica , Resistencia al CorteRESUMEN
This study investigated the effect of etching with distinct hydrofluoric (HF) acid concentrations on the cyclic load-to-failure (CLf) of simplified lithium disilicate glass-ceramic restorations adhesively cemented to a dentin analogue (nâ¯=â¯20): non-etched/control (CTRL), or etched for 20â¯s with HF acid at 3% (HF3), 5% (HF5), or 10% (HF10). A silane coating was then applied onto the ceramic surfaces. Fatigue tests followed the staircase approach (initial load= 720â¯N; step-size= 70â¯N; 500,000 cycles per sample; 20â¯Hz) using a hemispheric stainless-steel piston (Ø= 40â¯mm) under water. The CLf data were analyzed using Dixon and Mood method. Topographic and fractographic analyses were conducted. CLf (in N) of HF3 (1355⯱â¯32.0) and HF5 (1335⯱â¯58.8) groups were the highest and statistically similar; HF10 presented intermediate CLf (1175⯱â¯132.9), while the non-etched group had the lowest one (965⯱â¯145.0). Topographical analysis showed that the higher the HF acid concentration, the more pronounced the topographical changes. All failures (radial cracks) started from the inner surface of the ceramic discs. Topographical changes promoted by intermediate HF acid concentrations (3% and 5%) may improve fatigue performance for adhesively-cemented lithium disilicate restorations.
Asunto(s)
Porcelana Dental/química , Fracaso de la Restauración Dental , Ácido Fluorhídrico/química , Animales , Ensayo de Materiales , Soporte de PesoRESUMEN
INTRODUCTION: The purpose of this study was to clinically evaluate the effect of low-level laser therapy (LLLT) as a method of reducing pain reported by patients after placement of their first orthodontic archwires. METHODS: The sample comprised 60 orthodontic patients (ages, 12-18 years; mean, 15.9 years). All patients had fixed orthodontic appliances placed in 1 dental arch (maxillary or mandibular), received the first archwire, and were then randomly assigned to the experimental (laser), placebo, or control group. This was a double-blind study. LLLT was started in the experimental group immediately after placement of the first archwire. Each tooth received a dose of 2.5 J per square centimeter on each side (buccal and lingual). The placebo group had the laser probe positioned into the mouth at the same areas overlying the dental root and could hear a sound every 10 seconds. The control group had no laser intervention. All patients received a survey to be filled out at home describing their pain during the next 7 days. RESULTS: The patients in the LLLT group had lower mean scores for oral pain and intensity of pain on the most painful day. Also, their pain ended sooner. LLLT did not affect the start of pain perception or alter the most painful day. There was no significant difference in pain symptomatology in the maxillary or mandibular arches in an evaluated parameter. CONCLUSIONS: Based on these findings, we concluded that LLLT efficiently controls pain caused by the first archwire.
Asunto(s)
Dolor Facial/radioterapia , Láseres de Semiconductores/uso terapéutico , Terapia por Luz de Baja Intensidad/métodos , Alambres para Ortodoncia/efectos adversos , Adolescente , Análisis de Varianza , Niño , Método Doble Ciego , Femenino , Humanos , Masculino , Mandíbula , Maxilar , Ortodoncia/métodos , Resultado del TratamientoRESUMEN
The aim of this study was to qualitatively demonstrate surface micro-morphological changes after the employment of different surface conditioning methods on high-alumina and glassy-matrix dental ceramics. Three disc-shaped high-alumina specimens (In-Ceram Alumina, INC) and 4 glassy-matrix ceramic specimens (Vitadur Alpha, V) (diameter: 5 mm and height: 5 mm) were manufactured. INC specimens were submitted to 3 different surface conditioning methods: INC1--Polishing with silicon carbide papers (SiC); INC2--Chairside air-borne particle abrasion (50 microm Al2O3); INC3 - Chairside silica coating (CoJet; 30 microm SiOx). Vitadur Alpha (V) specimens were subjected to 4 different surface conditioning methods: V1--Polishing with SiC papers; V2 - HF acid etching; V3--Chairside air-borne particle abrasion (50 microm Al2O3); V4--Chairside silica coating (30 microm SiOx). Following completion of the surface conditioning methods, the specimens were analyzed using SEM. After polishing with SiC, the surfaces of V specimens remained relatively smooth while those of INC exhibited topographic irregularities. Chairside air-abrasion with either aluminum oxide or silica particles produced retentive patterns on both INC and V specimens, with smoother patterns observed after silica coating. V specimens etched with HF presented a highly porous surface. Chairside tribochemical silica coating resulted in smoother surfaces with particles embedded on the surface even after air-blasting. Surface conditioning using air-borne particle abrasion with either 50 microm alumina or 30 microm silica particles exhibited qualitatively comparable rough surfaces for both INC and V. HF acid gel created the most micro-retentive surface for the glassy-matrix ceramic tested.
