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Synthesis and structural characterization of fluorinated thiosemicarbazones.
Bautista, Juan L; Flores-Alamo, Marcos; Tiburcio, Jorge; Vieto, Rebeca; Torrens, Hugo.
Molecules ; 18(10): 13111-23, 2013 Oct 22.
Article in English | MEDLINE | ID: mdl-24152598

ABSTRACT

Six new fluorinated thiosemicarbazones R­C(R')=N-NH-C(S)NH(2) (R = 2,4-C(6)H(3)F(2), R' = H (1); R = 2,5-C(6)H(3)F(2), R' = H (2); R = 2,6-C(6)H(3)F(2), R' = H (3); R = 3,4-C(6)H(3)F(2), R' = H (4); R = 3,5-C(6)H(3)F(2), R' = H (5) and R = 4-C(6)H(4)F, R' = C(6)H(5), (6)) have been prepared. The molecular structures of compounds 1 to 6 have been determined.


Subject(s)
Hydrocarbons, Fluorinated/chemical synthesis , Thiosemicarbazones/chemical synthesis , Benzaldehydes/chemical synthesis , Benzaldehydes/chemistry , Crystallography, X-Ray , Halogenation , Hydrocarbons, Fluorinated/chemistry , Hydrogen Bonding , Models, Molecular , Molecular Conformation , Thiosemicarbazones/chemistry
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