RESUMEN
Aim: To compare the effect of different zirconia surface treatments on cement bond strength to dentine. Materials and Methods: Stick-shaped pre-sintered zirconia (N = 128) were prepared and divided into eight groups (n = 16). Three surface treatments (sandblasting, neodymium-doped yttrium aluminum garnet [Nd:YAG] or carbon dioxide laser irradiation) were applied, either before (later to be sintered) or after sintering. The last test group was sintered zirconia coated with feldspathic veneering ceramic. Sintered zirconia without surface treatment was tested as the control group. Zirconia samples were cemented to dentine using Panavia F2 cement. The micro-shear bond strength was measured after 24 h (n = 8) or 10,000 thermocycling (n = 8). Statistical Analysis: Data were analyzed using one-way analysis of variances and Student's t-tests. Results: Zirconia coated with feldspathic ceramic revealed the highest bond strength (P < 0.001). Presintered zirconia treated with Nd: YAG laser showed a significantly improved bond strength compared to the control group before and after thermocycling. The bond strength after thermocycling was significantly reduced in presintered zirconia treated with Nd: YAG or sandblasting. Adhesive failure at the zirconia-cement interface was the dominant failure type. Conclusions: Surface treatment of presintered zirconia by Nd:YAG laser or coating of the sintered specimens with feldspathic veneering ceramic increased the zirconia-cement bond strength.
RESUMEN
Introduction: Increased demand for metal free fixed partial denture in recent years led to the developing of all ceramic material with excellent mechanical properties. One of the most popular all ceramic is zirconia which shows poor bonding properties. Recently, universal primer contains of silane and phosphate monomer for bond to zirconia have been introduced. The aim of this study is determination of the best method for bonding to zirconia based on the selection of the correct primer, suitable adhesive and best surface pretreatment. Methods: In this in vitro experimental study 16 sintered-zirconia blocks prepared in dimension of (18×6×2 mm) by CAD/CAM technology. Sample cleansed by ultrasonic device contain of 96% ethanol in 6 minutes, after air-drying, based on surface treatment randomly divided into 4 groups which each group divided into 2 sub-groups based on the use of a primer or universal bond: (1) no treatment: (a) cement + zirconia primer, (b) cement + universal bond. (2) Alumina pretreatment: (a) cement + zirconia primer, (b) cement + universal bond. (3) Cojet sand pretreatment: (a) cement + zirconia primer, (b) cement + universal bond. (4) laser pretreatment (a) cement + zirconia primer, (b) cement + universal bond. Composite disc prepared with condensation of composite resin in Tygon tube with integral diminution of 0.7 mm which cured for 40 sconds. Universal bond or zirconia primmer apply on the surface of the zirconia samples then cemented to composite disks by Panavia F2 according manufacture instructions. Microshear bond strength determined with universal testing machine. Failure mode assessed under stereomicroscope. Selected sample based on surface treatment evaluated under SEM. Data were analyzed using one-way analysis of variance (ANOVA). Results: Comparison of the 4 surface treatment groups revealed a significant difference and the highest bond belonged to Cojet and the lowest one to laser group. Conclusion: It seems that Universal Adhesive can to be considered as an alternative to bond to zirconia but the Cojet method is still required.