Asunto(s)
Grabado Ácido Dental/métodos , Óxido de Aluminio/química , Cerámica/química , Recubrimiento Dental Adhesivo/métodos , Cementos de Resina/química , Abrasión Dental por Aire , Cementación/métodos , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Propiedades de Superficie , Resistencia a la TracciónRESUMEN
The aim of this study was to qualitatively demonstrate surface micro-morphological changes after the employment of different surface conditioning methods on high-alumina and glassy-matrix dental ceramics. Three disc-shaped high-alumina specimens (In-Ceram Alumina, INC) and 4 glassy-matrix ceramic specimens (Vitadur Alpha, V) (diameter: 5 mm and height: 5 mm) were manufactured. INC specimens were submitted to 3 different surface conditioning methods: INC1 - Polishing with silicon carbide papers (SiC); INC2 - Chairside air-borne particle abrasion (50 µm Al2O3); INC3 - Chairside silica coating (CoJet; 30 µm SiOx). Vitadur Alpha (V) specimens were subjected to 4 different surface conditioning methods: V1 - Polishing with SiC papers; V2 - HF acid etching; V3 - Chairside air-borne particle abrasion (50 µm Al2O3); V4 - Chairside silica coating (30 µm SiOx). Following completion of the surface conditioning methods, the specimens were analyzed using SEM. After polishing with SiC, the surfaces of V specimens remained relatively smooth while those of INC exhibited topographic irregularities. Chairside air-abrasion with either aluminum oxide or silica particles produced retentive patterns on both INC and V specimens, with smoother patterns observed after silica coating. V specimens etched with HF presented a highly porous surface. Chairside tribochemical silica coating resulted in smoother surfaces with particles embedded on the surface even after air-blasting. Surface conditioning using air-borne particle abrasion with either 50 µm alumina or 30 µm silica particles exhibited qualitatively comparable rough surfaces for both INC and V. HF acid gel created the most micro-retentive surface for the glassy-matrix ceramic tested.
Asunto(s)
Grabado Ácido Dental/métodos , Óxido de Aluminio/química , Cerámica/química , Recubrimiento Dental Adhesivo/métodos , Cementos de Resina/química , Abrasión Dental por Aire , Cementación/métodos , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Propiedades de Superficie , Resistencia a la TracciónRESUMEN
PURPOSE: The aim of this study was to evaluate the effect of two surface conditioning methods on the microtensile bond strength of a resin cement to three high-strength core ceramics: high alumina-based (In-Ceram Alumina, Procera AllCeram) and zirconia-reinforced alumina-based (In-Ceram Zirconia) ceramics. MATERIALS AND METHODS: Ten blocks (5 x 6 x 8 mm) of In-Ceram Alumina (AL), In-Ceram Zirconia (ZR), and Procera (PR) ceramics were fabricated according to each manufacturer's instructions and duplicated in composite. The specimens were assigned to one of the two following treatment conditions: (1) airborne particle abrasion with 110-microm Al2O3 particles + silanization, (2) silica coating with 30 microm SiOx particles (CoJet, 3M ESPE) + silanization. Each ceramic block was duplicated in composite resin (W3D-Master, Wilcos, Petrópolis, RJ, Brazil) using a mold made out of silicon impression material. Composite resin layers were incrementally condensed into the mold to fill up the mold and each layer was light polymerized for 40 s. The composite blocks were bonded to the surface-conditioned ceramic blocks using a resin cement system (Panavia F, Kuraray, Okayama, Japan). One composite resin block was fabricated for each ceramic block. The ceramic-composite was stored at 37 degrees C in distilled water for 7 days prior to bond tests. The blocks were cut under water cooling to produce bar specimens (n = 30) with a bonding area of approximately 0.6 mm2. The bond strength tests were performed in a universal testing machine (crosshead speed: 1 mm/min). Bond strength values were statistically analyzed using two-way ANOVA and Tukey's test (< or = 0.05). RESULTS: Silica coating with silanization increased the bond strength significantly for all three high-strength ceramics (18.5 to 31.2 MPa) compared to that of airborne particle abrasion with 110-microm Al2O3 (12.7-17.3 MPa) (ANOVA, p < 0.05). PR exhibited the lowest bond strengths after both Al2O3 and silica coating (12.7 and 18.5 MPa, respectively). CONCLUSION: Conditioning the high-strength ceramic surfaces with silica coating and silanization provided higher bond strengths of the resin cement than with airborne particle abrasion with 110-microm Al2O3 and silanization.
