RESUMEN
Materials presenting high optical nonlinearity, such as materials containing metal nanoparticles (NPs), can be used in various applications in photonics. This motivated the research presented in this paper, where morphological, linear and nonlinear optical characteristics of gold NPs on the surface of bulk soda-lime glass substrates were investigated as a function of nanoparticle height. The NPs were obtained by annealing gold (Au) thin films previously deposited on the substrates. Pixel intensity histogram fitting on Atomic Force Microscopy (AFM) images was performed to obtain the thickness of the deposited film. Image analysis was employed to obtain the statistical distribution of the average height of the NPs. In addition, absorbance spectra of the samples before and after annealing were measured. Finally, the nonlinear refractive index (n2) and the nonlinear absorption index (α2) at 800 nm were obtained before and after annealing by using the thermally managed eclipse Z-scan (TM-EZ) technique with a Ti:Sapphire laser (150 fs pulses). Results show that both n2 and α2 at this wavelength change signs after the annealing and that the samples presented a high nonlinear refractive index.
Asunto(s)
Compuestos de Calcio/química , Oro/química , Nanopartículas/química , Nanopartículas/ultraestructura , Óxidos/química , Refractometría/métodos , Hidróxido de Sodio/química , Adsorción , Vidrio/química , Luz , Modelos Lineales , Ensayo de Materiales , Dinámicas no Lineales , Dispersión de Radiación , Propiedades de SuperficieRESUMEN
The analysis of the quality of food oils is of paramount importance, because the degradation of oils can lead to formation of harmful substances to the human organism. With the increase of the degradation of oils an increase of its refractive index occurs. The objective of this work is to develop and to characterize optical fiber refractometers sensitive to variations of refractive index of food oil samples. The optical fiber refractometers thanks to the intrinsic characteristics make them suitable for monitoring the quality of frying oils. They possess the advantages to require small volumes of sample for analysis, do not contaminate the sample, and supply the response in real time. In this work a long period grating (LPG) as refractometer is used because of their sensitivity to refractive index of the external media: degraded and not degraded frying oil samples. The oil samples had been characterized by the analysis of total polar components. The refractive index of oil is above 1.47, this region the LPG does not show enough sensitivity, a nanolayer of an organic material was coated onto the fiber. Using the Langmuir-Blodgett technique the response of LPG is modified according to the refractive index and thickness of the film. The deposition of the film modifies the rates effective modes of cladding, thus improving the response of the changes in the refractive index of the external media higher than that the refractive index of the cladding (n=1.457).
Asunto(s)
Análisis de los Alimentos/instrumentación , Aceites/análisis , Fibras Ópticas , Refractometría/instrumentación , Diseño de EquipoRESUMEN
A micrometric Fabry-Perot refractometer based on an end-of-fiber polymer tip is proposed. The fiber tip, with a length of 36 mum, was fabricated by self-guiding photopolymerization. The two-wave interferometric operation was achieved by combining the light waves generated at the interface between the single-mode fiber and the polymer tip, and at the fiber tip end (Fresnel reflection). The Fabry-Perot interferometer is coherence addressed and heterodyne interrogated, resulting into a liquid refractive index resolution of approximately 7.5x10(-4).
Asunto(s)
Polímeros , Refractometría/métodos , Procesos Fotoquímicos , Polímeros/químicaRESUMEN
In this work, sensitivity to strain and temperature of a sensor relying on modal interferometry in hollow-core photonic crystal fibers is studied. The sensing structure is simply a piece of hollow-core fiber connected in both ends to standard single mode fiber. An interference pattern that is associated to the interference of light that propagates in the hollow core fundamental mode with light that propagates in other modes is observed. The phase of this interference pattern changes with the measurand interaction, which is the basis for considering this structure for sensing. The phase recovery is performed using a white light interferometric technique. Resolutions of +/- 1.4 microepsilon and +/- 0.2 degrees C were achieved for strain and temperature, respectively. It was also found that the fiber structure is not sensitive to curvature.
RESUMEN
A novel Mach-Zehnder interferometer based on a fiber multimode interference structure combined with a long-period fiber grating (LPG) is proposed. The multimode interference is achieved through the use of a MMF section spliced between two single-mode fibers, with a length adjusted to couple a fraction of light into the cladding modes. A LPG placed after the MMF couples light back into the fiber core, completing the Mach-Zehnder interferometer. This novel configuration was demonstrated as a bending sensor.
RESUMEN
A novel in-fiber modal interferometer is presented that is based on a nonadiabatic biconical fused taper that couples light between the cladding and the core, combined with the Fresnel reflection at the fiber end. It is observed that the returned light from this fiber structure shows a channeled spectrum similar to that of a two-wave Michelson interferometer. The application of this device as a fiber optic flowmeter sensor is demonstrated.
RESUMEN
In this study, our objective was to evaluate Etest strips containing exponential gradients of isoniazid (INH), rifampin (RIF), and streptomycin (STR) for susceptibility testing of Mycobacterium tuberculosis. M. tuberculosis isolates were tested for antimicrobial susceptibilities by the standard proportion method using Löwenstein-Jensen (LJ) medium and by the Etest. The MICs determined by the Etest were obtained at 5, 7, or 10 days. In some strains with Etest-discrepant results, radiometric susceptibility testing (BACTEC) was performed to determine a consensus result. M. tuberculosis concordance between the two methods was 97% (86 of 89 isolates) for RIF, 96% for INH (84 of 87 isolates), and 80% (61 of 76 isolates) for STR. Most of the MICs determined by the Etest were easy to interpret and readable within 5 days. Results correlated well with those obtained by the LJ proportion and BACTEC methods for INH and RIF. However, a high proportion of false-sensitive and false-resistant results were observed, most often for STR. We also observed that variations in the inoculum size of M. tuberculosis isolates affected the MICs to a substantial degree. These discrepancies, along with the expense of the media, the Etest strips, and the specialized equipment required (CO2 incubator), make this method less useful in developing countries.