Asunto(s)
Óxido de Aluminio/química , Cerámica/química , Recubrimiento Dental Adhesivo , Porcelana Dental/química , Cementos de Resina/química , Circonio/química , Abrasión Dental por Aire , Resinas Compuestas/química , Análisis del Estrés Dental/instrumentación , Humanos , Ensayo de Materiales , Silanos/química , Dióxido de Silicio/química , Estrés Mecánico , Propiedades de Superficie , Temperatura , Resistencia a la Tracción , Agua/químicaRESUMEN
A reconstrução coronária, realizada por meio de pinos intra-radiculares de fibras associados a materiais restauradores adesivos tem possibilitado obter o máximo de preservação das estruturas dentais bem como diminuir o risco de fratura radicular geralmente inerente quando da utilização de retentores metálicos. Assim sendo, a proposta deste estudo foi abordar aspectos científicos atuais relacionados à técnica de reconstrução direta com pinos de fibras e materiais resinosos adesivos, especialmente, o risco de fratura radicular associado a diferentes ancoragem intra-radiculares. Os autores apresentaram uma técnica de restauração de dentes tratados endodonticamente, com pinos intra-radiculares de fibras de quartzo associados a materiais adesivos (sistema adesivo, cimento resinoso e resina composta)
Asunto(s)
Pins Dentales , Materiales de Obturación del Conducto Radicular , Fracturas de los Dientes , Resinas Compuestas , Recubrimientos Dentinarios , Técnica de Perno MuñónRESUMEN
The purpose of this study was to test the hypothesis that mechanical polishing methods of ceramic surfaces allow similar superficial roughness to that of glazed surfaces. Twenty-five Vitadur Alpha ceramic discs (5 mm x 2 mm) were prepared according to the manufacturer's specifications. All specimens were glazed and randomly assigned to 5 groups (n=5), according to finishing and polishing protocols: G1: glazed (control); G2: diamond bur finishing; G3: G2 + silicon rubber tip polishing; G4: G3 + felt disc/diamond polishing paste; G5: G3 + felt disc impregnated with fine-particle diamond paste. Next, surface roughness means (Ra - microm) were calculated. Qualitative analysis was made by scanning electron microscopy. Surface roughness data were submitted to ANOVA and Tukey's test at 5% significance level. G1 and G4 were statistically similar (p>0.05). G2 presented the highest roughness means (p<0.05) followed by groups G3, G5, G4 and G1 in a decreasing order. The hypothesis was partially confirmed as only the mechanical polishing (G4) produced similar superficial roughness to that of surface glazing, although finishing and polishing are technically critical procedures.
Asunto(s)
Óxido de Aluminio/química , Silicatos de Aluminio/química , Cerámica/química , Pulido Dental/métodos , Porcelana Dental/química , Compuestos de Potasio/química , Pulido Dental/instrumentación , Diamante/química , Humanos , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Elastómeros de Silicona/química , Propiedades de SuperficieRESUMEN
The purpose of this study was to test the hypothesis that mechanical polishing methods of ceramic surfaces allow similar superficial roughness to that of glazed surfaces. Twenty-five Vitadur Alpha ceramic discs (5 mm x 2 mm) were prepared according to the manufacturer's specifications. All specimens were glazed and randomly assigned to 5 groups (n=5), according to finishing and polishing protocols: G1: glazed (control); G2: diamond bur finishing; G3: G2 + silicon rubber tip polishing; G4: G3 + felt disc/diamond polishing paste; G5: G3 + felt disc impregnated with fine-particle diamond paste. Next, surface roughness means (Ra - æm) were calculated. Qualitative analysis was made by scanning electron microscopy. Surface roughness data were submitted to ANOVA and Tukey's test at 5 percent significance level. G1 and G4 were statistically similar (p>0.05). G2 presented the highest roughness means (p<0.05) followed by groups G3, G5, G4 and G1 in a decreasing order. The hypothesis was partially confirmed as only the mechanical polishing (G4) produced similar superficial roughness to that of surface glazing, although finishing and polishing are technically critical procedures.
O objetivo deste estudo foi testar a hipótese de que o acabamento e o polimento da superfície cerâmica produzem rugosidade superficial semelhante à superfície cerâmica vitrificada. Vinte e cinco corpos-de-prova (5 mm x 2 mm) da cerâmica Vitadur Alpha foram obtidos de acordo com as recomendações do fabricante. Todas os corpos-de-prova foram vitrificados e aleatoriamente divididos em 5 grupos (n=5), de acordo com os seguintes protocolos de acabamento e polimento: G1: vitrificação (controle); G2: abrasão com ponta diamantada; G3: G2 + acabamento com borrachas abrasivas; G4: G3 + polimento com pasta diamantada/disco de feltro; G5: G3 + disco de feltro impregnado com pasta diamantada. Após 6 análises individuais foi obtida 1 média por corpo-de-prova da rugosidade (Ra). A análise qualitativa foi realizada por microscopia eletrônica de varredura. Os valores médios de rugosidade foram submetidos à ANOVA e ao teste de Tukey com nível de significância de 5 por cento. G1 e G4 foram estatisticamente semelhantes (p>0.05). O grupo G2 apresentou o maior valor médio de rugosidade (p<0.05) seguido por G3, G5, G4 e G1 em ordem decrescente. A hipótese foi parcialmente confirmada, pois somente o polimento mecânico do grupo G4 produziu rugosidade superficial semelhante à da superfície vitrificada, embora o acabamento e o polimento sejam procedimentos críticos tecnicamente.
Asunto(s)
Humanos , Óxido de Aluminio/química , Silicatos de Aluminio/química , Cerámica/química , Pulido Dental/métodos , Porcelana Dental/química , Compuestos de Potasio/química , Pulido Dental/instrumentación , Diamante/química , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Propiedades de Superficie , Elastómeros de Silicona/químicaRESUMEN
Os implantes osseointegrados têm sido utilizados na Odontologia com taxas de sucesso consideráveis, todavia, falhas poderão ocorrer, entre elas, a infecção microbiana conhecida por periimplantite. A periimplantite é uma condição patológica caracterizada pela inflamação do tecido mole ao redor dos implantes, sangramento, supuração e rápida perda óssea. Diversas formas de tratamento da periimplantite vêm sendo propostas, com o objetivo de manter o implante integrado ao tecido ósseo. De forma similar à terapêutica utilizada para a doença periodontal, na infecção periimplantar ela deverá ser focada especificamente na eliminação das bactérias presentes no local infectado. Assim sendo, terapias à base de agentes antimicrobianos, associados ou não a métodos cirúrgicos de regeneração tecidual guiada e enxerto, logicamente, dependendo do grau de evolução da patologia, devem ser empregadas. Por esta razão, este estudo propôs-se a avaliar, através da revisão da literatura, as diferentes abordagens terapêuticas em casos de periimplantite
Asunto(s)
Antiinfecciosos Locales , Implantes Dentales , Pérdida de la Inserción Periodontal , Periodontitis , Antiinfecciosos , Implantación Dental Endoósea , InflamaciónRESUMEN
Em uma breve revisão da literatura sobre o complexo conceito de Proporção Áurea, os autores citam que este vem sendo utilizado desde a Antigüidade pelos gregos, que reconheceram seu papel dominante nas proporções do corpo humano. Para a Proporção Áurea, têm sido atribuídos vários sinônimos, como, por exemplo: Seção Áurea, Porcentagem de Ouro, Proporção Divina, Número de Ouro, Valor Dourado, Phi, entre outros. A série matemática exponencial de Fibonacci (1, 1, 2, 3, 5, 8, 13, 21...) demonstra que cada termo é a soma dos dois termos anteriores, e a razão entre dois termos consecutivos tende a se aproximar da Seção Áurea (1,618). Esta proporção vem sendo utilizada em diversas especialidades odontológicas, dentre elas a Odontologia Estética. A forma e o contorno, o comprimento e a largura dos dentes, o posicionamento da linha do sorriso e da linha média, a inclinação axial e o posicionamento da borda incisal de cada dente são alguns dos princípios estéticos considerados e usados no desenho do sorriso. Portanto, a Proporção Dourada merece uma atenção especial no estudo da beleza facial, pois possibilita critérios mais preciosos para a análise estético-morfológica dos dentes
RESUMEN
Embora as cerâmicas possuam alta resistência à compressäo, apresentam friabilidade devido à sua baixa resistência à traçäo e, desta forma, possuem menor capacidade de absorver impactos. Este trabalho avaliou a tenacidade à fratura de diferentes sistemas cerâmicos, que refere-se à medida da habilidade de absorçäo da energia de deformaçäo de um material friável. Foram confeccionados 30 corpos-de-prova em forma de discos (5mmx3mm) utilizando-se três diferentes materiais cerâmicos, os quais foram divididos em 3 grupos: G1-10 amostras confeccionadas com a cerâmica Vitadur Alpha (Vita-Zahnfabrik); G2-10 amostras confeccionadas com a cerâmica IPS Empress 2 (Ivoclar-Vivadent) e G3-10 amostras confeccionadas com a cerâmica In-Ceram Alumina (Vita-Zahnfabrik). Para a obtençäo dos valores de tenacidade foi utilizada a técnica da indentaçäo que se baseia na série de fissuras que se formam sob uma carga pesada. Foram realizadas 4 impressöes por amostra, utilizado um microdurômetro (Digital Microhardness Tester FM) com uma carga de 500gf, durante 10 segundos. A análise estatística dos dados (Testes ANOVA de Kruskal-Wallis e Dunn), indica que a cerâmica In-Ceram Alumina apresentou valor mediano (2,96N/m3/2), estatisticamente diferente do apresentado pela IPS Empress 2 (1,05N/m3/2), enquanto que a cerâmica Vitadur Alpha apresentou valores intermediários (2,08N/m3/2), sem diferenças estatísticas dos outros dois materiais. Conclui-se que as cerâmicas apresentam diferentes desempenhos de tenacidade à fratura, sendo a In-Ceram capaz de absorver maior energia comparada a Vitadur Alpha e ao IPS Empress2
Asunto(s)
Cerámica/clasificación , Cerámica/química , Fuerza Compresiva , Materiales Dentales/clasificación , Materiales Dentales/químicaRESUMEN
Verniz fluoretado é um agente com capacidade de prolongar o período de contato do flúor com esmalte dentário. Possui alta concentração de flúor, sendo bastante eficaz na remineralização da estrutura dentária. Indicado, principalmente, nos casos de hipersensibilidade dentinária e na prevenção de cáries em adultos e crianças. O objetivo deste trabalho é relatar vantagens e desvantagens dos vernizes, bem como verificar que produtos estão à disposição dos profissionais.
Asunto(s)
Resinas Compuestas , Luz , Polímeros , Efectos de la Radiación , Tecnología OdontológicaRESUMEN
The purpose of this study was to compare the microhardness of four indirect composite resins. Forty cylindrical samples were prepared according to the manufacturers recommendations using a Teflon mold. Ten specimens were produced from each tested material, constituting four groups (n=10) as follows: G1 - Artglass; G2 - Sinfony; G3 - Solidex; G4 - Targis. Microhardness was determined by the Vickers indentation technique with a load of 300g for 10 seconds. Four indentations were made on each sample, determining the mean microhardness values for each specimen. Descriptive statistics data for the experimental conditions were: G1 - Artglass (mean ±ï standard deviation: 55.26 ± 1.15HVN; median: 52.6); G2 - Sinfony (31.22 ± 0.65HVN; 31.30); G3 - Solidex (52.25 ± 1.55HVN; 52.60); G4 - Targis (72.14 ± 2.82HVN; 73.30). An exploratory data analysis was performed to determine the most appropriate statistical test through: (I) Levene's for homogeneity of variances; (II) ANOVA on ranks (Kruskal-Wallis); (III) Dunn's multiple comparison test (0.05). Targis presented the highest microhardness values while Sinfony presented the lowest. Artglass and Solidex were found as intermediate materials. These results indicate that distinct mechanical properties may be observed at specific materials. The composition of each material as well as variations on polymerization methods are possibly responsibles for the difference found in microhardness. Therefore, indirect composite resin materials that guarantee both good esthetics and adequate mechanical properties may be considered as substitutes of natural teeth.
RESUMEN
Although ceramics present high compressive strength, they are brittle materials due to their low tensile strength so they have lower capacity to absorb shocks. This study evaluated the fracture toughness of different ceramic systems, which refers to the ability of a friable material to absorb defformation energy. Three ceramic systems were investigated. Ten cylindrical samples (5,0mm x 3,0mm), were obtained from each ceramic material as follows: G1- 10 samples of Vitadur Alpha (Vita-Zahnfabrik); G2- 10 samples of IPS Empress2 (Ivoclar-Vivadent); G3- 10 samples of In-Ceram Alumina (Vita-Zahnfabrik). Fracture toughness values were collected upon indentation tests that were performed under a heavy load. A microhardness tester (Digital Microhardness Tester FM) utilized a 500gf load cell during 10seconds to perform four impressions on each sample. Statistically significant results were observed (ANOVA and Kruskal-Wallis tests). In-Ceram Alumina presented the highest median toughness values (2,96N/m3/2), followed by Vitadur Alpha (2,08N/m3/2) and IPS Empress2 (1,05N/m3/2). It may be concluded that different ceramic systems present distinct fracture toughness values, thus In-Ceram is capable of absorbing superior stress when compared to Vitadur Alpha and IPS Empress2.